page source_page_order layout_page_order layout_order ref label role_guess included_in_body excluded_risk_level body_decision_reason parser_body_decision_reason production_usage visual_asset_type visual_asset_label visual_asset_caption_preview truncation_marker inside_body_region body_region_id zone column column_index column_count region_id background_rgb background_class is_gray_background has_frame_evidence bbox text_preview cleaned_text_preview 1 1 1 0 #/texts/0 page_header page_header False low docling_page_header docling_page_header True p1:body_region:1 top_margin column_2_of_2 2 2 p1:top_margin:column_2_of_2:white [255, 255, 255] white False False [224.72, 33.45, 145.08, 11.73] Journal of Power Sources 580 (2023) 233437 Journal of Power Sources 580 (2023) 233437 1 2 2 1 #/texts/1 section_header front_matter_heading False low first_page_metadata first_page_metadata True p1:body_region:1 front_matter column_2_of_2 2 2 p1:front_matter:front_panel:gray [230, 230, 230] gray True False [228.42, 63.48, 142.99, 7.31] Contents lists available at ScienceDirect Contents lists available at ScienceDirect 1 3 3 2 #/texts/2 section_header title_candidate False low first_page_front_matter_heading first_page_front_matter_heading True p1:body_region:1 front_matter column_2_of_2 2 2 p1:front_matter:front_panel:gray [230, 230, 230] gray True False [219.29, 87.36, 163.01, 12.79] Journal of Power Sources Journal of Power Sources 1 4 4 3 #/texts/3 text front_matter_heading False low first_page_metadata first_page_metadata True p1:body_region:1 front_matter column_2_of_2 2 2 p1:front_matter:front_panel:gray [230, 230, 230] gray True False [195.48, 119.22, 208.78, 6.67] journal homepage: www.elsevier.com/locate/jpowsour journal homepage: 1 5 5 4 #/texts/4 section_header title_candidate False low first_page_front_matter_heading first_page_front_matter_heading True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 168.03, 450.29, 46.81] Efficient improvement in electrochemical properties of high-voltage Li-rich Mn-based layered oxide cathode by addition of 1,3-divinyltetramethyldisiloxane to electrolyte Efficient improvement in electrochemical properties of high-voltage Li-rich Mn-based layered oxide cathode by addition of 1,3-divinyltetramethyldisiloxane to electrolyte 1 6 6 5 #/texts/5 text affiliation False low first_page_author_or_affiliation first_page_author_or_affiliation True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 229.44, 339.84, 9.69] Tao Huang, Xiangzhen Zheng, Chunfeng Yan, Ying Pan , Maoxiang Wu Tao Huang, Xiangzhen Zheng, Chunfeng Yan, Ying Pan , Maoxiang Wu 1 8 7 6 #/texts/7 text affiliation False low first_page_author_or_affiliation first_page_author_or_affiliation True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 248.69, 437.99, 5.85] Key Laboratory of Optoelectronic Materials Chemistry and Physics, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Key Laboratory of Optoelectronic Materials Chemistry and Physics, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, 1 9 8 7 #/texts/8 text unknown_text False low before_body_started before_body_started True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 257.25, 56.39, 5.85] 350002, PR China 350002, PR China 1 10 9 8 #/texts/9 section_header front_matter_heading False low front_matter_heading front_matter_heading True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 289.44, 75.13, 6.4] H I G H L I G H T S H I G H L I G H T S 1 11 10 9 #/texts/10 list_item front_matter_candidate False low outside_body_flow_list_item outside_body_flow_list_item True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 308.87, 231.27, 6.58] DTMS improved cyclic stability of LRM cathode lithium-ion batteries. DTMS improved cyclic stability of LRM cathode lithium-ion batteries. 1 12 11 10 #/texts/11 list_item unknown_text False medium outside_body_flow_list_item outside_body_flow_list_item True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 318.9, 179.65, 6.58] The DTMS-derived layer maintains interface stability. The DTMS-derived layer maintains interface stability. 1 13 12 11 #/texts/12 list_item front_matter_candidate False low outside_body_flow_list_item outside_body_flow_list_item True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 328.99, 170.36, 6.58] DTMS reacts with the HF/F from the electrolyte. DTMS reacts with the HF/F from the electrolyte. 