page source_page_order layout_page_order layout_order ref label role_guess included_in_body excluded_risk_level body_decision_reason parser_body_decision_reason production_usage visual_asset_type visual_asset_label visual_asset_caption_preview truncation_marker inside_body_region body_region_id zone column column_index column_count region_id background_rgb background_class is_gray_background has_frame_evidence bbox text_preview cleaned_text_preview 1 2 1 0 #/texts/1 page_header page_header False low document_ui document_ui True p1:body_region:1 top_margin column_2_of_2 2 2 p1:top_margin:column_2_of_2:gray [88, 89, 91] gray True True [536.2, 60.48, 21.22, 7.35] Article Article 1 3 2 1 #/texts/2 text metadata False low document_web_address document_web_address True p1:body_region:1 front_matter column_2_of_2 2 2 p1:front_matter:column_2_of_2:white [255, 255, 255] white False False [509.95, 76.75, 54.42, 7.35] pubs.acs.org/cm pubs.acs.org/cm 1 4 3 2 #/texts/3 section_header title_candidate False low first_page_front_matter_heading first_page_front_matter_heading True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [60.49, 121.2, 479.34, 32.86] Feasibility of Using Li2MoO3 in Constructing Li-Rich High Energy Density Cathode Materials Feasibility of Using Li2MoO3 in Constructing Li-Rich High Energy Density Cathode Materials 1 5 4 3 #/texts/4 text affiliation False medium front_matter_author_line front_matter_author_line True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [60.49, 156.08, 504.0, 32.21] Jun Ma, † , ⊥ Yong-Ning Zhou, ‡ , ⊥ Yurui Gao, † Xiqian Yu, ‡ Qingyu Kong, * , § Lin Gu, ∥ Zhaoxiang Wang, * , † Xiao-Qing Yang, * , ‡ and Liquan Chen † Jun Ma, † , ⊥ Yong-Ning Zhou, ‡ , ⊥ Yurui Gao, † Xiqian Yu, ‡ Qingyu Kong, * , § Lin Gu, ∥ Zhaoxiang Wang, * , † Xiao-Qing Yang, * , ‡ and Liquan Chen † 1 6 5 4 #/texts/5 footnote affiliation False medium first_page_author_or_affiliation first_page_author_or_affiliation True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [60.49, 193.44, 503.98, 35.77] † Key Laboratory for Renewable Energy, Chinese Academy of Sciences; Beijing Key Laboratory for New Energy Materials and Devices; Beijing National Laboratory for Condensed Matter Physics; Institute of Physics, Chinese Ac… † Key Laboratory for Renewable Energy, Chinese Academy of Sciences; Beijing Key Laboratory for New Energy Materials and Devices; Beijing National Laboratory for Condensed Matter Physics; Institute of Physics, Chinese Ac… 1 1 6 5 #/texts/0 page_header affiliation False low first_page_author_or_affiliation first_page_author_or_affiliation False None front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [3.61, 214.63, 15.98, 356.87] Downloaded via JILIN UNIV on July 12, 2026 at 04:34:01 (UTC). 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See https:/pubs.acs.org/sharingguidelines for options on how to legitimately share published articles. 1 7 7 6 #/texts/6 footnote affiliation False low first_page_author_or_affiliation first_page_author_or_affiliation True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [60.49, 229.44, 393.16, 13.72] ‡ Department of Chemistry, Brookhaven National Laboratory, Upton, New York 11973, United States ‡ Department of Chemistry, Brookhaven National Laboratory, Upton, New York 11973, United States 1 8 8 7 #/texts/7 footnote affiliation False low first_page_author_or_affiliation first_page_author_or_affiliation True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [60.49, 243.86, 464.42, 13.3] § X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, United States § X-ray Science Division, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439, United States 1 9 9 8 #/texts/8 footnote affiliation False medium first_page_author_or_affiliation first_page_author_or_affiliation True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [60.49, 257.79, 503.96, 24.37] ∥ Laboratory for Advanced Materials & Electron Microscopy, Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, PO Box 603, Beijing 100190, China ∥ Laboratory for Advanced Materials & Electron Microscopy, Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, PO Box 603, Beijing 100190, China 1 10 10 9 #/texts/9 section_header title_candidate False low first_page_front_matter_heading first_page_front_matter_heading True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:column_1_of_2:white [255, 255, 255] white False False [69.45, 289.17, 101.14, 12.62] * S Supporting Information * S Supporting Information 1 11 11 10 #/texts/10 text abstract_candidate False medium implicit_abstract implicit_abstract True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:front_panel:colored [255, 247, 213] colored False False [69.45, 315.0, 249.52, 111.16] ABSTRACT: Layer-structured x Li2MnO3 · (1 -x )Li M O2 are promising cathode materials for high energy-density Li-ion batteries because they deliver high capacities due to the stabilizing e ff ect of Li2MnO3. However, th… ABSTRACT: Layer-structured x Li2MnO3 · (1 -x )Li M O2 are promising cathode materials for high energy-density Li-ion batteries because they deliver high capacities due to the stabilizing e ff ect of Li2MnO3. However, th… 1 12 12 