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achraf_28@yahoo.com (A.E.A.-G.); r2samir@yahoo.com (R.S.E.-T.); ahmedh242@yahoo.com (A.M.H.)", "text_preview": "1 Inorganic Chemistry Department, National Research Center, 33 El Bohouth St., (Former El Tahrir St.), Dokki, Giza 12622, Egypt; achraf_28@yahoo.com (A.E.A.-G.); r2samir@yahoo.com (R.S.E.-T.); ahmedh242@yahoo.com (A.M.H…", "word_count": 25, "cleaned_text": "1 Inorganic Chemistry Department, National Research Center, 33 El Bohouth St., (Former El Tahrir St.), Dokki, Giza 12622, Egypt; achraf_28@yahoo.com (A.E.A.-G.); r2samir@yahoo.com (R.S.E.-T.); ahmedh242@yahoo.com (A.M.H.)", "cleaned_text_preview": "1 Inorganic Chemistry Department, National Research Center, 33 El Bohouth St., (Former El Tahrir St.), Dokki, Giza 12622, Egypt; achraf_28@yahoo.com (A.E.A.-G.); r2samir@yahoo.com (R.S.E.-T.); ahmedh242@yahoo.com (A.M.H…", "included_in_body": false, "body_decision_reason": "first_page_metadata", "parser_body_decision_reason": "first_page_metadata", "production_usage": "", "visual_asset_type": "", "visual_asset_label": "", "visual_asset_caption_preview": "", "visual_asset_anchor_ref": "", "inside_body_region": true, "body_region_id": "p1:body_region:0", "role_guess": "metadata", "zone": "front_matter", "column": "right_crossing", "column_index": null, "column_count": null, "flags": { "docling_non_body_label": false, "page_margin_noise": false, "metadata_line": true, "affiliation_block": true, "reference_item": false, "body_sentence": false, "body_candidate": true, "body_heading": false, "heading_kind": null, "has_front_matter_zone": false, "visual_text": false, "publisher_landing_page": false, "caption_continuation_used_by_asset": false }, "background_rgb": [ 255, 255, 255 ], "page_background_rgb": [ 255, 255, 255 ], "background_delta": 0, "background_class": "white", "is_gray_background": false, "has_frame_evidence": false, "edge_dark_ratios": { "top": 0.009, "bottom": 0.0, "left": 0.031, "right": 0.01 }, "excluded_risk_level": "medium", "region_id": "p1:front_matter:right_crossing:white", "truncation_marker": "" }, { "ref": "#/texts/8", "page": 1, "label": "list_item", "order": 8000, "source_page_order": 9, "layout_order": 5, "layout_page_order": 6, "bbox": [ 166.39, 232.38, 360.32, 19.85 ], "page_size": { "width": 595.28, "height": 841.89 }, "text": "2 Institut de Minéralogie, de Physique des Matériaux et Cosmologie (IMPMC), Sorbonne Université, UMR-CNRS 7590, 4 Place Jussieu, 75752 Paris, France; 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In this study, new stoichiometric high-voltage Li-rich oxides with y = 0.0, 0.3, and 0.5 are synthesized in identical conditions using a sol-gel method. These compositions were analyzed to determine their optimal configuration and to understand their extraordinary behavior. Their nanostructural properties were investigated using XRD and Raman spectroscopy, while the morphology and grain-size distribution of the samples were characterized by BET, SEM and HRTEM analyses. The electrochemical performances of the integrated Liand Mn-rich compounds were evaluated through galvanostatic cycling and electrochemical impedance spectroscopy. The best cathode material 0.5Li2MnO3 · 0.5LiNi1/3 Co1/3 Mn1/3 O2 had a capacity retention of 83.6% after 100 cycles in the potential range 2.0-4.8 V vs. Li + /Li.", "text_preview": "Abstract: Integrated Li- and Mn-rich layered cathodes y Li2MnO3 · (1y )Li M O2 ( M = Mn, Co, and Ni) have shown their ability to deliver specific capacities close to 300 mAh g -1 , but their significant drawbacks are ca…", "word_count": 161, "cleaned_text": "Abstract: Integrated Li- and Mn-rich layered cathodes y Li2MnO3 · (1y )Li M O2 ( M = Mn, Co, and Ni) have shown their ability to deliver specific capacities close to 300 mAh g -1 , but their significant drawbacks are capacity fading and voltage decay during cycling. In this study, new stoichiometric high-voltage Li-rich oxides with y = 0.0, 0.3, and 0.5 are synthesized in identical conditions using a sol-gel method. These compositions were analyzed to determine their optimal configuration and to understand their extraordinary behavior. Their nanostructural properties were investigated using XRD and Raman spectroscopy, while the morphology and grain-size distribution of the samples were characterized by BET, SEM and HRTEM analyses. The electrochemical performances of the integrated Liand Mn-rich compounds were evaluated through galvanostatic cycling and electrochemical impedance spectroscopy. 