1 14 13 12 #/texts/13 section_header front_matter_heading False low front_matter_heading front_matter_heading True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 363.31, 88.53, 6.4] A R T I C L E I N F O A R T I C L E I N F O 1 20 14 13 #/texts/19 section_header abstract_heading False low abstract_heading abstract_heading True p1:body_region:0 front_matter column_2_of_2 2 2 p1:front_matter:column_2_of_2:white [255, 255, 255] white False False [202.0, 363.31, 67.15, 6.4] A B S T R A C T A B S T R A C T 1 15 15 14 #/texts/14 text front_matter_heading False low front_matter_heading front_matter_heading True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 382.2, 93.07, 40.15] Keywords: Lithium-ion battery Li-rich layered oxide cathode Solid electrolyte interphase film Interfacial stability Keywords: Lithium-ion battery Li-rich layered oxide cathode Solid electrolyte interphase film Interfacial stability 1 16 16 15 #/texts/15 text unknown_text False medium inside_front_matter inside_front_matter True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 425.06, 94.03, 5.85] 1,3-divinyltetramethyldisiloxane 1,3-divinyltetramethyldisiloxane 1 21 17 16 #/texts/20 text front_matter_candidate False low first_page_summary first_page_summary True p1:body_region:1 front_matter column_2_of_2 2 2 p1:front_matter:column_2_of_2:white [255, 255, 255] white False False [202.0, 382.68, 357.8, 73.53] 1,3-Divinyltetramethyldisiloxane (DTMS) is a multifunctional additive that is used to improves the cycling stability and capacity retention of Li-rich Mn-based layered oxide cathodes (LRMs). Cycling performance evaluati… 1,3-Divinyltetramethyldisiloxane (DTMS) is a multifunctional additive that is used to improves the cycling stability and capacity retention of Li-rich Mn-based layered oxide cathodes (LRMs). Cycling performance evaluati… 1 17 18 17 #/texts/16 section_header body_heading False low body_heading body_heading True p1:body_region:0 body_zone column_1_of_2 1 2 p1:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 488.79, 62.58, 7.31] 1. Introduction 1. Introduction 1 18 19 18 #/texts/17 text body True None body body True p1:body_region:0 body_zone column_1_of_2 1 2 p1:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 509.71, 253.44, 132.83] Lithium ion batteries (LIBs) have been used in electric vehicles because of their high energy density, safety, and low price; however, these qualities need to be further enhanced to extend the maximum distance that elec… Lithium ion batteries (LIBs) have been used in electric vehicles because of their high energy density, safety, and low price; however, these qualities need to be further enhanced to extend the maximum distance that elec… 1 19 20 19 #/texts/18 footnote footnote False low first_page_metadata first_page_metadata True p1:body_region:0 body_zone column_1_of_2 1 2 p1:body_zone:column_1_of_2:white [255, 255, 255] white False False [42.63, 672.84, 153.92, 16.16] * Corresponding author. E-mail address: mxwu@fjirsm.ac.cn (M. Wu). * Corresponding author. E-mail address: mxwu@fjirsm.ac.cn (M. Wu). 1 24 21 20 #/texts/23 page_footer page_footer False low first_page_metadata first_page_metadata True p1:body_region:0 body_zone column_1_of_2 1 2 p1:body_zone:column_1_of_2:white [254, 254, 254] white False False [37.59, 699.43, 160.64, 6.58] https://doi.org/10.1016/j.jpowsour.2023.233437 1 25 22 21 #/texts/24 page_footer page_footer False low first_page_metadata first_page_metadata True p1:body_region:0 body_zone column_1_of_2 1 2 p1:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.52, 708.95, 299.92, 17.48] Available online 26 July 2023 Received 28 February 2023; Received in revised form 7 June 2023; Accepted 17 July 2023 Available online 26 July 2023 Received 28 February 2023; Received in revised form 7 June 2023; Accepted 17 July 2023 1 26 23 22 #/texts/25 page_footer page_footer False low first_page_metadata first_page_metadata True p1:body_region:0 bottom_margin column_1_of_2 1 2 p1:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [37.52, 724.32, 167.09, 11.73] 0378-7753/© 2023 Elsevier B.V. All rights reserved. 0378-7753/© 2023 Elsevier B.V. All rights reserved. 1 7 24 23 #/texts/6 text unknown_text False medium empty_after_cleaning empty_after_cleaning True p1:body_region:1 front_matter column_2_of_2 2 2 p1:front_matter:column_2_of_2:white [255, 255, 255] white False False [379.16, 226.86, 6.28, 6.78] * 1 22 25 24 #/texts/21 text body True None body body True p1:body_region:1 body_zone column_2_of_2 2 2 p1:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.59, 488.79, 125.16, 7.31] electrode/electrolyte interface [9]. electrode/electrolyte interface [9]. 1 23 26 25 #/texts/22 text body True None body body True p1:body_region:1 body_zone column_2_of_2 2 2 p1:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.59, 499.22, 253.42, 143.32] To overcome these problems, several approaches have been explored in the past decade, including doping and coating [10 -13]. Recently, a simple and economical strategy has been developed: the formation of a protective i… To overcome these problems, several approaches have been explored in the past decade, including doping and coating [10 -13]. Recently, a simple and economical strategy has been developed: the formation of a protective i… 2 1 1 26 #/texts/26 page_header page_header False low docling_page_header docling_page_header True p2:body_region:1 top_margin column_2_of_2 2 2 p2:top_margin:column_2_of_2:white [255, 255, 255] white False False [433.38, 33.65, 124.91, 10.42] Journal of Power Sources 580 (2023) 233437 Journal of Power Sources 580 (2023) 233437 2 2 2 27 #/texts/27 text page_margin_header False low page_margin_header page_margin_header True p2:body_region:0 top_margin column_1_of_2 1 2 p2:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 37.0, 463.07, 5.85] T. Huang