11 #/texts/11 text abstract_candidate False medium first_page_summary first_page_summary True p1:body_region:0 front_matter column_1_of_2 1 2 p1:front_matter:front_panel:colored [255, 247, 213] colored False False [69.45, 426.58, 486.03, 55.79] ning transmission electron microscopy clarify its lithium extraction/insertion mechanism and shows that the Mo 4+ /Mo 6+ redox couple in Li 2 MoO3 can accomplish the task of charge compensation upon Li removal. Other pr… ning transmission electron microscopy clarify its lithium extraction/insertion mechanism and shows that the Mo 4+ /Mo 6+ redox couple in Li 2 MoO3 can accomplish the task of charge compensation upon Li removal. Other pr… 1 13 13 12 #/texts/12 section_header body_heading False low body_heading body_heading True p1:body_region:0 body_zone column_1_of_2 1 2 p1:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 496.13, 87.35, 23.65] ■ INTRODUCTION ■ INTRODUCTION 1 14 14 13 #/texts/13#prov0 text body True None body body True p1:body_region:0 bottom_margin column_1_of_2 1 2 p1:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [60.49, 523.43, 240.0, 233.93] Li-ion batteries (LIBs) have been powering most of the portable electronics for decades and are driving various types of electric vehicles nowadays. Safety, energy density, and cycle life are the essential criteria to e… Li-ion batteries (LIBs) have been powering most of the portable electronics for decades and are driving various types of electric vehicles nowadays. Safety, energy density, and cycle life are the essential criteria to e… 1 23 15 14 #/texts/21 page_footer page_footer False low first_page_metadata first_page_metadata True p1:body_region:0 bottom_margin column_1_of_2 1 2 p1:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [168.49, 771.24, 95.03, 5.88] © 2014 American Chemical Society © 2014 American Chemical Society 1 15 16 15 #/texts/13#prov1 text body True None body body True p1:body_region:1 body_zone column_2_of_2 2 2 p1:body_zone:column_2_of_2:white [255, 255, 255] white False False [324.45, 502.82, 240.04, 115.98] surface modi fi cation, 14,15 atomic substitution, 16 -18 and optimization of synthesis strategies 19,20 have been pursued to improve the performances of the composites, complete elimination of their drawbacks related t… surface modi fi cation, 14,15 atomic substitution, 16 -18 and optimization of synthesis strategies 19,20 have been pursued to improve the performances of the composites, complete elimination of their drawbacks related t… 1 16 17 16 #/texts/14 text body True None body body True p1:body_region:1 body_zone column_2_of_2 2 2 p1:body_zone:column_2_of_2:white [255, 255, 255] white False False [324.45, 621.22, 240.01, 88.63] Here, we propose to replace Li2MnO3 with Li2MoO3 with disordered NaFeO2 structure ( R 3 ̅ m ; a = 2.884 Å, c = 14.834 Å) 21 -24 to construct novel Li-rich x Li2MoO3 · (1 -x )Li M O2 cathodes and evaluate its feasibility… Here, we propose to replace Li2MnO3 with Li2MoO3 with disordered NaFeO2 structure ( R 3 ̅ m ; a = 2.884 Å, c = 14.834 Å) 21 -24 to construct novel Li-rich x Li2MoO3 · (1 -x )Li M O2 cathodes and evaluate its feasibility… 1 18 18 17 #/texts/16 text metadata False low first_page_metadata first_page_metadata True p1:body_region:1 body_zone column_2_of_2 2 2 p1:body_zone:column_2_of_2:white [255, 255, 255] white False False [367.99, 727.13, 55.06, 7.92] March 22, 2014 March 22, 2014 1 17 19 18 #/texts/15 text metadata False low first_page_metadata first_page_metadata True p1:body_region:1 body_zone column_2_of_2 2 2 p1:body_zone:column_2_of_2:white [253, 253, 253] white False False [324.45, 727.21, 34.65, 7.77] Received: Received: 1 20 20 19 #/texts/18 text metadata False low first_page_metadata first_page_metadata True p1:body_region:1 body_zone column_2_of_2 2 2 p1:body_zone:column_2_of_2:white [255, 255, 255] white False False [367.99, 738.19, 49.9, 7.92] April 30, 2014 April 30, 2014 1 19 21 20 #/texts/17 text metadata False low first_page_metadata first_page_metadata True p1:body_region:1 body_zone column_2_of_2 2 2 p1:body_zone:column_2_of_2:white [253, 253, 253] white False False [324.45, 738.27, 30.25, 7.77] Revised: Revised: 1 22 22 21 #/texts/20 text metadata False low first_page_metadata first_page_metadata True p1:body_region:1 bottom_margin column_2_of_2 2 2 p1:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [367.99, 749.19, 43.83, 7.92] May 1, 2014 May 1, 2014 1 21 23 22 #/texts/19 text metadata False low first_page_metadata first_page_metadata True p1:body_region:1 bottom_margin column_2_of_2 2 2 p1:bottom_margin:column_2_of_2:white [252, 252, 252] white False False [324.45, 749.27, 37.75, 7.77] Published: Published: 1 25 24 23 #/texts/23 page_footer page_footer False low first_page_metadata first_page_metadata True p1:body_region:1 bottom_margin column_2_of_2 2 2 p1:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [396.06, 769.98, 168.43, 7.74] dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 1 24 25 24 #/texts/22 page_footer page_footer False low docling_page_footer docling_page_footer True p1:body_region:0 bottom_margin column_2_of_2 2 2 p1:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [304.5, 