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layered oxides; cathode materials; Li-ion batteries", "text_preview": "Li-rich compounds; layered oxides; cathode materials; Li-ion batteries", "word_count": 8, "cleaned_text": "Li-rich compounds; layered oxides; cathode materials; Li-ion batteries", "cleaned_text_preview": "Li-rich compounds; layered oxides; cathode materials; Li-ion batteries", "included_in_body": false, "body_decision_reason": "outside_body_flow", "parser_body_decision_reason": "outside_body_flow", "production_usage": "", "visual_asset_type": "", "visual_asset_label": "", "visual_asset_caption_preview": "", "visual_asset_anchor_ref": "", "inside_body_region": true, "body_region_id": "p1:body_region:0", "role_guess": "front_matter_candidate", "zone": "front_matter", "column": "right_crossing", "column_index": null, "column_count": null, "flags": { "docling_non_body_label": false, "page_margin_noise": false, "metadata_line": false, "affiliation_block": false, "reference_item": false, "body_sentence": false, "body_candidate": false, "body_heading": false, "heading_kind": null, "has_front_matter_zone": false, "visual_text": false, "publisher_landing_page": false, "caption_continuation_used_by_asset": false }, "background_rgb": [ 255, 255, 255 ], "page_background_rgb": [ 255, 255, 255 ], "background_delta": 0, "background_class": "white", "is_gray_background": false, "has_frame_evidence": false, "edge_dark_ratios": { "top": 0.03, "bottom": 0.004, "left": 0.133, "right": 0.144 }, "excluded_risk_level": "low", "region_id": "p1:front_matter:right_crossing:white", "truncation_marker": "" }, { "ref": "#/texts/2", "page": 1, "label": "text", "order": 2000, "source_page_order": 3, "layout_order": 10, "layout_page_order": 11, "bbox": [ 35.44, 505.93, 108.67, 18.53 ], "page_size": { "width": 595.28, "height": 841.89 }, "text": "Academic Editor: Giovanni Battista Appetecchi", "text_preview": "Academic Editor: Giovanni Battista Appetecchi", "word_count": 5, "cleaned_text": "Academic Editor: Giovanni Battista Appetecchi", "cleaned_text_preview": "Academic Editor: Giovanni Battista Appetecchi", "included_in_body": false, "body_decision_reason": "before_body_started", "parser_body_decision_reason": "before_body_started", "production_usage": "", "visual_asset_type": "", "visual_asset_label": "", "visual_asset_caption_preview": "", "visual_asset_anchor_ref": "", "inside_body_region": false, "body_region_id": null, "role_guess": "unknown_text", "zone": "front_matter", "column": "left", "column_index": null, "column_count": null, "flags": { "docling_non_body_label": false, "page_margin_noise": false, "metadata_line": false, "affiliation_block": false, "reference_item": false, "body_sentence": false, "body_candidate": false, "body_heading": false, "heading_kind": null, "has_front_matter_zone": false, "visual_text": false, "publisher_landing_page": false, "caption_continuation_used_by_asset": false }, "background_rgb": [ 255, 255, 255 ], "page_background_rgb": [ 255, 255, 255 ], "background_delta": 0, "background_class": "white", "is_gray_background": false, "has_frame_evidence": false, "edge_dark_ratios": { "top": 0.047, "bottom": 0.041, "left": 0.036, "right": 0.024 }, "excluded_risk_level": "low", "region_id": "p1:front_matter:left:white", "truncation_marker": "" }, { "ref": "#/texts/13", "page": 1, "label": "section_header", "order": 13000, "source_page_order": 14, "layout_order": 11, "layout_page_order": 12, "bbox": [ 166.39, 511.4, 81.74, 11.05 ], "page_size": { "width": 595.28, "height": 841.89 }, "text": "1. 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Integrated Lithium-Rich y Li2MnO3 · (1y )LiNi1/3Co1/3Mn1/3O2 Layered Cathode Nanomaterials for Lithium-Ion Batteries. Int. J. Mol. Sci. 2025 , 26 , 1346. https://doi.org/ 10.3390/ijms26031346", "text_preview": "Citation: Abdel-Ghany, A.E.; El-Tawil, R.S.; Hashem, A.M.; Mauger, A.; Julien, C.M. Integrated Lithium-Rich y Li2MnO3 · (1y )LiNi1/3Co1/3Mn1/3O2 Layered Cathode Nanomaterials for Lithium-Ion Batteries. Int. J. Mol. Sci.…", "word_count": 35, "cleaned_text": "Citation: Abdel-Ghany, A.E.; El-Tawil, R.S.; Hashem, A.M.; Mauger, A.; Julien, C.M. Integrated Lithium-Rich y Li2MnO3 · (1y )LiNi1/3Co1/3Mn1/3O2 Layered Cathode Nanomaterials for Lithium-Ion Batteries. Int. J. Mol. Sci. 2025 , 26 , 1346. 10.3390/ijms26031346", "cleaned_text_preview": "Citation: Abdel-Ghany, A.E.; El-Tawil, R.S.; Hashem, A.M.; Mauger, A.; Julien, C.M. Integrated Lithium-Rich y Li2MnO3 · (1y )LiNi1/3Co1/3Mn1/3O2 Layered Cathode Nanomaterials for Lithium-Ion Batteries. Int. J. Mol. 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( a ) X-ray diffraction (XRD) patterns of integrated layered cathode materials. ( b ) XRD reflections at ca. 2 θ = 44.5°, ( c ) detailed XRD patterns in the 2 θ range 63-67°, and ( d -f ) Rietveld refinements of the as-prepared y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) prepared by the sol-gel method. Figure 2. ( a ) X-ray diffraction (XRD) patterns of integrated layered cathode materials. ( b ) XRD reflections at ca. 2 θ = 44.5 ◦ , ( c ) detailed XRD patterns in the 2 θ range 63-67 ◦ , and ( d -f ) Rietveld refinements of the as-prepared y Li2 MnO3 · (1y )LiNi 1/3 C 1/3 Mn1/3O2 (0.0 ≤ y ≤ 0.5) prepared by the sol-gel method.", "text_preview": "Figure 2. ( a ) X-ray diffraction (XRD) patterns of integrated layered cathode materials. ( b ) XRD reflections at ca. 2 θ = 44.5°, ( c ) detailed XRD patterns in the 2 θ range 63-67°, and ( d -f ) Rietveld refinements …", "word_count": 131, "cleaned_text": "Figure 2. ( a ) X-ray diffraction (XRD) patterns of integrated layered cathode materials. ( b ) XRD reflections at ca. 2 θ = 44.5°, ( c ) detailed XRD patterns in the 2 θ range 63-67°, and ( d -f ) Rietveld refinements of the as-prepared y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) prepared by the sol-gel method. Figure 2. ( a ) X-ray diffraction (XRD) patterns of integrated layered cathode materials. ( b ) XRD reflections at ca. 2 θ = 44.5 ◦ , ( c ) detailed XRD patterns in the 2 θ range 63-67 ◦ , and ( d -f ) Rietveld refinements of the as-prepared y Li2 MnO3 · (1y )LiNi 1/3 C 1/3 Mn1/3O2 (0.0 ≤ y ≤ 0.5) prepared by the sol-gel method.", "cleaned_text_preview": "Figure 2. ( a ) X-ray diffraction (XRD) patterns of integrated layered cathode materials. 