et al. T. Huang et al. 2 3 3 28 #/texts/28 text body True None body body True p2:body_region:0 top_margin column_1_of_2 1 2 p2:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 55.48, 253.45, 289.75] O2/Li cell from 81% to 26% after 200 cycles [16]. Lan et al. reported [17] that the electrode capacity retention in an electrolyte without any additive was 40%, which is much lower than the 72% observed in an electrolyt… O2/Li cell from 81% to 26% after 200 cycles [16]. Lan et al. reported [17] that the electrode capacity retention in an electrolyte without any additive was 40%, which is much lower than the 72% observed in an electrolyt… 2 4 4 29 #/texts/29 text body True None body body True p2:body_region:0 body_zone column_1_of_2 1 2 p2:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 348.41, 253.44, 90.99] Some studies have reported that the improvement of the electrochemical behavior of NCM622-based cells and LNMO-based cells are a result of silicon-based electrolyte additives [26 -28]. In this paper, 1, 3-divinyltetrame… Some studies have reported that the improvement of the electrochemical behavior of NCM622-based cells and LNMO-based cells are a result of silicon-based electrolyte additives [26 -28]. In this paper, 1, 3-divinyltetrame… 2 5 5 30 #/texts/30 section_header body_heading False low body_heading body_heading True p2:body_region:0 body_zone column_1_of_2 1 2 p2:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 453.13, 58.23, 7.31] 2. Experiment 2. Experiment 2 6 6 31 #/texts/31 section_header body_heading False low body_heading body_heading True p2:body_region:0 body_zone column_1_of_2 1 2 p2:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 474.05, 158.65, 7.31] 2.1. Preparation of electrolytes and electrodes 2.1. Preparation of electrolytes and electrodes 2 7 7 32 #/texts/32 text body True None body body True p2:body_region:0 body_zone column_1_of_2 1 2 p2:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 494.97, 253.43, 101.48] The LRM cathode was composed of 80 wt% LRM (LRM300, Ningbo Li-rich Battery Material Technology Co., Ltd., China), 10 wt% polyvinylidene fluoride (PVDF) binder, and 10 wt% acetylene black in N -methyl-2-pyrrolidone. The … The LRM cathode was composed of 80 wt% LRM (LRM300, Ningbo Li-rich Battery Material Technology Co., Ltd., China), 10 wt% polyvinylidene fluoride (PVDF) binder, and 10 wt% acetylene black in N -methyl-2-pyrrolidone. The … 2 8 8 33 #/texts/33 text body True None body body True p2:body_region:0 body_zone column_1_of_2 1 2 p2:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 599.57, 253.44, 38.72] A total of 1000 ppm of hydrofluoric acid (HF) was then added into the BE and BE + 2 vol%DTMS electrolytes to prepare HF-containing electrolytes using a 40 wt% HF aqueous solution [25]. All electrolytes were prepared in … A total of 1000 ppm of hydrofluoric acid (HF) was then added into the BE and BE + 2 vol%DTMS electrolytes to prepare HF-containing electrolytes using a 40 wt% HF aqueous solution [25]. All electrolytes were prepared in … 2 9 9 34 #/texts/34 section_header body_heading False low body_heading body_heading True p2:body_region:0 body_zone column_1_of_2 1 2 p2:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 652.4, 96.4, 7.31] 2.2. Electrochemical testing 2.2. Electrochemical testing 2 10 10 35 #/texts/35 text body True None body body True p2:body_region:0 bottom_margin column_1_of_2 1 2 p2:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 673.32, 253.45, 70.07] The charge -discharge performance of the cells was evaluated using a computer-controlled test system (CT2001A, China). The LRM/Li cells were pre-cycled in the following schedule: 0.1C (1C = 300 mA g 1 ) for three cycles… The charge -discharge performance of the cells was evaluated using a computer-controlled test system (CT2001A, China). The LRM/Li cells were pre-cycled in the following schedule: 0.1C (1C = 300 mA g 1 ) for three cycles… 2 11 11 36 #/texts/36 caption caption False low docling_caption docling_caption True p2:body_region:1 top_margin column_2_of_2 2 2 p2:top_margin:column_2_of_2:white [255, 255, 255] white False False [366.12, 56.3, 79.26, 16.16] Table 1 Calculated Eox (V vs. Li + Table 1 Calculated Eox (V vs. Li + 2 12 12 37 #/texts/37 text body True None body body True p2:body_region:1 front_matter column_2_of_2 2 2 p2:front_matter:column_2_of_2:white [255, 255, 255] white False False [366.12, 65.88, 134.12, 16.16] /Li) of EC, DMC, EMC, and DTMS. /Li) of EC, DMC, EMC, and DTMS. 2 13 13 38 #/texts/38 text body True None body body True p2:body_region:1 front_matter column_2_of_2 2 2 p2:front_matter:column_2_of_2:white [255, 255, 255] white False False [306.59, 153.91, 253.39, 28.23] impedance spectroscopy (EIS) was employed in the frequency range of 10 5 to 0.1 Hz with an amplitude of 5 mV, using a frequency response analyzer (VSP, Bio-logic). impedance spectroscopy (EIS) was employed in the frequency range of 10 5 to 0.1 Hz with an amplitude of 5 mV, using a frequency response analyzer (VSP, Bio-logic). 