770.73, 15.93, 6.54] 3256 3256 2 1 1 25 #/texts/24 page_header page_header False low docling_page_header docling_page_header True p2:body_region:0 top_margin column_1_of_2 1 2 p2:top_margin:column_1_of_2:gray [241, 242, 242] gray True False [60.49, 48.93, 98.47, 8.72] Chemistry of Materials Chemistry of Materials 2 3 2 26 #/texts/26 text body True None body body True p2:body_region:0 front_matter column_1_of_2 1 2 p2:front_matter:column_1_of_2:white [255, 255, 255] white False False [60.49, 69.37, 240.01, 372.97] in Li2MoO3 can exchange multiple electrons and supply a theoretical capacity up to 339 mAh g -1 . (2) Our fi rst-principles calculations indicate that Mo doping delays the oxygen release (i.e., oxygen evolution occurs o… in Li2MoO3 can exchange multiple electrons and supply a theoretical capacity up to 339 mAh g -1 . (2) Our fi rst-principles calculations indicate that Mo doping delays the oxygen release (i.e., oxygen evolution occurs o… 2 4 3 27 #/texts/27 section_header body_heading False low body_heading body_heading True p2:body_region:0 body_zone column_1_of_2 1 2 p2:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 442.33, 139.52, 23.65] ■ RESULTS AND DISCUSSION ■ RESULTS AND DISCUSSION 2 5 4 28 #/texts/28 text body True None body body True p2:body_region:0 body_zone column_1_of_2 1 2 p2:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 467.95, 239.99, 152.21] Structure of As-Prepared Li2MoO3. The re fi ned XRD pattern of the as-prepared Li2MoO3 powder matches well with the α -NaFeO2 structure R 3 ̅ m with lattice constants a = 2.8675(9) Å and c = 14.8357(6) Å (Figure 1a and … Structure of As-Prepared Li2MoO3. The re fi ned XRD pattern of the as-prepared Li2MoO3 powder matches well with the α -NaFeO2 structure R 3 ̅ m with lattice constants a = 2.8675(9) Å and c = 14.8357(6) Å (Figure 1a and … 2 6 5 29 #/texts/29#prov0 text body True None body body True p2:body_region:0 bottom_margin column_1_of_2 1 2 p2:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [60.49, 622.36, 240.0, 140.84] It is worthwhile to point out that the contrast of the highangle annular-dark- fi eld (HAADF) image exhibits a Z 1.7 dependence as compared with Z 1/3 for the annular-brightfi eld (ABF) image with respect to the atomic … It is worthwhile to point out that the contrast of the highangle annular-dark- fi eld (HAADF) image exhibits a Z 1.7 dependence as compared with Z 1/3 for the annular-brightfi eld (ABF) image with respect to the atomic … 2 2 6 30 #/texts/25 page_header page_header False low docling_page_header docling_page_header True p2:body_region:1 top_margin column_2_of_2 2 2 p2:top_margin:column_2_of_2:gray [88, 89, 91] gray True True [536.2, 49.99, 21.22, 7.35] Article Article 2 8 7 31 #/texts/30 caption caption False low outside_body_flow_caption outside_body_flow_caption True p2:body_region:1 front_matter column_2_of_2 2 2 p2:front_matter:column_2_of_2:white [255, 255, 255] white False False [324.45, 364.64, 240.03, 107.93] Figure 1. Structure of as-prepared Li 2 MoO3. (a) Schematic lattice of Li2MoO3. (b) The re fi ned XRD pattern of Li2MoO3 ( λ = 0.7747 Å) using GSAS program. (c) ABF STEM image of Li2MoO3 along the [100] zone axis with M… Figure 1. Structure of as-prepared Li 2 MoO3. (a) Schematic lattice of Li2MoO3. (b) The re fi ned XRD pattern of Li2MoO3 ( λ = 0.7747 Å) using GSAS program. (c) ABF STEM image of Li2MoO3 along the [100] zone axis with M… 2 7 8 32 #/texts/29#prov1 text body True None body body True p2:body_region:1 body_zone column_2_of_2 2 2 p2:body_zone:column_2_of_2:white [255, 255, 255] white False False [324.45, 488.15, 240.02, 100.18] columns show an αβγ -stacking with an irregular shift along the [010] direction (slipped O3 type; Supporting Information Figure S3), due to the presence of disordered Mo3O13 clusters in the Li -Mo layers (Supporting Inf… columns show an αβγ -stacking with an irregular shift along the [010] direction (slipped O3 type; Supporting Information Figure S3), due to the presence of disordered Mo3O13 clusters in the Li -Mo layers (Supporting Inf… 2 9 9 33 #/texts/31 text body True None body body True p2:body_region:1 bottom_margin column_2_of_2 2 2 p2:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [324.45, 588.93, 240.03, 174.27] Structural Transition and Mo-Ion Migration. Irreversible migration of the Mn ions into the transition metal layer to fi ll out the Li vacancies (a proposed layer-to-spinel transition) has been reported to be one of the … Structural Transition and Mo-Ion Migration. Irreversible migration of the Mn ions into the transition metal layer to fi ll out the Li vacancies (a proposed layer-to-spinel transition) has been reported to be one of the … 2 11 10 34 #/texts/33 page_footer page_footer False low docling_page_footer docling_page_footer True p2:body_region:1 bottom_margin column_2_of_2 2 2 p2:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [396.06, 773.27, 168.43, 7.74] dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 2 10 11 35 #/texts/32 page_footer page_footer False low docling_page_footer docling_page_footer False None bottom_margin column_2_of_2 2 2 