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Structural parameters obtained from Rietveld refinements of X-ray diffractograms of integrated y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 layered oxides synthesized by citric acid-assisted sol-gel method.", "text_preview": "Table 2. Structural parameters obtained from Rietveld refinements of X-ray diffractograms of integrated y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 layered oxides synthesized by citric acid-assisted sol-gel method.", "word_count": 35, "cleaned_text": "Table 2. Structural parameters obtained from Rietveld refinements of X-ray diffractograms of integrated y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 layered oxides synthesized by citric acid-assisted sol-gel method.", "cleaned_text_preview": "Table 2. 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Structural properties of y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 samples as a function of y (Li 2MnO3). ( a ) Evolution of the refined lattice parameters a hex and c hex using an hexagonal system. ( b ) Variation in the c/a ration and cell volume. ( c ) Variations in the R-factors. ( d ) Variation in the amount of Ni 2+ in the Li site and interslab thickness ( I (LiO2) ).", "text_preview": "Figure 3. Structural properties of y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 samples as a function of y (Li 2MnO3). ( a ) Evolution of the refined lattice parameters a hex and c hex using an hexagonal system. ( b ) …", "word_count": 84, "cleaned_text": "Figure 3. Structural properties of y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 samples as a function of y (Li 2MnO3). ( a ) Evolution of the refined lattice parameters a hex and c hex using an hexagonal system. ( b ) Variation in the c/a ration and cell volume. ( c ) Variations in the R-factors. ( d ) Variation in the amount of Ni 2+ in the Li site and interslab thickness ( I (LiO2) ).", "cleaned_text_preview": "Figure 3. Structural properties of y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 samples as a function of y (Li 2MnO3). ( a ) Evolution of the refined lattice parameters a hex and c hex using an hexagonal system. 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( a ) Analysis of microstrain from the full-width B at half-maximum of the XRD peaks according to Equation (1) ( b ) Evolution of the crystallite size and strain field (see Equation (1)) as a Figure 4. ( a ) Analysis of microstrain from the full-width B at half-maximum of the XRD peaks according to Equation (1) ( b ) Evolution of the crystallite size and strain field (see Equation (1)) as a function of Li2 MnO3 content ( y ).", "text_preview": "Figure 4. ( a ) Analysis of microstrain from the full-width B at half-maximum of the XRD peaks according to Equation (1) ( b ) Evolution of the crystallite size and strain field (see Equation (1)) as a Figure 4. ( a ) A…", "word_count": 84, "cleaned_text": "Figure 4. ( a ) Analysis of microstrain from the full-width B at half-maximum of the XRD peaks according to Equation (1) ( b ) Evolution of the crystallite size and strain field (see Equation (1)) as a Figure 4. 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( a -c ) EDX spectra and ( d ) comparison between theoretical and experimental values for 3D elements of prepared y Li2MnO3∙(1y ) LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) powders. Figure 7. ( a -c ) EDX spectra and ( d ) comparison between theoretical and experimental values for 3D elements of prepared y Li2 MnO3 · (1y ) LiNi 1/3 C 1/3 Mn1/3O2 (0.0 ≤ y ≤ 0.5) powders.", "text_preview": "Figure 7. ( a -c ) EDX spectra and ( d ) comparison between theoretical and experimental values for 3D elements of prepared y Li2MnO3∙(1y ) LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) powders. Figure 7. ( a -c ) EDX spectra and …", "word_count": 73, "cleaned_text": "Figure 7. ( a -c ) EDX spectra and ( d ) comparison between theoretical and experimental values for 3D elements of prepared y Li2MnO3∙(1y ) LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) powders. Figure 7. 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Rietveld and EDX analysis of Ni, Co, and Mn in the y Li2MnO3∙(1y ) LiNi1/3C1/3Mn1/3O2 composite powders in atomic percent (at. %) ratio of elements. Table 3. Rietveld and EDX analysis of Ni, Co, and Mn in the y Li2 MnO3 · (1y ) LiNi 1/3 C 1/3Mn1/3O2 composite powders in atomic percent (at. %) ratio of elements.", "text_preview": "Table 3. Rietveld and EDX analysis of Ni, Co, and Mn in the y Li2MnO3∙(1y ) LiNi1/3C1/3Mn1/3O2 composite powders in atomic percent (at. %) ratio of elements. Table 3. Rietveld and EDX analysis of Ni, Co, and Mn in the y…", "word_count": 60, "cleaned_text": "Table 3. Rietveld and EDX analysis of Ni, Co, and Mn in the y Li2MnO3∙(1y ) LiNi1/3C1/3Mn1/3O2 composite powders in atomic percent (at. %) ratio of elements. Table 3. Rietveld and EDX analysis of Ni, Co, and Mn in the y Li2 MnO3 · (1y ) LiNi 1/3 C 1/3Mn1/3O2 composite powders in atomic percent (at. %) ratio of elements.", "cleaned_text_preview": "Table 3. Rietveld and EDX analysis of Ni, Co, and Mn in the y Li2MnO3∙(1y ) LiNi1/3C1/3Mn1/3O2 composite powders in atomic percent (at. %) ratio of elements. Table 3. 