2 14 14 39 #/texts/39 section_header body_heading False low body_heading body_heading True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 197.1, 104.56, 7.31] 2.3. Physical characterization 2.3. Physical characterization 2 15 15 40 #/texts/40 text body True None body body True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 218.02, 253.4, 80.56] To understand the influence of DTMS on the cycling performance of LRM/Li cells, scanning electron microscopy (SEM; S-4800, Hitachi), transmission electron microscopy (TEM; JEM-2010, JELO), XRD analysis (XRD; Bruker D8 A… To understand the influence of DTMS on the cycling performance of LRM/Li cells, scanning electron microscopy (SEM; S-4800, Hitachi), transmission electron microscopy (TEM; JEM-2010, JELO), XRD analysis (XRD; Bruker D8 A… 2 16 16 41 #/texts/41 section_header body_heading False low body_heading body_heading True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 313.49, 61.58, 7.31] 2.4. Calculations 2.4. Calculations 2 17 17 42 #/texts/42 text body True None body body True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 334.41, 253.4, 38.72] The Gaussian 09 software package was used for theoretical calculations. The equilibrium structures were determined using the B3LYP/6311G(d,p) level [28]. The oxidation potential (Eox) was obtained as follows[28]: The Gaussian 09 software package was used for theoretical calculations. The equilibrium structures were determined using the B3LYP/6311G(d,p) level [28]. The oxidation potential (Eox) was obtained as follows[28]: 2 18 18 43 #/texts/43 text body True None body body True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 380.54, 236.56, 9.34] Eox (Li + /Li) = [G(M + ) - G(M)]/F - 1.4 V Eox (Li + /Li) = [G(M + ) - G(M)]/F - 1.4 V 2 19 19 44 #/texts/44 section_header body_heading False low body_heading body_heading True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 420.93, 100.96, 7.31] 3. Results and discussion 3. Results and discussion 2 20 20 45 #/texts/45 section_header body_heading False low body_heading body_heading True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 441.84, 114.37, 7.31] 3.1. Oxidative stability of DTMS 3.1. Oxidative stability of DTMS 2 21 21 46 #/texts/46 text body True None body body True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 460.54, 253.42, 166.47] The as-calculated oxidation potential and Li + binding affinity (Eb) are often used to forecast the oxidation tendency of an additive on the cathode surface [29,30]. The film-forming electrolyte additives have a lower o… The as-calculated oxidation potential and Li + binding affinity (Eb) are often used to forecast the oxidation tendency of an additive on the cathode surface [29,30]. The film-forming electrolyte additives have a lower o… 2 22 22 47 #/texts/47 section_header body_heading False low body_heading body_heading True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [306.6, 641.91, 167.94, 7.31] 3.2. Impact of DTMS at electrochemical perform 3.2. Impact of DTMS at electrochemical perform 2 23 23 48 #/texts/48#prov0 text back_matter_heading False low early_back_matter_heading early_back_matter_heading True p2:body_region:1 bottom_margin column_2_of_2 2 2 p2:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [306.6, 662.83, 253.42, 80.56] Supplementary Material. 2 shows the charge -discharge curve performance of LRM/Li cells with and without 2 vol% DTMS electrolytes during the first pre-cycle process. It can be found that the cells in the 2 vol% DTMS-con… Supplementary Material. 2 shows the charge -discharge curve performance of LRM/Li cells with and without 2 vol% DTMS electrolytes during the first pre-cycle process. It can be found that the cells in the 2 vol% DTMS-con… 2 24 24 49 #/texts/49 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p2:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [296.21, 754.45, 3.59, 10.42] 2 2 3 2 1 50 #/texts/50 page_header page_header False low docling_page_header docling_page_header True p3:body_region:1 top_margin column_2_of_2 2 2 p3:top_margin:column_2_of_2:white [255, 255, 255] white False False [433.38, 33.65, 124.91, 10.42] Journal of Power Sources 580 (2023) 233437 Journal of Power Sources 580 (2023) 233437 3 1 2 51 #/texts/48#prov1 text page_margin_header False low page_margin_header page_margin_header True p3:body_region:0 top_margin column_1_of_2 1 2 p3:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 36.99, 463.07, 5.85] T. Huang et al. T. Huang et al. 3 3 3 52 #/texts/51 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_2_of_2 2 2 p3:page_body:column_2_of_2:white [255, 255, 255] white False False [179.09, 187.18, 241.32, 8.3] Fig. 1. Optimized structures and Eb values of solvents-Li + and DTMS-Li + . Fig. 1. Optimized structures and Eb values of solvents-Li + and DTMS-Li + . 3 4 4 53 #/texts/52 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p3:page_body:column_1_of_2:white [255, 255, 255] white False False [38.95, 472.99, 521.55, 6.58] Fig. 2. (a) Cycling performance and (b) rate capability of LRM/Li cell. (c) (d) 1st, 20th, 50th, and 100th charge -discharge curves of LRM/Li cell during cycling. Fig. 2. (a) Cycling performance and (b) rate capability of LRM/Li cell. (c) (d) 1st, 20th, 50th, and 100th charge -discharge curves of LRM/Li cell during cycling. 