p2:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [304.5, 774.02, 15.93, 6.54] 3257 3257 3 1 1 36 #/texts/34 page_header page_header False low docling_page_header docling_page_header True p3:body_region:0 top_margin column_1_of_2 1 2 p3:top_margin:column_1_of_2:gray [241, 242, 242] gray True False [60.49, 48.93, 98.47, 8.72] Chemistry of Materials Chemistry of Materials 3 3 2 37 #/texts/36 text body True None body body True p3:body_region:0 page_body column_1_of_2 1 2 p3:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 69.37, 240.0, 30.8] In order to investigate the structural changes of Li2MoO3 during electrochemical (de)lithiation between 2.0 and 4.8 V, in situ XRD characterization was performed (Figure 2a and In order to investigate the structural changes of Li2MoO3 during electrochemical (de)lithiation between 2.0 and 4.8 V, in situ XRD characterization was performed (Figure 2a and 3 4 3 38 #/texts/37 caption caption False low outside_body_flow_caption outside_body_flow_caption True p3:body_region:0 page_body column_1_of_2 1 2 p3:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 381.99, 240.01, 57.93] Figure 2. Structural evolution of Li2MoO3 during the initial delithiation and lithiation. (a) In situ XRD patterns of Li2 -x MoO3 (0 ≤ x ≤ 2) electrodes while a Li 2 MoO3/Li cell is charged and discharged at a current d… Figure 2. Structural evolution of Li2MoO3 during the initial delithiation and lithiation. (a) In situ XRD patterns of Li2 -x MoO3 (0 ≤ x ≤ 2) electrodes while a Li 2 MoO3/Li cell is charged and discharged at a current d… 3 5 4 39 #/texts/38 text back_matter_heading False low back_matter_heading back_matter_heading stop_trigger True p3:body_region:0 page_body column_1_of_2 1 2 p3:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 457.38, 239.95, 41.8] Supporting Information Figure S9). Before the cell is charged to ca. 3.1 V, a solid-solution reaction occurs with negligible variation of cell parameters (Li2MoO3 → Li1.75MoO3 + 0.25Li + ). Supporting Information Figure S9). Before the cell is charged to ca. 3.1 V, a solid-solution reaction occurs with negligible variation of cell parameters (Li2MoO3 → Li1.75MoO3 + 0.25Li + ). 3 6 5 40 #/texts/39 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:0 page_body column_1_of_2 1 2 p3:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 501.37, 240.04, 206.83] As the cell is further charged to ca. 3.6 V, the (003) di ff raction peak shifts to lower angles and gradually becomes broader. Meanwhile, the intensities of the other peaks indexed to Li2MoO3 decrease while those of ne… As the cell is further charged to ca. 3.6 V, the (003) di ff raction peak shifts to lower angles and gradually becomes broader. Meanwhile, the intensities of the other peaks indexed to Li2MoO3 decrease while those of ne… 3 7 6 41 #/texts/40#prov0 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:0 bottom_margin column_1_of_2 1 2 p3:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [60.49, 710.4, 239.96, 53.96] In the subsequent Li-ion insertion process, these di ff raction peaks keep unchanged at fi rst (Li0.53MoO3 + 0.44Li + → Li 0.97 MoO3) and then continuously shift to higher di ff raction angles very close to that of Li2M… In the subsequent Li-ion insertion process, these di ff raction peaks keep unchanged at fi rst (Li0.53MoO3 + 0.44Li + → Li 0.97 MoO3) and then continuously shift to higher di ff raction angles very close to that of Li2M… 3 2 7 42 #/texts/35 page_header page_header False low after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:1 top_margin column_2_of_2 2 2 p3:top_margin:column_2_of_2:gray [88, 89, 91] gray True True [536.2, 49.99, 21.22, 7.35] Article Article 3 8 8 43 #/texts/40#prov1 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:1 page_body column_2_of_2 2 2 p3:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 69.37, 240.02, 63.8] with Li-ion insertion. Interestingly, the insertion of Li ions to Li0.53MoO3 and Li0.97MoO3 seems to be a solid-solution reaction, di ff erent from that in the charge process. These indicate that the structure of Li2MoO… with Li-ion insertion. Interestingly, the insertion of Li ions to Li0.53MoO3 and Li0.97MoO3 seems to be a solid-solution reaction, di ff erent from that in the charge process. These indicate that the structure of Li2MoO… 3 9 9 44 #/texts/41 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:1 page_body column_2_of_2 2 2 p3:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 135.36, 240.0, 41.8] STEM HAADF images of Li2MoO3 at di ff erent states in the fi rst charge and discharge processes were recorded to check the Mo-ion migration and the resultant structural transition during Li-ion insertion/extraction at t… STEM HAADF images of Li2MoO3 at di ff erent states in the fi rst charge and discharge processes were recorded to check the Mo-ion migration and the resultant structural transition during Li-ion insertion/extraction at t… 3 10 10 45 #/texts/42 caption caption False low after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:1 page_body column_2_of_2 2 2 p3:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 452.29, 240.02, 87.92] Figure 3. Detection of Mo-ion migration