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( a -c ) Nitrogen adsorption-desorption isotherms for y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) powders. ( d ) Variation in specific surface area and pore volume as function of y (Li2MnO3). Figure 8. ( a -c ) Nitrogen adsorption-desorption isotherms for y Li2 MnO3 · (1y )LiNi 1/3 C 1/3 Mn 1/3 O 2 (0.0 ≤ y ≤ 0.5) powders. ( d ) Variation in specific surface area and pore volume as function of y (Li2 MnO3).", "text_preview": "Figure 8. ( a -c ) Nitrogen adsorption-desorption isotherms for y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) powders. ( d ) Variation in specific surface area and pore volume as function of y (Li2MnO3). Figure 8. (…", "word_count": 81, "cleaned_text": "Figure 8. ( a -c ) Nitrogen adsorption-desorption isotherms for y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) powders. ( d ) Variation in specific surface area and pore volume as function of y (Li2MnO3). Figure 8. ( a -c ) Nitrogen adsorption-desorption isotherms for y Li2 MnO3 · (1y )LiNi 1/3 C 1/3 Mn 1/3 O 2 (0.0 ≤ y ≤ 0.5) powders. ( d ) Variation in specific surface area and pore volume as function of y (Li2 MnO3).", "cleaned_text_preview": "Figure 8. ( a -c ) Nitrogen adsorption-desorption isotherms for y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 (0.0 ≤ y ≤ 0.5) powders. ( d ) Variation in specific surface area and pore volume as function of y (Li2MnO3). Figure 8. 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BET results and pore structure parameters for y Li2 MnO3 · (1y )LiNi 1/3 C 1/3Mn1/3O2 powders.", "text_preview": "Table 4. BET results and pore structure parameters for y Li2 MnO3 · (1y )LiNi 1/3 C 1/3Mn1/3O2 powders.", "word_count": 19, "cleaned_text": "Table 4. BET results and pore structure parameters for y Li2 MnO3 · (1y )LiNi 1/3 C 1/3Mn1/3O2 powders.", "cleaned_text_preview": "Table 4. 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Raman scattering spectra of integrated y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 powders: ( a ) y = 0.0, ( b ) y = 0.3, ( c ) y = 0.5. ( d ) Frequency shift in the A 1g and E g modes against the composition. Figure 9. Raman scattering spectra of integrated y Li2 MnO3 · (1y )LiNi 1/3 C 1/3 Mn 1/3 O 2 powders: ( a ) y = 0.0, ( b ) y = 0.3, ( c ) y = 0.5. ( d ) Frequency shift in the A 1g and E g modes against the composition.", "text_preview": "Figure 9. Raman scattering spectra of integrated y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 powders: ( a ) y = 0.0, ( b ) y = 0.3, ( c ) y = 0.5. ( d ) Frequency shift in the A 1g and E g modes against the composition. Figure 9.…", "word_count": 100, "cleaned_text": "Figure 9. Raman scattering spectra of integrated y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 powders: ( a ) y = 0.0, ( b ) y = 0.3, ( c ) y = 0.5. ( d ) Frequency shift in the A 1g and E g modes against the composition. Figure 9. Raman scattering spectra of integrated y Li2 MnO3 · (1y )LiNi 1/3 C 1/3 Mn 1/3 O 2 powders: ( a ) y = 0.0, ( b ) y = 0.3, ( c ) y = 0.5. ( d ) Frequency shift in the A 1g and E g modes against the composition.", "cleaned_text_preview": "Figure 9. Raman scattering spectra of integrated y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 powders: ( a ) y = 0.0, ( b ) y = 0.3, ( c ) y = 0.5. ( d ) Frequency shift in the A 1g and E g modes against the composition. 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Galvanostatic charge-discharge capacity curves recorded at C/10 rate in potential range 2.0-4.8 V vs. Li + /Li for ( a ) LiNi1/3Co1/3Mn1/3O2, ( b ) Li1.134Ni0.2Co0.2Mn0.466O, ( c ) Li1.2Ni0.13Co0.13Mn0.54O2 until 5 cycles, ( d ) Li1.2Ni0.13Co0.13Mn0.54O2 over 100 cycles. Figure 10. Galvanostatic charge-discharge capacity curves recorded at C/10 rate in potential range 2.0-4.8 V vs. Li + /Li for ( a ) LiNi1/3 Co 1/3 Mn 1/3 O2 , ( b ) Li1.134 Ni 0.2Co0.2Mn0.466O, ( c ) Li 1.2 Ni0.13 Co0.13 Mn0.54 O 2 until 5 cycles, ( d ) Li 1.2 Ni0.13 Co0.13 Mn0.54 O 2 over 100 cycles.", "text_preview": "Figure 10. Galvanostatic charge-discharge capacity curves recorded at C/10 rate in potential range 2.0-4.8 V vs. Li + /Li for ( a ) LiNi1/3Co1/3Mn1/3O2, ( b ) Li1.134Ni0.2Co0.2Mn0.466O, ( c ) Li1.2Ni0.13Co0.13Mn0.54O2 u…", "word_count": 104, "cleaned_text": "Figure 10. 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Theoretical charge, discharge-specific capacities, irreversible capacities (IRs), and Coulombic efficiency (CE) of corresponding components in y Li2 MnO3 · (1y )LiNi 1/3 Co 1/3 Mn 1/3 O 2 based on mass ratio of electrode material compared with observed values corresponding to individual stage.", "text_preview": "Table 5. Theoretical charge, discharge-specific capacities, irreversible capacities (IRs), and Coulombic efficiency (CE) of corresponding components in y Li2 MnO3 · (1y )LiNi 1/3 Co 1/3 Mn 1/3 O 2 based on mass ratio of…", "word_count": 45, "cleaned_text": "Table 5. Theoretical charge, discharge-specific capacities, irreversible capacities (IRs), and Coulombic efficiency (CE) of corresponding components in y Li2 MnO3 · (1y )LiNi 1/3 Co 1/3 Mn 1/3 O 2 based on mass ratio of electrode material compared with observed values corresponding to individual stage.", "cleaned_text_preview": "Table 5. 