3 5 5 54 #/texts/53 text body_candidate_excluded False high inside_back_matter inside_back_matter True p3:body_region:0 page_body column_1_of_2 1 2 p3:page_body:column_1_of_2:white [255, 255, 255] white False False [37.59, 494.91, 253.44, 174.67] different electrolytes. The LRM/Li cells with 2 vol% DTMS showed great cycling stability. The discharge capacity of LRM/Li cells in the BE electrolyte decreased from 262.3 to 57.7 mAh g 1 after 100 cycles (57.2% capacit… different electrolytes. The LRM/Li cells with 2 vol% DTMS showed great cycling stability. The discharge capacity of LRM/Li cells in the BE electrolyte decreased from 262.3 to 57.7 mAh g 1 after 100 cycles (57.2% capacit… 3 6 6 55 #/texts/54#prov0 text body_candidate_excluded False high inside_back_matter inside_back_matter True p3:body_region:0 bottom_margin column_1_of_2 1 2 p3:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 672.7, 253.44, 70.07] EIS was carried out on LRM/Li cells after pre-cycling and cycling with the BE and 2 vol% DTMS-containing electrolytes, as shown in Fig. 3. The results can be divided into two parts: a depressed semicircle followed by a … EIS was carried out on LRM/Li cells after pre-cycling and cycling with the BE and 2 vol% DTMS-containing electrolytes, as shown in Fig. 3. The results can be divided into two parts: a depressed semicircle followed by a … 3 7 7 56 #/texts/54#prov1 text body_candidate_excluded False high inside_back_matter inside_back_matter True p3:body_region:1 page_body column_2_of_2 2 2 p3:page_body:column_2_of_2:white [255, 255, 255] white False False [306.59, 494.91, 253.4, 38.66] in Rf and Rct compared with the cells with the DTMS-containing electrolyte. The electrolyte decomposition substantially deteriorates the properties of the interface between the LRM and BE electrolyte and thereby reduces… in Rf and Rct compared with the cells with the DTMS-containing electrolyte. The electrolyte decomposition substantially deteriorates the properties of the interface between the LRM and BE electrolyte and thereby reduces… 3 8 8 57 #/texts/55 text body_candidate_excluded False high inside_back_matter inside_back_matter True p3:body_region:1 page_body column_2_of_2 2 2 p3:page_body:column_2_of_2:white [255, 255, 255] white False False [306.59, 536.75, 253.43, 122.34] The surface morphologies of the cathodes in the BE and DTMScontaining electrolytes were analyzed after cycling by SEM and TEM (Fig. 4). As shown in Fig. 4a, the cathode surface in the BE electrolyte was covered with a t… The surface morphologies of the cathodes in the BE and DTMScontaining electrolytes were analyzed after cycling by SEM and TEM (Fig. 4). As shown in Fig. 4a, the cathode surface in the BE electrolyte was covered with a t… 3 9 9 58 #/texts/56 text body_candidate_excluded False high inside_back_matter inside_back_matter True p3:body_region:1 bottom_margin column_2_of_2 2 2 p3:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [306.59, 662.27, 253.42, 80.5] Fig. 5a depicts the obtained XPS of LRM cells with BE and DMSEcontaining electrolytes after cycling. The C 1s peaks at 290.3 and 285.4 eV correspond to PVDF [19,25], and the peak at 284.6 eV is assigned to acetylene bla… Fig. 5a depicts the obtained XPS of LRM cells with BE and DMSEcontaining electrolytes after cycling. The C 1s peaks at 290.3 and 285.4 eV correspond to PVDF [19,25], and the peak at 284.6 eV is assigned to acetylene bla… 3 10 10 59 #/texts/57 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p3:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [296.21, 754.45, 3.59, 10.42] 3 3 4 1 1 60 #/texts/58 page_header page_header False low docling_page_header docling_page_header True p4:body_region:1 top_margin column_2_of_2 2 2 p4:top_margin:column_2_of_2:white [255, 255, 255] white False False [433.38, 33.65, 124.91, 10.42] Journal of Power Sources 580 (2023) 233437 Journal of Power Sources 580 (2023) 233437 4 2 2 61 #/texts/59 text page_margin_header False low page_margin_header page_margin_header True p4:body_region:0 top_margin column_1_of_2 1 2 p4:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 36.99, 463.07, 5.85] T. Huang et al. T. Huang et al. 4 3 3 62 #/texts/60 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p4:page_body:column_1_of_2:white [255, 255, 255] white False False [86.63, 307.39, 426.25, 6.58] Fig. 3. EIS results of LRM/Li cell in BE and 2 vol% DTMS electrolyte after (a) pre-cycling and (b) cycling. (c) Values of Rf and Rct. Fig. 3. EIS results of LRM/Li cell in BE and 2 vol% DTMS electrolyte after (a) pre-cycling and (b) cycling. (c) Values of Rf and Rct. 4 4 4 63 #/texts/61 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p4:page_body:column_1_of_2:white [255, 255, 255] white False False [112.82, 587.51, 373.83, 6.58] Fig. 4. TEM and SEM images of LRM cathodes after cycling (a), (c) with BE and (b), (d) 2 vol% DTMS electrolyte. Fig. 4. TEM and SEM images of LRM cathodes after cycling (a), (c) with BE and (b), (d) 2 vol% DTMS electrolyte. 