in atomic scale. (a) HAADF image of the as-prepared Li 2 MoO3 along the [100] zone axis. (c and e) HAADF images of the charged and discharged Li2MoO3 along the [1 ̅ 00] zone axis,… Figure 3. Detection of Mo-ion migration in atomic scale. (a) HAADF image of the as-prepared Li 2 MoO3 along the [100] zone axis. (c and e) HAADF images of the charged and discharged Li2MoO3 along the [1 ̅ 00] zone axis,… 3 11 11 46 #/texts/43 text back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:1 page_body column_2_of_2 2 2 p3:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 553.0, 240.01, 133.16] Supporting Information Figure S12 -S15). After Li-ion extraction, the Mo ions migrate from 3b to 3a sites, implying the disaggregation of the Mo3O13 clusters. As a result, the atoms in the 3b and 3a sites have similar c… Supporting Information Figure S12 -S15). After Li-ion extraction, the Mo ions migrate from 3b to 3a sites, implying the disaggregation of the Mo3O13 clusters. As a result, the atoms in the 3b and 3a sites have similar c… 3 12 12 47 #/texts/44 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:1 bottom_margin column_2_of_2 2 2 p3:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [324.45, 688.4, 239.99, 75.96] Phase transformation from faulted O1 type to O3 type seems to be the way that requires the lowest energy to bear the stress induced by the Li-ion insertion. The Mo -Mo distances parallel and vertical to the c axis are s… Phase transformation from faulted O1 type to O3 type seems to be the way that requires the lowest energy to bear the stress induced by the Li-ion insertion. The Mo -Mo distances parallel and vertical to the c axis are s… 3 14 13 48 #/texts/46 page_footer page_footer False low after_back_matter_stop after_back_matter_stop after_stop True p3:body_region:1 bottom_margin column_2_of_2 2 2 p3:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [396.06, 773.27, 168.43, 7.74] dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 3 13 14 49 #/texts/45 page_footer page_footer False low after_back_matter_stop after_back_matter_stop after_stop False None bottom_margin column_2_of_2 2 2 p3:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [304.5, 774.02, 15.93, 6.54] 3258 3258 4 1 1 50 #/texts/47 page_header page_header False low after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:0 top_margin column_1_of_2 1 2 p4:top_margin:column_1_of_2:gray [241, 242, 242] gray True False [60.49, 48.93, 98.47, 8.72] Chemistry of Materials Chemistry of Materials 4 3 2 51 #/texts/49 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:0 page_body column_1_of_2 1 2 p4:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 69.37, 239.97, 87.01] The di ff erence between surface and bulk might be originated from the inhomogeneous insertion of the Li ions. Therefore, the partially reversible migration of the Mo ions and the partial recovery of the Mo3O13 clusters… The di ff erence between surface and bulk might be originated from the inhomogeneous insertion of the Li ions. Therefore, the partially reversible migration of the Mo ions and the partial recovery of the Mo3O13 clusters… 4 4 3 52 #/texts/50 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:0 page_body column_1_of_2 1 2 p4:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 156.93, 239.99, 108.28] Extra Electron Donor and Charge Compensation. Oxygen release occurs in the fi rst (few) cycle(s) of x Li2MnO3 · (1 -x )Li M O2 because the Mn 4+ ions in Li2MnO3 cannot be further oxidized. O 2 -ions are the single elect… Extra Electron Donor and Charge Compensation. Oxygen release occurs in the fi rst (few) cycle(s) of x Li2MnO3 · (1 -x )Li M O2 because the Mn 4+ ions in Li2MnO3 cannot be further oxidized. O 2 -ions are the single elect… 4 5 4 53 #/texts/51 caption caption False low after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:0 page_body column_1_of_2 1 2 p4:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 571.0, 239.97, 88.99] Figure 4. Charge compensation of Li2MoO3 during the initial delithiation and lithiation. (a) XANES spectra of Mo K-edge of Li2MoO3 at di ff erent delithiation and lithiation states. (b) Fouriertransformed Mo K-edge EXAF… Figure 4. Charge compensation of Li2MoO3 during the initial delithiation and lithiation. (a) XANES spectra of Mo K-edge of Li2MoO3 at di ff erent delithiation and lithiation states. (b) Fouriertransformed Mo K-edge EXAF… 4 6 5 54 #/texts/52#prov0 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:0 bottom_margin column_1_of_2 1 2 p4:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [60.49, 677.35, 239.99, 87.01] spectra (XANES) of Mo K-edge at various states. The absorption edges shift to higher energy during charge. Using the reference spectra of MoO2 and MoO3 (Supporting Information Figure S16), the valence state of Mo is est… spectra (XANES) of Mo K-edge at various states. The absorption edges shift to higher energy during charge. Using the reference spectra of MoO2 and MoO3 (Supporting Information Figure S16), the valence state of Mo is est… 4 2 6 55 #/texts/48 page_header page_header False low after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:1 top_margin column_2_of_2 2 2 p4:top_margin:column_2_of_2:gray [88, 89, 91] gray True True [536.2, 49.99, 21.22, 7.35] Article Article 4 7 7 56 #/texts/52#prov1 text unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:1 page_body column_2_of_2 2 2 p4:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 69.37, 239.96, 30.92] the MoO6 octahedrons in the Mo3O13 clusters and other parts of the as-prepared Li2MoO3 become more and more distorted with increasing Li removal. the MoO6 octahedrons in the Mo3O13 clusters and other parts of the as-prepared Li2MoO3 become more and more distorted with increasing Li removal. 