page source_page_order layout_page_order layout_order ref label role_guess included_in_body excluded_risk_level body_decision_reason parser_body_decision_reason production_usage visual_asset_type visual_asset_label visual_asset_caption_preview truncation_marker inside_body_region body_region_id zone column column_index column_count region_id background_rgb background_class is_gray_background has_frame_evidence bbox text_preview cleaned_text_preview text cleaned_text 1 1 1 0 #/texts/0 page_header page_header False low docling_page_header docling_page_header True p1:body_region:0 top_margin column_2_of_3 2 3 p1:top_margin:column_2_of_3:white [255, 255, 255] white False False [224.33, 47.98, 146.5, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 1 2 2 1 #/texts/1 text front_matter_heading False low first_page_metadata first_page_metadata True p1:body_region:0 front_matter column_2_of_3 2 3 p1:front_matter:front_panel:gray [229, 229, 229] gray True False [223.6, 79.88, 151.02, 1.59] Contents lists available at ScienceDirect Contents lists available at ScienceDirect Contents lists available at ScienceDirect Contents lists available at ScienceDirect 1 3 3 2 #/texts/2 section_header title_candidate False low first_page_front_matter_heading first_page_front_matter_heading True p1:body_region:0 front_matter column_2_of_3 2 3 p1:front_matter:front_panel:gray [229, 229, 229] gray True False [204.04, 98.03, 190.03, 12.98] Journal of Energy Chemistry Journal of Energy Chemistry Journal of Energy Chemistry Journal of Energy Chemistry 1 5 4 3 #/texts/4 section_header title_candidate False low first_page_front_matter_heading first_page_front_matter_heading True p1:body_region:0 front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.59, 178.96, 407.61, 29.75] A versatile strategy to activate self-sacrificial templated Li2MnO3 by defect engineering toward advanced lithium storage A versatile strategy to activate self-sacrificial templated Li2MnO3 by defect engineering toward advanced lithium storage A versatile strategy to activate self-sacrificial templated Li2MnO3 by defect engineering toward advanced lithium storage A versatile strategy to activate self-sacrificial templated Li2MnO3 by defect engineering toward advanced lithium storage 1 6 5 4 #/texts/5 text front_matter_candidate False low before_body_started before_body_started True p1:body_region:0 front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.59, 218.76, 497.29, 26.45] Jian-En Zhou a,1 , Yanhua Peng a,1 , Xiaoyan Sang b , Chunlei Wu c , Yiqing Liu a , Zhijian Peng a , Hong Ou a , Yongbo Wu d , Xiaoming Lin a, ⇑ , Yuepeng Cai a, ⇑ Jian-En Zhou a,1 , Yanhua Peng a,1 , Xiaoyan Sang b , Chunlei Wu c , Yiqing Liu a , Zhijian Peng a , Hong Ou a , Yongbo Wu d , Xiaoming Lin a, ⇑ , Yuepeng Cai a, ⇑ Jian-En Zhou a,1 , Yanhua Peng a,1 , Xiaoyan Sang b , Chunlei Wu c , Yiqing Liu a , Zhijian Peng a , Hong Ou a , Yongbo Wu d , Xiaoming Lin a, ⇑ , Yuepeng Cai a, ⇑ Jian-En Zhou a,1 , Yanhua Peng a,1 , Xiaoyan Sang b , Chunlei Wu c , Yiqing Liu a , Zhijian Peng a , Hong Ou a , Yongbo Wu d , Xiaoming Lin a, ⇑ , Yuepeng Cai a, ⇑ 1 7 6 5 #/texts/6 footnote footnote False low first_page_summary first_page_summary True p1:body_region:0 front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.59, 250.75, 505.2, 24.33] a Guangzhou Key Laboratory of Materials for Energy Conversion and Storage, Joint Laboratory of Energy and Materials Chemistry (South China Normal University-Guangzhou Tianci New Materials Co., Ltd.), Key Laboratory of T… a Guangzhou Key Laboratory of Materials for Energy Conversion and Storage, Joint Laboratory of Energy and Materials Chemistry (South China Normal University-Guangzhou Tianci New Materials Co., Ltd.), Key Laboratory of T… a Guangzhou Key Laboratory of Materials for Energy Conversion and Storage, Joint Laboratory of Energy and Materials Chemistry (South China Normal University-Guangzhou Tianci New Materials Co., Ltd.), Key Laboratory of Theoretical Chemistry of Environment, Ministry of Education, School of Chemistry, South China Normal University, Guangzhou 510006, Guangdong, China a Guangzhou Key Laboratory of Materials for Energy Conversion and Storage, Joint Laboratory of Energy and Materials Chemistry (South China Normal University-Guangzhou Tianci New Materials Co., Ltd.), Key Laboratory of Theoretical Chemistry of Environment, Ministry of Education, School of Chemistry, South China Normal University, Guangzhou 510006, Guangdong, China 1 8 7 6 #/texts/7 footnote footnote False low docling_footnote docling_footnote True p1:body_region:0 front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.59, 276.43, 487.59, 15.77] b National Engineering Research Center for Carbohydrate Synthesis, Key Lab of Fluorine and Silicon for Energy Materials and Chemistry of Ministry of Education, Jiangxi Normal University, Nanchang 330022, Jiangxi, China b National Engineering Research Center for Carbohydrate Synthesis, Key Lab of Fluorine and Silicon for Energy Materials and Chemistry of Ministry of Education, Jiangxi Normal University, Nanchang 330022, Jiangxi, China b National Engineering Research Center for Carbohydrate Synthesis, Key Lab of Fluorine and Silicon for Energy Materials and Chemistry of Ministry of Education, Jiangxi Normal University, Nanchang 330022, Jiangxi, China b National Engineering Research Center for Carbohydrate Synthesis, Key Lab of Fluorine and Silicon for Energy Materials and Chemistry of Ministry of Education, Jiangxi Normal University, Nanchang 330022, Jiangxi, China 1 9 8 7 #/texts/8 footnote affiliation False low first_page_author_or_affiliation first_page_author_or_affiliation False None front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.64, 