4 5 5 64 #/texts/62#prov0 text body_candidate_excluded False high inside_back_matter inside_back_matter True p4:body_region:0 bottom_margin column_1_of_2 1 2 p4:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 609.43, 253.44, 132.83] (ROCO2Li, ROLi, and Li2CO3) at 286 and 288.8 eV were observed. The peak intensities for the electrolyte with DTMS were lower than those for the BE electrolyte. The same result can be observed in O 1s spectra. The peak i… (ROCO2Li, ROLi, and Li2CO3) at 286 and 288.8 eV were observed. The peak intensities for the electrolyte with DTMS were lower than those for the BE electrolyte. The same result can be observed in O 1s spectra. The peak i… 4 6 6 65 #/texts/62#prov1 text body_heading False low inside_back_matter inside_back_matter True p4:body_region:1 page_body column_2_of_2 2 2 p4:page_body:column_2_of_2:white [255, 255, 255] white False False [306.59, 609.43, 253.42, 49.15] conclusion, the peak intensities for the electrolyte decomposition products on the cathode in the DTMS-containing electrolyte were weaker, confirming that the electrolyte decomposition could be inhibited by DTMS. The ex… conclusion, the peak intensities for the electrolyte decomposition products on the cathode in the DTMS-containing electrolyte were weaker, confirming that the electrolyte decomposition could be inhibited by DTMS. The ex… 4 7 7 66 #/texts/63#prov0 text body_candidate_excluded False high inside_back_matter inside_back_matter True p4:body_region:1 bottom_margin column_2_of_2 2 2 p4:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [306.59, 661.76, 253.43, 80.5] The XRD results for the cathodes before and after cycling with the BE and 2% DTMS-containing electrolytes are shown in Fig. 5b: the XRD peak intensity of the cathode in the BE electrolyte reduces drastically after cycli… The XRD results for the cathodes before and after cycling with the BE and 2% DTMS-containing electrolytes are shown in Fig. 5b: the XRD peak intensity of the cathode in the BE electrolyte reduces drastically after cycli… 4 8 8 67 #/texts/64 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p4:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [296.21, 754.45, 3.59, 10.42] 4 4 5 2 1 68 #/texts/65 page_header page_header False low docling_page_header docling_page_header True p5:body_region:1 top_margin column_2_of_2 2 2 p5:top_margin:column_2_of_2:white [255, 255, 255] white False False [433.38, 33.65, 124.91, 10.42] Journal of Power Sources 580 (2023) 233437 Journal of Power Sources 580 (2023) 233437 5 1 2 69 #/texts/63#prov1 text page_margin_header False low page_margin_header page_margin_header True p5:body_region:0 top_margin column_1_of_2 1 2 p5:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 36.99, 463.07, 5.85] T. Huang et al. T. Huang et al. 5 3 3 70 #/texts/66 caption caption False low outside_body_flow_caption outside_body_flow_caption False None front_matter column_1_of_2 1 2 p5:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 557.13, 522.17, 16.1] Fig. 5. (a)XPS spectra of LRM cathodes after cycling with BE and 2 vol% DTMS electrolytes. (b) XRD patterns of LRM cathodes and (c) dissolution of transition metal on Li electrode taken from cell after cycling. Fig. 5. (a)XPS spectra of LRM cathodes after cycling with BE and 2 vol% DTMS electrolytes. (b) XRD patterns of LRM cathodes and (c) dissolution of transition metal on Li electrode taken from cell after cycling. 5 4 4 71 #/texts/67 text body_candidate_excluded False high inside_back_matter inside_back_matter True p5:body_region:0 front_matter column_1_of_2 1 2 p5:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 588.57, 253.44, 80.56] cathode was well maintained in DTMS-containing electrolyte. This further confirms that the DTMS is beneficial for maintaining structure stability during cycling. As shown in Fig. 5c, the Mn, Ni, and Co contents were 0.2… cathode was well maintained in DTMS-containing electrolyte. This further confirms that the DTMS is beneficial for maintaining structure stability during cycling. As shown in Fig. 5c, the Mn, Ni, and Co contents were 0.2… 5 5 5 72 #/texts/68 section_header body_heading False low body_heading body_heading True p5:body_region:0 body_zone column_1_of_2 1 2 p5:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 683.75, 124.69, 7.31] 3.3. Interaction of DTMS with HF/F 3.3. Interaction of DTMS with HF/F 5 6 6 73 #/texts/69#prov0 text body True None body body True p5:body_region:0 bottom_margin column_1_of_2 1 2 p5:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 704.67, 253.41, 38.72] To study the interaction of DTMS with HF/F , the cycling performance of the coin cell in the BE + 1000 ppm HF electrolyte and the 2 vol % DTMS-containing + 1000 ppm HF electrolyte was analyzed (Fig. 6a). A significant c… To study the interaction of DTMS with HF/F , the cycling performance of the coin cell in the BE + 1000 ppm HF electrolyte and the 2 vol % DTMS-containing + 1000 ppm HF electrolyte was analyzed (Fig. 6a). A significant c… 5 7 7 74 #/texts/69#prov1 text body True None body body True p5:body_region:1 front_matter column_2_of_2 2 2 