4 8 8 57 #/texts/53 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:1 page_body column_2_of_2 2 2 p4:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 102.48, 240.04, 163.52] In the discharge process, however, the absorption edges shift back to lower energy but do not return to their original positions, suggesting that the Mo ions are reduced during Liion insertion, but their average valence… In the discharge process, however, the absorption edges shift back to lower energy but do not return to their original positions, suggesting that the Mo ions are reduced during Liion insertion, but their average valence… 4 9 9 58 #/texts/54 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:1 page_body column_2_of_2 2 2 p4:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 268.2, 240.02, 119.36] Two dominant peaks can be observed in the Mo K-edge FTEXAFS spectrum of the as-prepared Li2MoO3 (Figure 4b). The peak at R ∼ 1.6 Å belongs to the Mo -O bond in the nearest MoO6 octahedra while the peak at R ∼ 2.3 Å is a… Two dominant peaks can be observed in the Mo K-edge FTEXAFS spectrum of the as-prepared Li2MoO3 (Figure 4b). The peak at R ∼ 1.6 Å belongs to the Mo -O bond in the nearest MoO6 octahedra while the peak at R ∼ 2.3 Å is a… 4 11 10 59 #/texts/56 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:1 page_body column_2_of_2 2 2 p4:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 386.38, 240.04, 166.89] The length of the Mo -O bond increases slightly but that of the Mo -Mo bond does not change at all when the material is charged to 3.6 V. When it is charged to 4.8 V, the Mo -O peak splits into two at around 1.3 and 1.7… The length of the Mo -O bond increases slightly but that of the Mo -Mo bond does not change at all when the material is charged to 3.6 V. When it is charged to 4.8 V, the Mo -O peak splits into two at around 1.3 and 1.7… 4 10 11 60 #/texts/55 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:1 bottom_margin column_2_of_2 2 2 p4:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [324.45, 552.09, 240.04, 211.05] After discharged to 2.5 V, the two Mo -O peaks of the charged sample move toward each other. Meanwhile, the intensity of the Mo(3b)-Mo(3b) peak increases, implying that the severely distorted MoO6 octahedra are changed … After discharged to 2.5 V, the two Mo -O peaks of the charged sample move toward each other. Meanwhile, the intensity of the Mo(3b)-Mo(3b) peak increases, implying that the severely distorted MoO6 octahedra are changed … 4 13 12 61 #/texts/58 page_footer page_footer False low after_back_matter_stop after_back_matter_stop after_stop True p4:body_region:1 bottom_margin column_2_of_2 2 2 p4:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [396.06, 773.27, 168.43, 7.74] dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 4 12 13 62 #/texts/57 page_footer page_footer False low after_back_matter_stop after_back_matter_stop after_stop False None bottom_margin column_2_of_2 2 2 p4:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [304.5, 774.02, 15.93, 6.54] 3259 3259 5 1 1 63 #/texts/59 page_header page_header False low after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:0 top_margin column_1_of_2 1 2 p5:top_margin:column_1_of_2:gray [241, 242, 242] gray True False [60.49, 48.93, 98.47, 8.72] Chemistry of Materials Chemistry of Materials 5 3 2 64 #/texts/61 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:0 page_body column_1_of_2 1 2 p5:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 69.37, 240.01, 307.12] The oxygen species play an important role in the safety and structural stability of the Li-rich layered materials. 2,12,13 Irreversible oxygen evolution in the fi rst (few) cycle(s) results in safety hazard and structur… The oxygen species play an important role in the safety and structural stability of the Li-rich layered materials. 