293.55, 300.24, 7.21] c Guangzhou Huifu Research Institute Co., Ltd, Nanxiang San Lu, Guangzhou 510663, Guangdong, China c Guangzhou Huifu Research Institute Co., Ltd, Nanxiang San Lu, Guangzhou 510663, Guangdong, China c Guangzhou Huifu Research Institute Co., Ltd, Nanxiang San Lu, Guangzhou 510663, Guangdong, China c Guangzhou Huifu Research Institute Co., Ltd, Nanxiang San Lu, Guangzhou 510663, Guangdong, China 1 10 9 8 #/texts/9 footnote affiliation False medium first_page_author_or_affiliation first_page_author_or_affiliation True p1:body_region:0 front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.59, 302.17, 509.06, 15.77] d Guangdong Provincial Key Laboratory of Quantum Engineering and Quantum Materials, National Demonstration Center for Experimental Physics Education, School of Physics and Telecommunication Engineering, South China Norm… d Guangdong Provincial Key Laboratory of Quantum Engineering and Quantum Materials, National Demonstration Center for Experimental Physics Education, School of Physics and Telecommunication Engineering, South China Norm… d Guangdong Provincial Key Laboratory of Quantum Engineering and Quantum Materials, National Demonstration Center for Experimental Physics Education, School of Physics and Telecommunication Engineering, South China Normal University, Guangzhou 510006, Guangdong, China d Guangdong Provincial Key Laboratory of Quantum Engineering and Quantum Materials, National Demonstration Center for Experimental Physics Education, School of Physics and Telecommunication Engineering, South China Normal University, Guangzhou 510006, Guangdong, China 1 11 10 9 #/texts/10 section_header front_matter_heading False low front_matter_heading front_matter_heading False None front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.7, 338.58, 94.35, 11.02] a r t i c l e i n f o a r t i c l e i n f o a r t i c l e i n f o a r t i c l e i n f o 1 20 11 10 #/texts/19 section_header abstract_heading False low abstract_heading abstract_heading True p1:body_region:0 front_matter column_2_of_3 2 3 p1:front_matter:column_2_of_3:white [255, 255, 255] white False False [202.22, 338.86, 65.22, 11.02] a b s t r a c t a b s t r a c t a b s t r a c t a b s t r a c t 1 12 12 11 #/texts/11 text front_matter_candidate False low outside_body_flow outside_body_flow False None front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.59, 361.66, 70.81, 31.61] Article history: Received 14 April 2023 Revised 11 May 2023 Accepted 14 May 2023 Article history: Received 14 April 2023 Revised 11 May 2023 Accepted 14 May 2023 Article history: Received 14 April 2023 Revised 11 May 2023 Accepted 14 May 2023 Article history: Received 14 April 2023 Revised 11 May 2023 Accepted 14 May 2023 1 13 13 12 #/texts/12 text metadata False low first_page_metadata first_page_metadata False None front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.59, 395.91, 91.28, 5.93] Available online 26 May 2023 Available online 26 May 2023 Available online 26 May 2023 Available online 26 May 2023 1 14 14 13 #/texts/13 text front_matter_heading False low front_matter_heading front_matter_heading False None front_matter column_1_of_3 1 3 p1:front_matter:column_1_of_3:white [255, 255, 255] white False False [37.59, 415.97, 77.77, 48.79] Keywords: Li2MnO3 Metal-organic framework Oxygen vacancy Lithium-ion battery Electrochemical activity Keywords: Li2MnO3 Metal-organic framework Oxygen vacancy Lithium-ion battery Electrochemical activity Keywords: Li2MnO3 Metal-organic framework Oxygen vacancy Lithium-ion battery Electrochemical activity Keywords: Li2MnO3 Metal-organic framework Oxygen vacancy Lithium-ion battery Electrochemical activity 1 21 15 14 #/texts/20 text front_matter_candidate False low first_page_summary first_page_summary True p1:body_region:0 front_matter column_2_of_3 2 3 p1:front_matter:column_2_of_3:white [255, 255, 255] white False False [202.17, 362.1, 355.49, 169.21] Despite the dazzling theoretical capacity, the devasting electrochemical activity of Li2MnO3 (LMO) caused by the difficult oxidation of Mn 4+ impedes its practical application as the lithium-ion battery (LIB) cathode. T… Despite the dazzling theoretical capacity, the devasting electrochemical activity of Li2MnO3 (LMO) caused by the difficult oxidation of Mn 4+ impedes its practical application as the lithium-ion battery (LIB) cathode. T… Despite the dazzling theoretical capacity, the devasting electrochemical activity of Li2MnO3 (LMO) caused by the difficult oxidation of Mn 4+ impedes its practical application as the lithium-ion battery (LIB) cathode. The efficacious activation of the Li2MnO3 by importing electrochemically active Mn 3+ ions or morphological engineering is instrumental to its lithium storage activity and structural integrity upon cycling. Herein, we propose a conceptual strategy with metal-organic frameworks (MOFs) as selfsacrificial templates to prepare oxygen-deficient Li2MnO3 (Ov-LMO) for exalted lithium storage performance. Attributed to optimized morphological features, LMO materials derived from Mn-BDC (H2BDC = 1,4-dicarboxybenzene) delivered superior cycling/rate performances compared with their counterparts derived from Mn-BTC (H3BTC = 1,3,5-benzenetricarboxylicacid) and Mn-PTC (H4PTC = pyromellitic acid). Both experimental and theoretical studies elucidate the efficacious activation of primitive LMO materials toward advanced lithium storage by importing oxygen deficiencies. Impressively, Ov-LMO derived from Mn-BDC (Ov-BDC-LMO) delivered intriguing reversible capacities (179.2 mA h g 1 at 20 mA g 1 after 200 cycles and 100.1 mA h g 1 at 80 mA g 1 after 300 cycles), which can be attributed to