p5:front_matter:column_2_of_2:white [255, 255, 255] white False False [306.59, 586.33, 253.42, 93.22] BE + 1000 ppm HF electrolyte: from 246.4 to 60.3 mAh g 1 . However, the discharge capacity in the 2 vol% DTMS-containing + 1000 ppm HF electrolyte changed from 240.3 to 190.6 mAh g 1 . DTMS can effectively suppress the … BE + 1000 ppm HF electrolyte: from 246.4 to 60.3 mAh g 1 . However, the discharge capacity in the 2 vol% DTMS-containing + 1000 ppm HF electrolyte changed from 240.3 to 190.6 mAh g 1 . DTMS can effectively suppress the … 5 8 8 75 #/texts/70#prov0 text body True None body body True p5:body_region:1 bottom_margin column_2_of_2 2 2 p5:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [306.6, 682.73, 253.42, 59.58] NMR spectra are used for analyzing the composition changes after storage for 24 h in the electrolyte upon the addition of HF [32] (Fig. 7). A pair of peaks at 75 ppm can be found for all electrolytes, which are assigned… NMR spectra are used for analyzing the composition changes after storage for 24 h in the electrolyte upon the addition of HF [32] (Fig. 7). A pair of peaks at 75 ppm can be found for all electrolytes, which are assigned… 5 9 9 76 #/texts/71 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p5:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [296.21, 754.45, 3.59, 10.42] 5 5 6 2 1 77 #/texts/72 page_header page_header False low docling_page_header docling_page_header False None top_margin column_2_of_2 2 2 p6:top_margin:column_2_of_2:white [255, 255, 255] white False False [433.38, 33.65, 124.91, 10.42] Journal of Power Sources 580 (2023) 233437 Journal of Power Sources 580 (2023) 233437 6 1 2 78 #/texts/70#prov1 text page_margin_header False low page_margin_header page_margin_header False None top_margin column_1_of_2 1 2 p6:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 36.99, 463.07, 5.85] T. Huang et al. T. Huang et al. 6 3 3 79 #/texts/73 caption caption False low outside_body_flow_caption outside_body_flow_caption False None page_body column_1_of_2 1 2 p6:page_body:column_1_of_2:white [255, 255, 255] white False False [37.59, 243.16, 522.15, 16.16] Fig. 6. (a) Discharge profiles of cell during cycling with BE + 1000 ppm HF and 2 vol% DTMS-containing + 1000 ppm HF; F 1s XPS spectra of LRM cathodes after cycling with (b) BE + 1000 ppm HF and (c) 2 vol% DTMS-containi… Fig. 6. (a) Discharge profiles of cell during cycling with BE + 1000 ppm HF and 2 vol% DTMS-containing + 1000 ppm HF; F 1s XPS spectra of LRM cathodes after cycling with (b) BE + 1000 ppm HF and (c) 2 vol% DTMS-containi… 6 4 4 80 #/texts/74 caption body True None recovered_unbound_docling_caption recovered_unbound_docling_caption False None page_body column_1_of_2 1 2 p6:page_body:column_1_of_2:white [255, 255, 255] white False False [92.13, 673.38, 415.22, 8.36] Fig. 7. 19 F NMR spectra of BE and DTMS-containing electrolytes before (a and b) and after (c and d) 1000 ppm HF was added. Fig. 7. 19 F NMR spectra of BE and DTMS-containing electrolytes before (a and b) and after (c and d) 1000 ppm HF was added. 6 5 5 81 #/texts/75#prov0 text body True None body body False None bottom_margin column_1_of_2 1 2 p6:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 697.02, 253.41, 38.72] assigned to PO2F2 formed from the partial hydrolysis of LiPF6 [25], and the peak at 190 ppm corresponds to HF. However, the HF peak intensity for the 2 vol% DTMS-containing + 1000 ppm HF electrolyte is lower than that f… assigned to PO2F2 formed from the partial hydrolysis of LiPF6 [25], and the peak at 190 ppm corresponds to HF. However, the HF peak intensity for the 2 vol% DTMS-containing + 1000 ppm HF electrolyte is lower than that f… 6 6 6 82 #/texts/75#prov1 text body True None body body False None bottom_margin column_2_of_2 2 2 p6:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [306.59, 697.02, 253.42, 38.72] new small peak at 162 ppm corresponding to the BE + 2 vol%DTMS containing 1000 ppm of the HF electrolyte is shown in Fig. 7d, which can be attributed to the reaction between DTMS and HF/F .Supplementary Material 3 prese… new small peak at 162 ppm corresponding to the BE + 2 vol%DTMS containing 1000 ppm of the HF electrolyte is shown in Fig. 7d, which can be attributed to the reaction between DTMS and HF/F .Supplementary Material 3 prese… 6 7 7 83 #/texts/76 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p6:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [296.21, 754.45, 3.59, 10.42] 6 6 7 2 1 84 #/texts/77 page_header page_header False low docling_page_header docling_page_header False None top_margin column_2_of_2 2 2 p7:top_margin:column_2_of_2:white [255, 255, 255] white False False [433.38, 33.65, 124.91, 10.42] Journal of Power Sources 580 (2023) 233437 Journal of Power Sources 580 (2023) 233437 7 1 2 85 #/texts/75#prov2 text page_margin_header False low page_margin_header page_margin_header True p7:body_region:0 top_margin column_1_of_2 1 2 p7:top_margin:column_1_of_2:white [255, 255, 255] white False False [37.59, 36.99, 463.07, 5.85] T. Huang et al. T. Huang et al. 7 4 3 86 #/texts/79 text body True None body body True p7:body_region:0 