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Differential capacity (-d Q /d V ) vs. V plots for ( a ) y Li2MnO3∙(1y ) LiNi1/3Co1/3Mn1/3O2 e trodes at first cycle, ( b ) pristine LiNi1/3Co1/3Mn1/3O2, ( c ) Li1.134Ni0.2Co0.2Mn0.466O2, and Li1.2Ni0.13Co0.13Mn0.54O2 at 1st and 100th cycles. Figure 11. Differential capacity ( -d Q /d V ) vs. V plots for ( a ) y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 electrodes at first cycle, ( b ) pristine LiNi1/3 Co 1/3 Mn 1/3 O2 , ( c ) Li1.134 Ni 0.2Co0.2Mn0.466O2, and ( d ) Li 1.2 Ni0.13 Co0.13 Mn0.54 O 2 at 1st and 100th cycles.", "text_preview": "Figure 11. Differential capacity (-d Q /d V ) vs. V plots for ( a ) y Li2MnO3∙(1y ) LiNi1/3Co1/3Mn1/3O2 e trodes at first cycle, ( b ) pristine LiNi1/3Co1/3Mn1/3O2, ( c ) Li1.134Ni0.2Co0.2Mn0.466O2, and Li1.2Ni0.13Co0.1…", "word_count": 109, "cleaned_text": "Figure 11. 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compared to other compositions.", "word_count": 5, "cleaned_text": "performance compared to other compositions.", "cleaned_text_preview": "performance compared to other compositions.", "included_in_body": false, "body_decision_reason": "inside_front_matter", "parser_body_decision_reason": "inside_front_matter", "production_usage": "", "visual_asset_type": "", "visual_asset_label": "", "visual_asset_caption_preview": "", "visual_asset_anchor_ref": "", "inside_body_region": true, "body_region_id": "p19:body_region:0", "role_guess": "body_heading", "zone": "top_margin", "column": "left_crossing", "column_index": null, "column_count": null, "flags": { "docling_non_body_label": false, "page_margin_noise": false, "metadata_line": false, "affiliation_block": false, "reference_item": false, "body_sentence": false, "body_candidate": false, "body_heading": true, "heading_kind": null, "has_front_matter_zone": false, "visual_text": false, "publisher_landing_page": false, "caption_continuation_used_by_asset": false }, "background_rgb": [ 255, 255, 255 ], "page_background_rgb": [ 255, 255, 255 ], "background_delta": 0, "background_class": "white", "is_gray_background": false, "has_frame_evidence": false, "edge_dark_ratios": { "top": 0.0, "bottom": 0.167, "left": 0.077, "right": 0.077 }, "excluded_risk_level": "low", "region_id": "p19:top_margin:left_crossing:white", "truncation_marker": "" }, { "ref": "#/texts/324", "page": 19, "label": "caption", "order": 324000, "source_page_order": 9, "layout_order": 343, "layout_page_order": 9, "bbox": [ 166.39, 252.92, 393.78, 27.07 ], "page_size": { "width": 595.28, "height": 841.89 }, "text": "Figure 12. ( a ) Cycling performance at C /10 rate and ( b ) rate capability for y Li2MnO3∙(1y ) LiNi1/3Co1/3Mn1/3O2 electrodes. Figure 12. ( a ) Cycling performance at C /10 rate and ( b ) rate capability for y Li2 MnO3 · (1y ) LiNi1/3 Co 1/3 Mn 1/3 O2 electrodes.", "text_preview": "Figure 12. ( a ) Cycling performance at C /10 rate and ( b ) rate capability for y Li2MnO3∙(1y ) LiNi1/3Co1/3Mn1/3O2 electrodes. Figure 12. ( a ) Cycling performance at C /10 rate and ( b ) rate capability for y Li2 MnO…", "word_count": 54, "cleaned_text": "Figure 12. ( a ) Cycling performance at C /10 rate and ( b ) rate capability for y Li2MnO3∙(1y ) LiNi1/3Co1/3Mn1/3O2 electrodes. Figure 12. ( a ) Cycling performance at C /10 rate and ( b ) rate capability for y Li2 MnO3 · (1y ) LiNi1/3 Co 1/3 Mn 1/3 O2 electrodes.", "cleaned_text_preview": "Figure 12. ( a ) Cycling performance at C /10 rate and ( b ) rate capability for y Li2MnO3∙(1y ) LiNi1/3Co1/3Mn1/3O2 electrodes. Figure 12. ( a ) Cycling performance at C /10 rate and ( b ) rate capability for y Li2 MnO…", "included_in_body": false, "body_decision_reason": "outside_body_flow_caption", "parser_body_decision_reason": "outside_body_flow_caption", "production_usage": "", "visual_asset_type": "", "visual_asset_label": "", "visual_asset_caption_preview": "", "visual_asset_anchor_ref": "", "inside_body_region": true, "body_region_id": "p19:body_region:0", "role_guess": "caption", "zone": "page_body", "column": "right_crossing", "column_index": null, "column_count": null, "flags": { "docling_non_body_label": true, "page_margin_noise": false, "metadata_line": false, "affiliation_block": false, "reference_item": false, "body_sentence": false, "body_candidate": true, "body_heading": false, "heading_kind": null, "has_front_matter_zone": false, "visual_text": false, "publisher_landing_page": false, "caption_continuation_used_by_asset": false }, "background_rgb": [ 255, 255, 255 ], "page_background_rgb": [ 255, 255, 255 ], "background_delta": 0, "background_class": "white", "is_gray_background": false, "has_frame_evidence": false, "edge_dark_ratios": { "top": 0.0, "bottom": 0.008, "left": 0.083, "right": 0.048 }, "excluded_risk_level": "low", "region_id": "p19:page_body:right_crossing:white", "truncation_marker": "" }, { "ref": "#/texts/325", "page": 19, "label": "text", "order": 325000, "source_page_order": 10, "layout_order": 344, "layout_page_order": 10, "bbox": [ 165.97, 286.12, 394.96, 462.37 ], "page_size": { "width": 595.28, "height": 841.89 }, "text": "Figure 12b illustrates the rate capability of the y Li₂MnO₃∙(1y )LiNi1/3Co1/3Mn1/3O₂ electrodes under various current densities ranging from 0.1C to 3C, in the voltage window 2.0-4.8 V vs. Li + /Li. For all three electrode compositions, the discharge capacity is normalized relative to their first discharge capacity at a 0.1C rate, allowing direct comparison. As a general trend, discharge capacity decreases moderately with increasing C rates for all electrodes, demonstrating the impact of higher C rates on the utilization of active materials and lithium-ion diffusion kinetics. Regarding LiNi1/3Co1/3Mn1/3O₂, this electrode exhibits typical behavior for a pristine R3 m layered structure. There is a continuous decrease in the discharge capacity as the current rate increases, retaining ~32 mAh g -1 when cycled at a high rate of 3C. In contrast to the pristine LiNi1/3Co1/3Mn1/3O₂, the Li-rich electrodes ( y = 0.3 and 0.5) demonstrate a significantly better retention of discharge capacity across current rates from 0.1C to 3C. This suggests an activation process that enhances their performance under high-rate conditions. At the 3C rate, the Li1.134Ni0.2Co0.2Mn0.467O2 and Li1.2Ni0.13Co0.13Mn0.54O2 electrodes deliver 90 and 123 mAhg -1 , respectively. The results align well with those reported in the literature [29,34,54-57]. This excellent rate capability can be attributed to several factors: (i) A well-formed layered structure, as the integrated Li2MnO3 regions enhance structural stability and facilitate lithium-ion transport during high-rate cycling. (ii) A small particle size: this reduces lithium-ion diffusion paths, promoting faster intercalation/deintercalation reactions [54]. (iii) A high specific surface area: this enhances contact between the active material and the electrolyte, improving reaction kinetics and capacity utilization. Kaewmala et al. [57] highlighted that the increased discharge capacity in the Li1.2Ni0.13Co0.13Mn0.54O2 electrode is closely associated with its higher c/a ratio. The elevated c/a ratio correlates with an increased interslab thickness ( I (LiO2)) as noted in Table 2, facilitating enhanced lithium diffusion. This structural advantage supports larger capacities even at a high current density. Upon reducing the current density back to 0.1C (Figure 12b), the electrode materials retained high discharge capacities: 250.6 mAh g -1 (a 95.68% retention of initial capacity) for y = 0.5, ~220 mAh g -1 (93.34% retention) for y = 0.3. For comparison, it is reduced to 168.1mAh g -1 (an 89.45% retention) for the pristine material ( y = 0). These results suggest that the electrode materials, particularly the Li1.2Ni0.13Co0.13Mn0.54O2 composition, maintain structural integrity and functionality even after extended cycling at high current densities. This resilience is likely due to the robust Figure 12b illustrates the rate capability of the y Li2MnO3 · (1y )LiNi1/3 Co1/3 Mn1/3 O2 electrodes under various current densities ranging from 0.1C to 3C, in the voltage window 2.0-4.8 V vs. Li + /Li. For all three electrode compositions, the discharge capacity is normalized relative to their first discharge capacity at a 0.1C rate, allowing direct comparison. As a general trend, discharge capacity decreases moderately with increasing C rates for all electrodes, demonstrating the impact of higher C rates on the utilization of active materials and lithium-ion diffusion kinetics. Regarding LiNi1/3 Co1/3 Mn1/3 O2, this electrode exhibits typical behavior for a pristine R -3 m layered structure. There is a continuous decrease in the discharge capacity as the current rate increases, retaining ~32 mAh g -1 when cycled at a high rate of 3C. In contrast to the pristine LiNi 1/3 Co 1/3 Mn 1/3 O2, the Li-rich electrodes ( y = 0.3 and 0.5) demonstrate a significantly better retention of discharge capacity across current rates from 0.1C to 3C. This suggests an activation process that enhances their performance under high-rate conditions. At the 3C rate, the Li1.134Ni0.2Co0.2Mn0.467O2 and Li1.2Ni0.13Co0.13Mn0.54O2 electrodes deliver 90 and 123 mAhg -1 , respectively. The results align well with those reported in the literature [29,34,54-57]. This excellent rate capability can be attributed to several factors: (i) A well-formed layered structure, as the integrated Li2MnO3 regions enhance structural stability and facilitate lithium-ion transport during high-rate cycling. (ii) A small particle size: this reduces lithium-ion diffusion paths, promoting faster intercalation/deintercalation reactions [54]. (iii) A high specific surface area: this enhances contact between the active material and the electrolyte, improving reaction kinetics and capacity utilization. Kaewmala et al. [57] highlighted that the increased discharge capacity in the Li1.2Ni0.13Co0.13Mn0.54O2 electrode is closely associated with its higher c / a ratio. The