the small particle size that shortens pathways for Li + /electron transport, the enhanced redox activity induced by abundant oxygen vacancies, and the optimized electronic configuration that contributes to the faster lithium diffusivity. This work provides insights into the rational design of LMO by morphological and atomic modulation to direct its activation and practical application as an advanced LIB cathode. Despite the dazzling theoretical capacity, the devasting electrochemical activity of Li2MnO3 (LMO) caused by the difficult oxidation of Mn 4+ impedes its practical application as the lithium-ion battery (LIB) cathode. The efficacious activation of the Li2MnO3 by importing electrochemically active Mn 3+ ions or morphological engineering is instrumental to its lithium storage activity and structural integrity upon cycling. Herein, we propose a conceptual strategy with metal-organic frameworks (MOFs) as selfsacrificial templates to prepare oxygen-deficient Li2MnO3 (Ov-LMO) for exalted lithium storage performance. Attributed to optimized morphological features, LMO materials derived from Mn-BDC (H2BDC = 1,4-dicarboxybenzene) delivered superior cycling/rate performances compared with their counterparts derived from Mn-BTC (H3BTC = 1,3,5-benzenetricarboxylicacid) and Mn-PTC (H4PTC = pyromellitic acid). Both experimental and theoretical studies elucidate the efficacious activation of primitive LMO materials toward advanced lithium storage by importing oxygen deficiencies. Impressively, Ov-LMO derived from Mn-BDC (Ov-BDC-LMO) delivered intriguing reversible capacities (179.2 mA h g 1 at 20 mA g 1 after 200 cycles and 100.1 mA h g 1 at 80 mA g 1 after 300 cycles), which can be attributed to the small particle size that shortens pathways for Li + /electron transport, the enhanced redox activity induced by abundant oxygen vacancies, and the optimized electronic configuration that contributes to the faster lithium diffusivity. This work provides insights into the rational design of LMO by morphological and atomic modulation to direct its activation and practical application as an advanced LIB cathode. 1 22 16 15 #/texts/21 text metadata False low first_page_metadata first_page_metadata True p1:body_region:0 front_matter column_2_of_3 2 3 p1:front_matter:column_2_of_3:white [255, 255, 255] white False False [202.17, 532.25, 355.42, 18.23] Ó 2023 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by ELSEVIER B.V. and Science Press. All rights reserved. Ó 2023 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by ELSEVIER B.V. and Science Press. Ó 2023 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by ELSEVIER B.V. and Science Press. All rights reserved. Ó 2023 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by ELSEVIER B.V. and Science Press. 1 15 17 16 #/texts/14 section_header body_heading False low body_heading body_heading False None body_zone column_1_of_3 1 3 p1:body_zone:column_1_of_3:white [255, 255, 255] white False False [37.7, 605.71, 60.13, 7.96] 1. Introduction 1. Introduction 1. Introduction 1. Introduction 1 17 19 18 #/texts/16 footnote footnote False low first_page_metadata first_page_metadata False None body_zone column_1_of_3 1 3 p1:body_zone:column_1_of_3:white [255, 255, 255] white False False [42.07, 692.51, 78.23, 13.76] ⇑ Corresponding authors. ⇑ Corresponding authors. ⇑ Corresponding authors. ⇑ Corresponding authors. 1 18 20 19 #/texts/17 footnote footnote False low first_page_metadata first_page_metadata False None body_zone column_1_of_3 1 3 p1:body_zone:column_1_of_3:off_white [247, 250, 251] off_white False False [48.81, 705.11, 220.95, 5.93] E-mail addresses: linxm@scnu.edu.cn (X. Lin), caiyp@scnu.edu.cn (Y. Cai). E-mail addresses: linxm@scnu.edu.cn (X. Lin), caiyp@scnu.edu.cn (Y. Cai). E-mail addresses: linxm@scnu.edu.cn (X. Lin), caiyp@scnu.edu.cn (Y. Cai). E-mail addresses: linxm@scnu.edu.cn (X. Lin), caiyp@scnu.edu.cn (Y. Cai). 1 19 21 20 #/texts/18 footnote footnote False low docling_footnote docling_footnote False None body_zone column_1_of_3 1 3 p1:body_zone:column_1_of_3:white [255, 255, 255] white False False [43.09, 712.68, 148.31, 7.21] 1 These authors contributed equally to this work. 1 These authors contributed equally to this work. 1 These authors contributed equally to this work. 1 These authors contributed equally to this work. 1 25 22 21 #/texts/24 page_footer page_footer False low first_page_metadata first_page_metadata False None bottom_margin column_1_of_3 1 3 p1:bottom_margin:column_1_of_3:white [255, 255, 255] white False True [37.59, 731.92, 136.91, 5.93] https://doi.org/10.1016/j.jechem.2023.05.014 https://doi.org/10.1016/j.jechem.2023.05.014 1 4 23 22 #/texts/3 text front_matter_candidate False low outside_body_flow outside_body_flow True p1:body_region:0 front_matter column_2_of_3 2 3 p1:front_matter:front_panel:gray [229, 229, 229] gray True True [176.71, 135.67, 247.4, 1.59] j o u r n a l homepage: www.elsevier.com/locate/jechem j o u r n a l homepage: j o u r n a l homepage: www.elsevier.com/locate/jechem j o u r n a l homepage: 1 26 26 25 #/texts/25 page_footer page_footer False low first_page_metadata first_page_metadata True p1:body_region:0 bottom_margin column_1_of_3 1 3 p1:bottom_margin:column_1_of_3:white [255, 255, 255] white False False [37.59, 738.73, 520.05, 8.3] 2095-4956/ Ó 2023 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by ELSEVIER B.V. and Science Press. All rights reserved. 2095-4956/ Ó 2023 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by ELSEVIER B.V. and Science Press. 2095-4956/ Ó 2023 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by ELSEVIER B.V. and Science Press. All rights reserved. 