2,12,13 Irreversible oxygen evolution in the fi rst (few) cycle(s) results in safety hazard and structur… 5 4 3 65 #/texts/62 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:0 page_body column_1_of_2 1 2 p5:page_body:column_1_of_2:white [255, 255, 255] white False False [60.49, 378.75, 240.0, 163.46] In the lithiation process, the intensity of the 535.6 eV peak decreases slightly, indicating that the charge compensation from oxygen is partially reversible. In contrast, the XAS spectra in the FY mode, which mainly gi… In the lithiation process, the intensity of the 535.6 eV peak decreases slightly, indicating that the charge compensation from oxygen is partially reversible. In contrast, the XAS spectra in the FY mode, which mainly gi… 5 5 4 66 #/texts/63#prov0 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:0 bottom_margin column_1_of_2 1 2 p5:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [60.49, 544.03, 240.01, 219.17] (De)lithiation Mechanism. Based on the above comprehensive XRD, STEM, and XAS studies of Li2MoO3 at various charge/discharge states, a possible phase transition diagram of Li 2 -x MoO3 (0 ≤ x ≤ 1.47) can be drawn (Figur… (De)lithiation Mechanism. Based on the above comprehensive XRD, STEM, and XAS studies of Li2MoO3 at various charge/discharge states, a possible phase transition diagram of Li 2 -x MoO3 (0 ≤ x ≤ 1.47) can be drawn (Figur… 5 2 5 67 #/texts/60 page_header page_header False low after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:1 top_margin column_2_of_2 2 2 p5:top_margin:column_2_of_2:gray [88, 89, 91] gray True True [536.2, 49.99, 21.22, 7.35] Article Article 5 7 6 68 #/texts/64 caption caption False low after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:1 page_body column_2_of_2 2 2 p5:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 246.09, 240.04, 37.92] Figure 5. Structural transition of Li2MoO3 in the initial electrochemical (de)lithiation process. The lattice structure variation demonstrates that solid-solution reaction and two-phase reaction occur in consequence. Figure 5. Structural transition of Li2MoO3 in the initial electrochemical (de)lithiation process. The lattice structure variation demonstrates that solid-solution reaction and two-phase reaction occur in consequence. 5 6 7 69 #/texts/63#prov1 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:1 page_body column_2_of_2 2 2 p5:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 299.98, 240.02, 111.22] solution reaction of Li 2 -x MoO3 (1.25 ≤ x ≤ 1.47) with increasing Li vacancies, the MoO6 octahedron distortion and Mo-ion interlayer migration. In the discharge process (Regions IV and V), solid-solution reaction of L… solution reaction of Li 2 -x MoO3 (1.25 ≤ x ≤ 1.47) with increasing Li vacancies, the MoO6 octahedron distortion and Mo-ion interlayer migration. In the discharge process (Regions IV and V), solid-solution reaction of L… 5 8 8 70 #/texts/65 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:1 page_body column_2_of_2 2 2 p5:page_body:column_2_of_2:white [255, 255, 255] white False False [324.45, 413.39, 240.02, 151.78] Although further experimental and theoretical studies are required to fi nd out more details of the phase transitions during the initial and the subsequent cycles, such as the paths of the Liion di ff usion and the Mo-i… Although further experimental and theoretical studies are required to fi nd out more details of the phase transitions during the initial and the subsequent cycles, such as the paths of the Liion di ff usion and the Mo-i… 5 9 9 71 #/texts/66 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:1 bottom_margin column_2_of_2 2 2 p5:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [324.45, 567.36, 240.02, 197.0] It is the irreversible oxygen release and the transition metal migration in highly delithiated Li2MnO3 that lead to its irreversible structural transition and capacity loss. Di ff erent from that, introduction of the Mo… It is the irreversible oxygen release and the transition metal migration in highly delithiated Li2MnO3 that lead to its irreversible structural transition and capacity loss. Di ff erent from that, introduction of the Mo… 5 11 10 72 #/texts/68 page_footer page_footer False low after_back_matter_stop after_back_matter_stop after_stop True p5:body_region:1 bottom_margin column_2_of_2 2 2 p5:bottom_margin:column_2_of_2:white [255, 255, 255] white False False [396.06, 773.27, 168.43, 7.74] dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 dx.doi.org/10.1021/cm501025r | Chem. Mater. 2014, 26, 3256 -3262 5 10 11 73 #/texts/67 page_footer page_footer False low after_back_matter_stop after_back_matter_stop after_stop False None bottom_margin column_2_of_2 2 2 p5:bottom_margin:column_2_of_2:white [254, 254, 254] white False False [304.5, 774.02, 15.93, 6.54] 3260 3260 6 1 1 74 #/texts/69 page_header page_header False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 top_margin column_1_of_2 1 2 p6:top_margin:column_1_of_2:gray [241, 242, 242] gray True False [60.49, 48.93, 98.47, 8.72] Chemistry of Materials Chemistry of Materials 6 3 2 75 #/texts/71 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 front_matter column_1_of_2 1 2 p6:front_matter:column_1_of_2:white [255, 255, 255] white False False [60.49, 69.37, 239.98, 53.7] and Li2MoO3-based cathode materials do not need to be charged to such high (4.8 V) potentials. In that case, the reversibility of the Mo-ion migration and O 2 --ion oxidation, structural stability and the compatibility … and Li2MoO3-based cathode materials do not need to be charged to such high (4.8 V) potentials. In that case, the reversibility of the Mo-ion migration and O 2 --ion oxidation, structural stability and the compatibility … 6 4 3 76 #/texts/72 section_header body_heading False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 127.63, 