elevated c / a ratio correlates with an increased interslab thickness ( I (LiO2) ) as noted in Table 2, facilitating enhanced lithium diffusion. This structural advantage supports larger capacities even at a high current density. Upon reducing the current density back to 0.1C (Figure 12b), the electrode materials retained high discharge capacities: 250.6 mAh g -1 (a 95.68% retention of initial capacity) for y = 0.5, ~220 mAh g -1 (93.34% retention) for y = 0.3. For comparison, it is reduced to 168.1mAh g -1 (an 89.45% retention) for the pristine material ( y = 0). These results suggest that the electrode materials, particularly the Li1.2Ni0.13Co0.13Mn0.54O2 composition, maintain structural integrity and functionality even after extended cycling at high current densities. This resilience is likely due to the robust layered structure and structural benefits provided by the Li2MnO3 component, ensuring excellent cyclability and capacity retention.", "text_preview": "Figure 12b illustrates the rate capability of the y Li₂MnO₃∙(1y )LiNi1/3Co1/3Mn1/3O₂ electrodes under various current densities ranging from 0.1C to 3C, in the voltage window 2.0-4.8 V vs. Li + /Li. For all three electr…", "word_count": 862, "cleaned_text": "Figure 12b illustrates the rate capability of the y Li₂MnO₃∙(1y )LiNi1/3Co1/3Mn1/3O₂ electrodes under various current densities ranging from 0.1C to 3C, in the voltage window 2.0-4.8 V vs. Li + /Li. For all three electrode compositions, the discharge capacity is normalized relative to their first discharge capacity at a 0.1C rate, allowing direct comparison. As a general trend, discharge capacity decreases moderately with increasing C rates for all electrodes, demonstrating the impact of higher C rates on the utilization of active materials and lithium-ion diffusion kinetics. Regarding LiNi1/3Co1/3Mn1/3O₂, this electrode exhibits typical behavior for a pristine R3 m layered structure. There is a continuous decrease in the discharge capacity as the current rate increases, retaining ~32 mAh g -1 when cycled at a high rate of 3C. In contrast to the pristine LiNi1/3Co1/3Mn1/3O₂, the Li-rich electrodes ( y = 0.3 and 0.5) demonstrate a significantly better retention of discharge capacity across current rates from 0.1C to 3C. This suggests an activation process that enhances their performance under high-rate conditions. At the 3C rate, the Li1.134Ni0.2Co0.2Mn0.467O2 and Li1.2Ni0.13Co0.13Mn0.54O2 electrodes deliver 90 and 123 mAhg -1 , respectively. The results align well with those reported in the literature [29,34,54-57]. This excellent rate capability can be attributed to several factors: (i) A well-formed layered structure, as the integrated Li2MnO3 regions enhance structural stability and facilitate lithium-ion transport during high-rate cycling. (ii) A small particle size: this reduces lithium-ion diffusion paths, promoting faster intercalation/deintercalation reactions [54]. (iii) A high specific surface area: this enhances contact between the active material and the electrolyte, improving reaction kinetics and capacity utilization. Kaewmala et al. [57] highlighted that the increased discharge capacity in the Li1.2Ni0.13Co0.13Mn0.54O2 electrode is closely associated with its higher c/a ratio. The elevated c/a ratio correlates with an increased interslab thickness ( I (LiO2)) as noted in Table 2, facilitating enhanced lithium diffusion. This structural advantage supports larger capacities even at a high current density. Upon reducing the current density back to 0.1C (Figure 12b), the electrode materials retained high discharge capacities: 250.6 mAh g -1 (a 95.68% retention of initial capacity) for y = 0.5, ~220 mAh g -1 (93.34% retention) for y = 0.3. For comparison, it is reduced to 168.1mAh g -1 (an 89.45% retention) for the pristine material ( y = 0). These results suggest that the electrode materials, particularly the Li1.2Ni0.13Co0.13Mn0.54O2 composition, maintain structural integrity and functionality even after extended cycling at high current densities. This resilience is likely due to the robust Figure 12b illustrates the rate capability of the y Li2MnO3 · (1y )LiNi1/3 Co1/3 Mn1/3 O2 electrodes under various current densities ranging from 0.1C to 3C, in the voltage window 2.0-4.8 V vs. Li + /Li. For all three electrode compositions, the discharge capacity is normalized relative to their first discharge capacity at a 0.1C rate, allowing direct comparison. As a general trend, discharge capacity decreases moderately with increasing C rates for all electrodes, demonstrating the impact of higher C rates on the utilization of active materials and lithium-ion diffusion kinetics. Regarding LiNi1/3 Co1/3 Mn1/3 O2, this electrode exhibits typical behavior for a pristine R -3 m layered structure. There is a continuous decrease in the discharge capacity as the current rate increases, retaining ~32 mAh g -1 when cycled at a high rate of 3C. In contrast to the pristine LiNi 1/3 Co 1/3 Mn 1/3 O2, the Li-rich electrodes ( y = 0.3 and 0.5) demonstrate a significantly better retention of discharge capacity across current rates from 0.1C to 3C. This suggests an activation process that enhances their performance under high-rate conditions. At