2095-4956/ Ó 2023 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by ELSEVIER B.V. and Science Press. 2 1 1 26 #/texts/26 page_header page_header False low docling_page_header docling_page_header True p2:body_region:0 top_margin column_1_of_2 1 2 p2:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 2 2 5 30 #/texts/27 page_header page_header False low docling_page_header docling_page_header True p2:body_region:1 top_margin column_2_of_2 2 2 p2:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.77, 48.15, 139.86, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 2 8 8 33 #/texts/32 section_header body_heading False low body_heading body_heading True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.65, 433.65, 62.99, 7.96] 2. Experimental 2. Experimental 2. Experimental 2. Experimental 2 9 9 34 #/texts/33 section_header body_heading False low body_heading body_heading True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.65, 455.0, 90.87, 7.42] 2.1. Material preparation 2.1. Material preparation 2.1. Material preparation 2.1. Material preparation 2 12 12 37 #/texts/36 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p2:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 165 165 165 165 3 1 1 38 #/texts/37 page_header page_header False low docling_page_header docling_page_header True p3:body_region:0 top_margin column_1_of_2 1 2 p3:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 3 4 3 40 #/texts/40 section_header body_heading False low body_heading body_heading True p3:body_region:0 body_zone column_1_of_2 1 2 p3:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.7, 99.31, 106.87, 7.42] 2.2. Material characterization 2.2. Material characterization 2.2. Material characterization 2.2. Material characterization 3 6 5 42 #/texts/42 section_header body_heading False low body_heading body_heading True p3:body_region:0 body_zone column_1_of_2 1 2 p3:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.7, 360.83, 123.51, 7.42] 2.3. Electrochemical measurement 2.3. Electrochemical measurement 2.3. Electrochemical measurement 2.3. Electrochemical measurement 3 8 7 44 #/texts/44 section_header body_heading False low body_heading body_heading True p3:body_region:0 body_zone column_1_of_2 1 2 p3:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.7, 706.04, 77.39, 7.42] 2.4. Theoretical study 2.4. Theoretical study 2.4. Theoretical study 2.4. Theoretical study 3 2 9 46 #/texts/38 page_header page_header False low docling_page_header docling_page_header True p3:body_region:1 top_margin column_2_of_2 2 2 p3:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.71, 48.21, 139.91, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 3 11 11 48 #/texts/46 section_header body_heading False low body_heading body_heading True p3:body_region:1 body_zone column_2_of_2 2 2 p3:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.65, 213.96, 99.65, 7.96] 3. Results and discussion 3. Results and discussion 3. Results and discussion 3. Results and discussion 3 12 12 49 #/texts/47 section_header body_heading False low body_heading body_heading True p3:body_region:1 body_zone column_2_of_2 2 2 p3:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.65, 235.31, 160.25, 7.42] 3.1. Structural and morphological properties 3.1. Structural and morphological properties 3.1. Structural and morphological properties 3.1. Structural and morphological properties 3 16 16 53 #/texts/51 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p3:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 166 166 166 166 4 3 1 54 #/texts/52 page_header page_header False low docling_page_header docling_page_header False None top_margin left None None p4:top_margin:left:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 4 4 2 55 #/texts/53 page_header page_header False low docling_page_header docling_page_header False None top_margin right None None p4:top_margin:right:white [255, 255, 255] white False False [417.77, 48.15, 139.86, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 4 5 3 56 #/texts/54 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body full None None p4:page_body:full:white [255, 255, 255] white False False [37.59, 689.57, 520.05, 14.84] Fig. 1. (a) The synthetic procedure of Ov-BDC-LMO, Ov-BTC-LMO, and Ov-PTC-LMO. XRD patterns of (b) (Ov-)BDC-LMO, (e) (Ov-)BTC-LMO, and (h) (Ov-)PTC-LMO. Rietveld refinements of (c) Ov-BDC-LMO, (d) BDC-LMO, (f) Ov-BTC-LM… Fig. 1. (a) The synthetic procedure of Ov-BDC-LMO, Ov-BTC-LMO, and Ov-PTC-LMO. XRD patterns of (b) (Ov-)BDC-LMO, (e) (Ov-)BTC-LMO, and (h) (Ov-)PTC-LMO. Rietveld refinements of (c) Ov-BDC-LMO, (d) BDC-LMO, (f) Ov-BTC-LM… Fig. 1. (a) The synthetic procedure of Ov-BDC-LMO, Ov-BTC-LMO, and Ov-PTC-LMO. XRD patterns of (b) (Ov-)BDC-LMO, (e) (Ov-)BTC-LMO, and (h) (Ov-)PTC-LMO. Rietveld refinements of (c) Ov-BDC-LMO, (d) BDC-LMO, (f) Ov-BTC-LMO, (g) BTC-LMO, (i) Ov-PTC-LMO, and (j) PTC-LMO. Fig. 1. (a) The synthetic procedure of Ov-BDC-LMO, Ov-BTC-LMO, and Ov-PTC-LMO. XRD patterns of (b) (Ov-)BDC-LMO, (e) (Ov-)BTC-LMO, and (h) (Ov-)PTC-LMO. Rietveld refinements of (c) Ov-BDC-LMO, (d) BDC-LMO, (f) Ov-BTC-LMO, (g) BTC-LMO, (i) Ov-PTC-LMO, and (j) PTC-LMO. 4 6 6 59 #/texts/55 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin left_crossing None None p4:bottom_margin:left_crossing:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 167 167 167 167 5 2 1 60 #/texts/56 page_header page_header False low docling_page_header docling_page_header True p5:body_region:0 top_margin column_1_of_2 1 2 p5:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 5 3 2 61 #/texts/57 page_header page_header False low docling_page_header docling_page_header True p5:body_region:1 top_margin