77.3, 23.65] ■ CONCLUSION ■ CONCLUSION 6 5 4 77 #/texts/73 text body_candidate_excluded False medium after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 154.87, 240.0, 345.62] In summary, comprehensive in situ XRD and ex situ STEM and XAS studies clarify the electrochemical (de)lithiation mechanism of Li2MoO3 and prove the feasibility of replacing Li 2 MnO3 with its iso-structured Li2MoO3 to … In summary, comprehensive in situ XRD and ex situ STEM and XAS studies clarify the electrochemical (de)lithiation mechanism of Li2MoO3 and prove the feasibility of replacing Li 2 MnO3 with its iso-structured Li2MoO3 to … 6 6 5 78 #/texts/74 section_header unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 504.98, 121.71, 23.65] ■ ASSOCIATED CONTENT ■ ASSOCIATED CONTENT 6 7 6 79 #/texts/75 section_header unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 530.62, 113.35, 12.62] * S Supporting Information * S Supporting Information 6 8 7 80 #/texts/76 text body_heading False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 545.48, 239.99, 87.38] Experimental section, re fi ned structural parameters, SEM images of the as-prepared Li2MoO3, its electrochemical performance, the original STEM images and the corresponding charge/discharge potential pro fi les of Li2M… Experimental section, re fi ned structural parameters, SEM images of the as-prepared Li2MoO3, its electrochemical performance, the original STEM images and the corresponding charge/discharge potential pro fi les of Li2M… 6 9 8 81 #/texts/77 section_header unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 637.35, 125.07, 23.65] ■ AUTHOR INFORMATION ■ AUTHOR INFORMATION 6 10 9 82 #/texts/78 section_header metadata False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 665.18, 97.03, 8.29] Corresponding Authors Corresponding Authors 6 11 10 83 #/texts/79 text metadata False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 674.48, 107.39, 12.07] * Email: zxwang@iphy.ac.cn. * Email: zxwang@iphy.ac.cn. 6 12 11 84 #/texts/80 text metadata False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 685.47, 94.61, 12.07] * Email: xyang@bn-l.gov. * Email: xyang@bn-l.gov. 6 13 12 85 #/texts/81 text metadata False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 696.47, 107.28, 12.07] * Email: qkong@aps.anl.gov. * Email: qkong@aps.anl.gov. 6 14 13 86 #/texts/82 section_header back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 714.33, 88.22, 8.29] Author Contributions Author Contributions 6 15 14 87 #/texts/83 text unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 722.45, 198.07, 13.43] ⊥ J.M. and Y.-N.Z. contributed equally to this work. ⊥ J.M. and Y.-N.Z. contributed equally to this work. 6 16 15 88 #/texts/84 section_header unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 body_zone column_1_of_2 1 2 p6:body_zone:column_1_of_2:white [255, 255, 255] white False False [60.49, 741.66, 23.72, 8.29] Notes Notes 6 17 16 89 #/texts/85 text unknown_text False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:0 bottom_margin column_1_of_2 1 2 p6:bottom_margin:column_1_of_2:white [255, 255, 255] white False False [60.49, 754.4, 201.38, 8.8] The authors declare no competing fi nancial interest. The authors declare no competing fi nancial interest. 6 2 17 90 #/texts/70 page_header page_header False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:1 top_margin column_2_of_2 2 2 p6:top_margin:column_2_of_2:gray [88, 89, 91] gray True True [536.2, 49.99, 21.22, 7.35] Article Article 6 18 18 91 #/texts/86 section_header back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:1 top_margin column_2_of_2 2 2 p6:top_margin:column_2_of_2:white [255, 255, 255] white False False [324.45, 58.18, 114.79, 23.65] ■ ACKNOWLEDGMENTS ■ ACKNOWLEDGMENTS 6 19 19 92 #/texts/87 text back_matter_text False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:1 front_matter column_2_of_2 2 2 p6:front_matter:column_2_of_2:white [255, 255, 255] white False False [324.45, 84.97, 240.02, 111.02] This work was fi nancially supported by the National Natural Science Foundation of China (NSFC No. 51372268) and the National 973 Program of China (2009CB220100). The work at Brookhaven National Laboratory was supported… This work was fi nancially supported by the National Natural Science Foundation of China (NSFC No. 51372268) and the National 973 Program of China (2009CB220100). The work at Brookhaven National Laboratory was supported… 6 20 20 93 #/texts/88 section_header back_matter_heading False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:1 body_zone column_2_of_2 2 2 p6:body_zone:column_2_of_2:white [255, 255, 255] white False False [324.45, 200.54, 73.27, 23.65] ■ REFERENCES ■ REFERENCES 6 21 21 94 #/texts/89 list_item reference False low after_back_matter_stop after_back_matter_stop after_stop True p6:body_region:1 body_zone column_2_of_2 2 2 p6:body_zone:column_2_of_2:white [255, 255, 255] white False False [324.45, 227.33, 240.0, 18.84] Thackeray, M. M.; Kang, S.-H.; Johnson, C. S.; Vaughey, J. T.; Benedek, R.; Hackney, S. A. J. Mater. Chem. 2007 , 17 , 3112 -3125. Thackeray, M. 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