the 3C rate, the Li1.134Ni0.2Co0.2Mn0.467O2 and Li1.2Ni0.13Co0.13Mn0.54O2 electrodes deliver 90 and 123 mAhg -1 , respectively. The results align well with those reported in the literature [29,34,54-57]. This excellent rate capability can be attributed to several factors: (i) A well-formed layered structure, as the integrated Li2MnO3 regions enhance structural stability and facilitate lithium-ion transport during high-rate cycling. (ii) A small particle size: this reduces lithium-ion diffusion paths, promoting faster intercalation/deintercalation reactions [54]. (iii) A high specific surface area: this enhances contact between the active material and the electrolyte, improving reaction kinetics and capacity utilization. Kaewmala et al. [57] highlighted that the increased discharge capacity in the Li1.2Ni0.13Co0.13Mn0.54O2 electrode is closely associated with its higher c / a ratio. The elevated c / a ratio correlates with an increased interslab thickness ( I (LiO2) ) as noted in Table 2, facilitating enhanced lithium diffusion. This structural advantage supports larger capacities even at a high current density. Upon reducing the current density back to 0.1C (Figure 12b), the electrode materials retained high discharge capacities: 250.6 mAh g -1 (a 95.68% retention of initial capacity) for y = 0.5, ~220 mAh g -1 (93.34% retention) for y = 0.3. For comparison, it is reduced to 168.1mAh g -1 (an 89.45% retention) for the pristine material ( y = 0). These results suggest that the electrode materials, particularly the Li1.2Ni0.13Co0.13Mn0.54O2 composition, maintain structural integrity and functionality even after extended cycling at high current densities. This resilience is likely due to the robust layered structure and structural benefits provided by the Li2MnO3 component, ensuring excellent cyclability and capacity retention.", "cleaned_text_preview": "Figure 12b illustrates the rate capability of the y Li₂MnO₃∙(1y )LiNi1/3Co1/3Mn1/3O₂ electrodes under various current densities ranging from 0.1C to 3C, in the voltage window 2.0-4.8 V vs. Li + /Li. 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EIS measurements ( Z ′′ vs. Z ′ plots) of y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 ( y = 0.0, 0.3, and 0.5) electrodes: ( a ) Fresh electrodes, ( b ) after 50 cycles at a 0.1C rate, ( c ) equivalent model circuit. Plots of the real part of the impedance vs. ω -1/2 for ( d ) fresh electrodes and ( e ) after 100 cycles.", "text_preview": "Figure 13. EIS measurements ( Z ′′ vs. Z ′ plots) of y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 ( y = 0.0, 0.3, and 0.5) electrodes: ( a ) Fresh electrodes, ( b ) after 50 cycles at a 0.1C rate, ( c ) equivalent mode…", "word_count": 79, "cleaned_text": "Figure 13. EIS measurements ( Z ′′ vs. Z ′ plots) of y Li2 MnO3 · (1y ) LiNi 1/3 Co 1/3 Mn 1/3 O 2 ( y = 0.0, 0.3, and 0.5) electrodes: ( a ) Fresh electrodes, ( b ) after 50 cycles at a 0.1C rate, ( c ) equivalent model circuit. Plots of the real part of the impedance vs. ω -1/2 for ( d ) fresh electrodes and ( e ) after 100 cycles.", "cleaned_text_preview": "Figure 13. 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Fitting results of Nyquist plots for the y Li2 MnO3 · (1y ) LiNi 1/3 C 1/3Mn1/3O2 ( y =0.0, 0.3 and 0.5) electrodes before cycling and after 100 cycles.", "text_preview": "Table 6. Fitting results of Nyquist plots for the y Li2 MnO3 · (1y ) LiNi 1/3 C 1/3Mn1/3O2 ( y =0.0, 0.3 and 0.5) electrodes before cycling and after 100 cycles.", "word_count": 32, "cleaned_text": "Table 6. Fitting results of Nyquist plots for the y Li2 MnO3 · (1y ) LiNi 1/3 C 1/3Mn1/3O2 ( y =0.0, 0.3 and 0.5) electrodes before cycling and after 100 cycles.", "cleaned_text_preview": "Table 6. 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Area-specific impedance (ASI) of parent and y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 ( y =0.0, 0.3, and 0.5) as a function of depth of discharge (DOD): ( a ) fresh cell and ( b ) after 100 cycles. Figure 14. Area-specific impedance (ASI) of parent and y Li2 MnO3 · (1y )LiNi 1/3 C 1/3 Mn1/3O2 ( y = 0.0, 0.3, and 0.5) as a function of depth of discharge (DOD): ( a ) fresh cell and ( b ) after 100 cycles.", "text_preview": "Figure 14. Area-specific impedance (ASI) of parent and y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 ( y =0.0, 0.3, and 0.5) as a function of depth of discharge (DOD): ( a ) fresh cell and ( b ) after 100 cycles. Figure 14. Area-sp…", "word_count": 82, "cleaned_text": "Figure 14. Area-specific impedance (ASI) of parent and y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 ( y =0.0, 0.3, and 0.5) as a function of depth of discharge (DOD): ( a ) fresh cell and ( b ) after 100 cycles. Figure 14. Area-specific impedance (ASI) of parent and y Li2 MnO3 · (1y )LiNi 1/3 C 1/3 Mn1/3O2 ( y = 0.0, 0.3, and 0.5) as a function of depth of discharge (DOD): ( a ) fresh cell and ( b ) after 100 cycles.", "cleaned_text_preview": "Figure 14. Area-specific impedance (ASI) of parent and y Li2MnO3∙(1y )LiNi1/3C1/3Mn1/3O2 ( y =0.0, 0.3, and 0.5) as a function of depth of discharge (DOD): ( a ) fresh cell and ( b ) after 100 cycles. Figure 14. 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