column_2_of_2 2 2 p5:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.71, 48.21, 139.91, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 5 4 3 62 #/texts/58 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p5:page_body:column_1_of_2:white [255, 255, 255] white False False [37.59, 576.81, 520.03, 14.84] Fig. 2. (a-c) The panoramic Raman spectra and the high-resolution XPS spectra of (d-f) Li 1 s , (g-i) O 1 s , and (j-l) Mn 2 p for (Ov-)BDC-LMO, (Ov-)BTC-LMO, and (Ov-)PTC-LMO, respectively. Fig. 2. (a-c) The panoramic Raman spectra and the high-resolution XPS spectra of (d-f) Li 1 s , (g-i) O 1 s , and (j-l) Mn 2 p for (Ov-)BDC-LMO, (Ov-)BTC-LMO, and (Ov-)PTC-LMO, respectively. Fig. 2. (a-c) The panoramic Raman spectra and the high-resolution XPS spectra of (d-f) Li 1 s , (g-i) O 1 s , and (j-l) Mn 2 p for (Ov-)BDC-LMO, (Ov-)BTC-LMO, and (Ov-)PTC-LMO, respectively. Fig. 2. (a-c) The panoramic Raman spectra and the high-resolution XPS spectra of (d-f) Li 1 s , (g-i) O 1 s , and (j-l) Mn 2 p for (Ov-)BDC-LMO, (Ov-)BTC-LMO, and (Ov-)PTC-LMO, respectively. 5 7 7 66 #/texts/61 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p5:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 168 168 168 168 6 2 1 67 #/texts/62 page_header page_header False low docling_page_header docling_page_header True p6:body_region:0 top_margin column_1_of_2 1 2 p6:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 6 3 4 70 #/texts/63 page_header page_header False low docling_page_header docling_page_header True p6:body_region:1 top_margin column_2_of_2 2 2 p6:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.77, 48.15, 139.86, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 6 8 8 74 #/texts/67 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p6:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 169 169 169 169 7 2 1 75 #/texts/68 page_header page_header False low docling_page_header docling_page_header True p7:body_region:0 top_margin column_1_of_2 1 2 p7:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 7 3 2 76 #/texts/69 page_header page_header False low docling_page_header docling_page_header True p7:body_region:1 top_margin column_2_of_2 2 2 p7:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.71, 48.21, 139.91, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 7 4 3 77 #/texts/70 caption caption False low outside_body_flow_caption outside_body_flow_caption False None front_matter column_1_of_2 1 2 p7:front_matter:column_1_of_2:white [255, 255, 255] white False False [51.02, 441.88, 493.16, 6.37] Fig. 3. The SEM images of (a) Mn-BDC, (b) BDC-LMO, (c) Ov-BDC-LMO, (d) Mn-BTC, (e) BTC-LMO, (f) Ov-BTC-LMO, (g) Mn-PTC, (h) PTC-LMO, and (i) Ov-PTC-LMO. Fig. 3. The SEM images of (a) Mn-BDC, (b) BDC-LMO, (c) Ov-BDC-LMO, (d) Mn-BTC, (e) BTC-LMO, (f) Ov-BTC-LMO, (g) Mn-PTC, (h) PTC-LMO, and (i) Ov-PTC-LMO. Fig. 3. The SEM images of (a) Mn-BDC, (b) BDC-LMO, (c) Ov-BDC-LMO, (d) Mn-BTC, (e) BTC-LMO, (f) Ov-BTC-LMO, (g) Mn-PTC, (h) PTC-LMO, and (i) Ov-PTC-LMO. Fig. 3. The SEM images of (a) Mn-BDC, (b) BDC-LMO, (c) Ov-BDC-LMO, (d) Mn-BTC, (e) BTC-LMO, (f) Ov-BTC-LMO, (g) Mn-PTC, (h) PTC-LMO, and (i) Ov-PTC-LMO. 7 5 5 79 #/texts/71 section_header body_heading False low body_heading body_heading True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.7, 716.52, 110.65, 7.42] 3.2. Electrochemical properties 3.2. Electrochemical properties 3.2. Electrochemical properties 3.2. Electrochemical properties 7 9 9 83 #/texts/74 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p7:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.38, 5.93] 170 170 170 170 8 3 1 84 #/texts/75 page_header page_header False low docling_page_header docling_page_header True p8:body_region:0 top_margin column_1_of_2 1 2 p8:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 8 4 2 85 #/texts/76 page_header page_header False low docling_page_header docling_page_header True p8:body_region:1 top_margin column_2_of_2 2 2 p8:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.77, 48.15, 139.86, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 8 5 3 86 #/texts/77 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p8:page_body:column_1_of_2:white [255, 255, 255] white False False [37.59, 603.74, 520.03, 14.84] Fig. 4. (a-f) TEM images, (g-l) HRTEM images, (m-r) SAED patterns, and (s-x) HAADF-STEM images and corresponding element mappings of BDC-LMO, BTC-LMO, PTC-LMO, Ov-BDC-LMO, Ov-BTC-LMO, and Ov-PTC-LMO, respectively. Fig. 4. (a-f) TEM images, (g-l) HRTEM images, (m-r) SAED patterns, and (s-x) HAADF-STEM images and corresponding element mappings of BDC-LMO, BTC-LMO, PTC-LMO, Ov-BDC-LMO, Ov-BTC-LMO, and Ov-PTC-LMO, respectively. Fig. 4. (a-f) TEM images, (g-l) HRTEM images, (m-r) SAED patterns, and (s-x) HAADF-STEM images and corresponding element mappings of BDC-LMO, BTC-LMO, PTC-LMO, Ov-BDC-LMO, Ov-BTC-LMO, and Ov-PTC-LMO, respectively. Fig. 4. (a-f) TEM images, (g-l) HRTEM images, (m-r) SAED patterns, and (s-x) HAADF-STEM images and corresponding element mappings of BDC-LMO, BTC-LMO, PTC-LMO, Ov-BDC-LMO, Ov-BTC-LMO, and Ov-PTC-LMO, respectively. 