front_matter column_1_of_2 1 2 p7:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 189.96, 253.44, 49.15] electrolytes collected from the LRM/Li cells after evaluating their cycling performance. In them, the peak at 162 ppm corresponding to the products of the reaction of DTMS with HF/F disappears. Combined with the Si 2p X… electrolytes collected from the LRM/Li cells after evaluating their cycling performance. In them, the peak at 162 ppm corresponding to the products of the reaction of DTMS with HF/F disappears. Combined with the Si 2p X… 7 6 4 87 #/texts/81 text body True None body body True p7:body_region:0 front_matter column_1_of_2 1 2 p7:front_matter:column_1_of_2:white [255, 255, 255] white False False [37.59, 242.23, 253.43, 28.23] The possible DTMS reaction on the interface of the cathode is shown in Fig. 8. We hypothesize that the Si -O bond can react with HF, Lewis acids, and EC [28,33]. The possible DTMS reaction on the interface of the cathode is shown in Fig. 8. We hypothesize that the Si -O bond can react with HF, Lewis acids, and EC [28,33]. 7 7 5 88 #/texts/82 section_header body_heading False low body_heading body_heading True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 284.81, 60.27, 7.31] 4. Conclusions 4. Conclusions 7 8 6 89 #/texts/83 text body True None body body True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 305.72, 253.42, 80.56] In conclusion, the cycling performance of the LRM cathode can be greatly improved by adding DTMS. The capacity loss decreased from 57.2% to 25% at 0.5C after 100 cycles. Experimental results show that DTMS is preferenti… In conclusion, the cycling performance of the LRM cathode can be greatly improved by adding DTMS. The capacity loss decreased from 57.2% to 25% at 0.5C after 100 cycles. Experimental results show that DTMS is preferenti… 7 9 7 90 #/texts/84 section_header back_matter_heading False low back_matter_heading back_matter_heading stop_trigger True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 400.63, 164.27, 7.31] CRediT authorship contribution statement CRediT authorship contribution statement 7 10 8 91 #/texts/85 text affiliation False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 421.55, 253.42, 38.66] Tao Huang: Investigation, Methodology, Writing -original draft. Xiangzhen Zheng: Investigation. Chunfeng Yan: Validation. Ying Pan: Software. Maoxiang Wu: Conceptualization, Writing -review & editing. Tao Huang: Investigation, Methodology, Writing -original draft. Xiangzhen Zheng: Investigation. Chunfeng Yan: Validation. Ying Pan: Software. Maoxiang Wu: Conceptualization, Writing -review & editing. 7 11 9 92 #/texts/86 section_header back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 476.94, 130.92, 7.31] Declaration of competing interest Declaration of competing interest 7 12 10 93 #/texts/87 text unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [49.55, 497.86, 187.21, 7.31] The authors declare no competing financial interest. The authors declare no competing financial interest. 7 13 11 94 #/texts/88 section_header back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 518.78, 65.84, 7.31] Data availability Data availability 7 14 12 95 #/texts/89 text unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [49.55, 539.7, 142.71, 7.31] Data will be made available on request. Data will be made available on request. 7 15 13 96 #/texts/90 section_header back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 561.35, 72.63, 7.31] Acknowledgement Acknowledgement 7 16 14 97 #/texts/91 text back_matter_text False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 582.27, 253.44, 28.23] This work was supported by the Science and Technology Planning Project of Fujian Province (Grant No. 2022H0038, 2020H0037, 2022T3001). This work was supported by the Science and Technology Planning Project of Fujian Province (Grant No. 2022H0038, 2020H0037, 2022T3001). 7 17 15 98 #/texts/92 section_header unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 624.85, 130.96, 7.31] Appendix A. Supplementary data Appendix A. Supplementary data 7 18 16 99 #/texts/93 text reference False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 645.77, 253.41, 17.74] Supplementary data to this article can be found online at https://doi. org/10.1016/j.jpowsour.2023.233437. Supplementary data to this article can be found online at org/10.1016/j.jpowsour.2023.233437. 7 19 17 100 #/texts/94 section_header back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [37.59, 677.86, 43.55, 7.31] References References 7 20 18 101 #/texts/95 list_item reference False low after_back_matter_stop after_back_matter_stop after_stop True p7:body_region:0 body_zone column_1_of_2 1 2 p7:body_zone:column_1_of_2:white [255, 255, 255] white False False [40.99, 697.3, 240.3, 21.78] M. Hu, X. Pang, Z. Zhou, Recent progress in high-voltage lithium ion batteries, J. Power Sources 68 (1997) 604 -608, https://doi.org/10.1016/j. jpowsour.2013.03.024. M. Hu, X. Pang, Z. Zhou, Recent progress in high-voltage lithium ion batteries, J. 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