8 6 6 89 #/texts/78 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p8:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 171 171 171 171 9 2 1 90 #/texts/79 page_header page_header False low docling_page_header docling_page_header False None top_margin column_1_of_2 1 2 p9:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 9 3 2 91 #/texts/80 page_header page_header False low docling_page_header docling_page_header False None top_margin column_2_of_2 2 2 p9:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.71, 48.21, 139.91, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 9 4 3 92 #/texts/81 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p9:page_body:column_1_of_2:white [255, 255, 255] white False False [37.59, 629.65, 520.04, 14.9] Fig. 5. (a-f) Spherical aberration-corrected HAADF-STEM and (g-l) spherical aberration-corrected ABF-STEM images for BDC-LMO, BTC-LMO, PTC-LMO, Ov-BDC-LMO, OvBTC-LMO, and Ov-PTC-LMO, respectively. Fig. 5. (a-f) Spherical aberration-corrected HAADF-STEM and (g-l) spherical aberration-corrected ABF-STEM images for BDC-LMO, BTC-LMO, PTC-LMO, Ov-BDC-LMO, OvBTC-LMO, and Ov-PTC-LMO, respectively. Fig. 5. (a-f) Spherical aberration-corrected HAADF-STEM and (g-l) spherical aberration-corrected ABF-STEM images for BDC-LMO, BTC-LMO, PTC-LMO, Ov-BDC-LMO, OvBTC-LMO, and Ov-PTC-LMO, respectively. Fig. 5. (a-f) Spherical aberration-corrected HAADF-STEM and (g-l) spherical aberration-corrected ABF-STEM images for BDC-LMO, BTC-LMO, PTC-LMO, Ov-BDC-LMO, OvBTC-LMO, and Ov-PTC-LMO, respectively. 9 6 6 95 #/texts/83 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p9:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 172 172 172 172 10 1 1 96 #/texts/84 page_header page_header False low docling_page_header docling_page_header True p10:body_region:0 top_margin column_1_of_2 1 2 p10:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 10 2 2 97 #/texts/85 page_header page_header False low docling_page_header docling_page_header True p10:body_region:1 top_margin column_2_of_2 2 2 p10:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.77, 48.15, 139.86, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 10 3 3 98 #/texts/86 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p10:page_body:column_1_of_2:white [255, 255, 255] white False False [37.59, 530.55, 520.08, 24.48] Fig. 6. The cycling performance at 20 mA g 1 for 200 loops of (a) (Ov-)BDC-LMO, (b) (Ov-)BTC-LMO, and (c) (Ov-)PTC-LMO. The rate performance at 0.1, 0.2, 0.4, 1, and 2 C (1 C = 200 mA g 1 ) of (d) (Ov-)BDC-LMO, (e) … Fig. 6. The cycling performance at 20 mA g 1 for 200 loops of (a) (Ov-)BDC-LMO, (b) (Ov-)BTC-LMO, and (c) (Ov-)PTC-LMO. The rate performance at 0.1, 0.2, 0.4, 1, and 2 C (1 C = 200 mA g 1 ) of (d) (Ov-)BDC-LMO, (e) … Fig. 6. The cycling performance at 20 mA g 1 for 200 loops of (a) (Ov-)BDC-LMO, (b) (Ov-)BTC-LMO, and (c) (Ov-)PTC-LMO. The rate performance at 0.1, 0.2, 0.4, 1, and 2 C (1 C = 200 mA g 1 ) of (d) (Ov-)BDC-LMO, (e) (Ov-)BTC-LMO, and (f) (Ov-)PTC-LMO. The GCD profiles at the 1st, 25th, 50th, and 100th cycle during the cycling test at 20 mA g 1 of (g) Ov-BDC-LMO, (h) Ov-BTC-LMO, and (i) Ov-PTC-LMO. Nyquist plots after 100 cycles at 20 mA g 1 for (j) (Ov-)BDC-LMO, (k) (Ov-)BTC-LMO, and (l) (Ov-)PTC-LMO. Fig. 6. The cycling performance at 20 mA g 1 for 200 loops of (a) (Ov-)BDC-LMO, (b) (Ov-)BTC-LMO, and (c) (Ov-)PTC-LMO. The rate performance at 0.1, 0.2, 0.4, 1, and 2 C (1 C = 200 mA g 1 ) of (d) (Ov-)BDC-LMO, (e) (Ov-)BTC-LMO, and (f) (Ov-)PTC-LMO. The GCD profiles at the 1st, 25th, 50th, and 100th cycle during the cycling test at 20 mA g 1 of (g) Ov-BDC-LMO, (h) Ov-BTC-LMO, and (i) Ov-PTC-LMO. Nyquist plots after 100 cycles at 20 mA g 1 for (j) (Ov-)BDC-LMO, (k) (Ov-)BTC-LMO, and (l) (Ov-)PTC-LMO. 10 7 7 102 #/texts/89 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p10:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 173 173 173 173 11 2 1 103 #/texts/90 page_header page_header False low docling_page_header docling_page_header True p11:body_region:0 top_margin column_1_of_2 1 2 p11:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 11 3 6 108 #/texts/91 page_header page_header False low docling_page_header docling_page_header True p11:body_region:1 top_margin column_2_of_2 2 2 p11:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.71, 48.21, 139.91, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 11 10 10 112 #/texts/97 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p11:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 174 174 174 174 12 1 1 113 #/texts/98 page_header page_header False low docling_page_header docling_page_header False None top_margin left None None p12:top_margin:left:white [255, 255, 255] white False False [37.59, 48.2, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 12 2 2 114 #/texts/99 page_header page_header False low docling_page_header docling_page_header False None top_margin right None None p12:top_margin:right:white [255, 255, 255] white False False [417.77, 48.15, 139.86, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 12 3 3 115 #/texts/100 caption caption False low outside_body_flow_caption outside_body_flow_caption False None bottom_margin full None None p12:bottom_margin:full:white [255, 255, 255] white False False [37.59, 714.69, 520.07, 24.53] Fig. 7. The CV curves for the first 3 cycles at 0.2 mV s 1 for (a) Ov-BDC-LMO, (b) Ov-BTC-LMO, (c) Ov-PTC-LMO, (d) BDC-LMO, (e) BTC-LMO, and (f) PTC-LMO. The schematic illustrations of the first cycle for (g) Ov-LMO a… Fig. 7. The CV curves for the first 3 cycles at 0.2 mV s 1 for (a) Ov-BDC-LMO, (b) Ov-BTC-LMO, (c) Ov-PTC-LMO, (d) BDC-LMO, (e) BTC-LMO, and (f) PTC-LMO. The schematic illustrations of the first cycle for (g) Ov-LMO a… Fig. 7. The CV curves for the first 3 cycles at 0.2 mV s 1 for (a) Ov-BDC-LMO, (b) Ov-BTC-LMO, (c) Ov-PTC-LMO, (d) BDC-LMO, (e) BTC-LMO, and (f) PTC-LMO. The schematic illustrations of the first cycle for (g) Ov-LMO and (h) LMO. The separation of the pseudocapacitive contribution at 0.4 mV s 1 for (i) Ov-BDC-LMO, (j) Ov-BTC-LMO, and (k) OvPTC-LMO. The pseudocapacitive contribution ratios at 0.2-1.0 mV s 1 for (l) Ov-BDC-LMO, (m) Ov-BTC-LMO, and (n) Ov-PTC-LMO. Fig. 7. The CV curves for the first 3 cycles at 0.2 mV s 1 for (a) Ov-BDC-LMO, (b) Ov-BTC-LMO, (c) Ov-PTC-LMO, (d) BDC-LMO, (e) BTC-LMO, and (f) PTC-LMO. The schematic illustrations of the first cycle for (g) Ov-LMO and (h) LMO. The separation of the pseudocapacitive contribution at 0.4 mV s 1 for (i) Ov-BDC-LMO, (j) Ov-BTC-LMO, and (k) OvPTC-LMO. The pseudocapacitive contribution ratios at 0.2-1.0 mV s 1 for (l) Ov-BDC-LMO, (m) Ov-BTC-LMO, and (n) Ov-PTC-LMO. 12 4 4 116 #/texts/101 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin right_crossing None None p12:bottom_margin:right_crossing:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 175 175 175 175 13 2 1 117 #/texts/102 page_header page_header False low docling_page_header docling_page_header True p13:body_region:0 top_margin column_1_of_2 1 2 p13:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 13 3 5 121 #/texts/103 page_header page_header False low docling_page_header docling_page_header True p13:body_region:1 top_margin column_2_of_2 2 2 p13:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.71, 48.21, 139.91, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 13 9 9 125 #/texts/108 section_header body_heading False low body_heading body_heading True p13:body_region:1 body_zone column_2_of_2 2 2 p13:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.65, 680.01, 97.57, 7.42] 3.3. DFT calculation results 3.3. DFT calculation results 3.3. DFT calculation results 3.3. DFT calculation results 13 11 11 127 #/texts/110 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p13:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 176 176 176 176 14 2 1 128 #/texts/111 page_header page_header False low docling_page_header docling_page_header True p14:body_region:0 top_margin column_1_of_2 1 2 p14:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.21, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 14 3 2 129 #/texts/112 page_header page_header False low docling_page_header docling_page_header True p14:body_region:1 top_margin column_2_of_2 2 2 p14:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.77, 48.15, 139.86, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 14 4 3 130 #/texts/113 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p14:page_body:column_1_of_2:white [255, 255, 255] white False False [37.59, 575.68, 520.03, 31.96] Fig. 8. The single-step profiles of GITT titration during the charging process for (a) Ov-BDC-LMO, (b) Ov-BTC-LMO, and (c) Ov-PTC-LMO. The GITT curves of (d) Ov-BDC-LMO, (e) Ov-BTC-LMO, and (f) Ov-PTC-LMO. (g) The calcu… Fig. 8. The single-step profiles of GITT titration during the charging process for (a) Ov-BDC-LMO, (b) Ov-BTC-LMO, and (c) Ov-PTC-LMO. The GITT curves of (d) Ov-BDC-LMO, (e) Ov-BTC-LMO, and (f) Ov-PTC-LMO. (g) The calcu… Fig. 8. The single-step profiles of GITT titration during the charging process for (a) Ov-BDC-LMO, (b) Ov-BTC-LMO, and (c) Ov-PTC-LMO. The GITT curves of (d) Ov-BDC-LMO, (e) Ov-BTC-LMO, and (f) Ov-PTC-LMO. (g) The calculated Li + diffusion coefficients upon charging for all samples. (h) The schematic illustration of the mechanism of boosted lithium diffusion for Ov-LMO samples. (i) Ex situ XRD patterns at different cycling states (before cycling, after 50 cycles, and after 100 cycles) and (j) Ex situ high-resolution XPS spectra at different charge/discharge states (before charging, charge to 4.7 V, and discharge to 2.5 V) of Mn 2 p for Ov-BDC-LMO during the initial cycle. Fig. 8. The single-step profiles of GITT titration during the charging process for (a) Ov-BDC-LMO, (b) Ov-BTC-LMO, and (c) Ov-PTC-LMO. The GITT curves of (d) Ov-BDC-LMO, (e) Ov-BTC-LMO, and (f) Ov-PTC-LMO. (g) The calculated Li + diffusion coefficients upon charging for all samples. (h) The schematic illustration of the mechanism of boosted lithium diffusion for Ov-LMO samples. (i) Ex situ XRD patterns at different cycling states (before cycling, after 50 cycles, and after 100 cycles) and (j) Ex situ high-resolution XPS spectra at different charge/discharge states (before charging, charge to 4.7 V, and discharge to 2.5 V) of Mn 2 p for Ov-BDC-LMO during the initial cycle. 14 8 8 135 #/texts/116 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p14:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 177 177 177 177 15 1 1 136 #/texts/117 page_header page_header False low docling_page_header docling_page_header False None top_margin left None None p15:top_margin:left:white [255, 255, 255] white False False [37.59, 48.2, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 15 2 2 137 #/texts/118 page_header page_header False low docling_page_header docling_page_header False None top_margin right None None p15:top_margin:right:white [255, 255, 255] white False False [417.71, 48.2, 139.91, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 15 3 3 138 #/texts/119 caption caption False low outside_body_flow_caption outside_body_flow_caption False None bottom_margin full None None p15:bottom_margin:full:white [255, 255, 255] white False False [37.59, 715.76, 520.05, 23.46] Fig. 9. The optimized models of (a) LMO and (b) Ov-LMO. (c) The 3D differential charge density distribution of Ov-LMO. (d) The TDOS curves of LMO and Ov-LMO. The PDOS curves of (e) LMO and (f) Ov-LMO. The energy barrier… Fig. 9. The optimized models of (a) LMO and (b) Ov-LMO. (c) The 3D differential charge density distribution of Ov-LMO. (d) The TDOS curves of LMO and Ov-LMO. The PDOS curves of (e) LMO and (f) Ov-LMO. The energy barrier… Fig. 9. The optimized models of (a) LMO and (b) Ov-LMO. (c) The 3D differential charge density distribution of Ov-LMO. (d) The TDOS curves of LMO and Ov-LMO. The PDOS curves of (e) LMO and (f) Ov-LMO. The energy barriers during delithiation for (g) LMO and (h) Ov-LMO. The lithium vacancy migration paths and corresponding energy barrier curves for (i) LMO and (j) Ov-LMO. Fig. 9. The optimized models of (a) LMO and (b) Ov-LMO. (c) The 3D differential charge density distribution of Ov-LMO. (d) The TDOS curves of LMO and Ov-LMO. The PDOS curves of (e) LMO and (f) Ov-LMO. The energy barriers during delithiation for (g) LMO and (h) Ov-LMO. The lithium vacancy migration paths and corresponding energy barrier curves for (i) LMO and (j) Ov-LMO. 15 4 4 139 #/texts/120 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin left_crossing None None p15:bottom_margin:left_crossing:white [255, 255, 255] white False False [291.91, 764.24, 11.45, 5.93] 178 178 178 178 16 2 1 140 #/texts/121 page_header page_header False low docling_page_header docling_page_header True p16:body_region:0 top_margin column_1_of_2 1 2 p16:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 48.2, 93.88, 5.93] J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. J.-E. Zhou, Y. Peng, X. Sang et al. 16 7 6 145 #/texts/126 section_header body_heading False low body_heading body_heading True p16:body_region:0 body_zone column_1_of_2 1 2 p16:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.7, 716.09, 57.15, 7.96] 4. Conclusions 4. Conclusions 4. Conclusions 4. Conclusions 16 3 8 147 #/texts/122 page_header page_header False low docling_page_header docling_page_header True p16:body_region:1 top_margin column_2_of_2 2 2 p16:top_margin:column_2_of_2:white [255, 255, 255] white False False [417.77, 48.15, 139.86, 5.93] Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 Journal of Energy Chemistry 85 (2023) 164-180 16 10 10 149 #/texts/128 section_header back_matter_heading False low back_matter_heading back_matter_heading stop_trigger True p16:body_region:1 front_matter column_2_of_2 2 2 p16:front_matter:column_2_of_2:white [255, 255, 255] white False False [306.6, 298.54, 134.88, 7.96] Declaration of competing interest Declaration of competing interest Declaration of competing interest Declaration of competing interest 16 11 11 150 #/texts/129 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p16:body_region:1 front_matter column_2_of_2 2 2 p16:front_matter:column_2_of_2:white [255, 255, 255] white False False [306.6, 319.9, 251.12, 28.34] The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper. The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper. The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper. The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper. 16 12 12 151 #/texts/130 section_header back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p16:body_region:1 front_matter column_2_of_2 2 2 p16:front_matter:column_2_of_2:white [255, 255, 255] white False False [306.6, 362.22, 73.61, 7.96] Acknowledgments Acknowledgments Acknowledgments Acknowledgments 16 13 13 152 #/texts/131 text back_matter_text False low after_back_matter_stop after_back_matter_stop after_stop True p16:body_region:1 front_matter column_2_of_2 2 2 p16:front_matter:column_2_of_2:white [255, 255, 255] white False False [306.6, 383.57, 251.08, 101.58] We gratefully acknowledge the financial support from the Special Funds for the Cultivation of Guangdong College Students' Scientific and Technological Innovation (''Climbing Program' Special Funds, pdjh2023b0145), the R… We gratefully acknowledge the financial support from the Special Funds for the Cultivation of Guangdong College Students' Scientific and Technological Innovation (''Climbing Program' Special Funds, pdjh2023b0145), the R… We gratefully acknowledge the financial support from the Special Funds for the Cultivation of Guangdong College Students' Scientific and Technological Innovation (''Climbing Program' Special Funds, pdjh2023b0145), the Research and Development Plan Project in Key Fields of Guangdong Province (2020B0101030005), the Applied special project of Guangdong Provincial Science and Technology Plan (2017B090917002), and the Basic and Applied Basic Research Fund of Guangdong Province (2019B1515120027). Furthermore, the authors would like to thank the Shiyanjia lab (https://www.shiyanjia.com) for the TEM test. We gratefully acknowledge the financial support from the Special Funds for the Cultivation of Guangdong College Students' Scientific and Technological Innovation (''Climbing Program' Special Funds, pdjh2023b0145), the Research and Development Plan Project in Key Fields of Guangdong Province (2020B0101030005), the Applied special project of Guangdong Provincial Science and Technology Plan (2017B090917002), and the Basic and Applied Basic Research Fund of Guangdong Province (2019B1515120027). Furthermore, the authors would like to thank the Shiyanjia lab ( for the TEM test. 16 14 14 153 #/texts/132 section_header unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p16:body_region:1 front_matter column_2_of_2 2 2 p16:front_matter:column_2_of_2:white [255, 255, 255] white False False [306.65, 500.83, 147.31, 7.96] Appendix A. Supplementary material Appendix A. Supplementary material Appendix A. Supplementary material Appendix A. Supplementary material 16 15 15 154 #/texts/133 text reference False low after_back_matter_stop after_back_matter_stop after_stop True p16:body_region:1 front_matter column_2_of_2 2 2 p16:front_matter:column_2_of_2:white [255, 255, 255] white False False [306.6, 522.18, 251.04, 17.91] Supplementary data to this article can be found online at https://doi.org/10.1016/j.jechem.2023.05.014. Supplementary data to this article can be found online at Supplementary data to this article can be found online at https://doi.org/10.1016/j.jechem.2023.05.014. 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