Excluded Docling blocks

这里是差集：Docling 全量解析 text block 减去最终会进入正文的 block。优先人工检查 risk=high / medium。

layout_review.html excluded_blocks.json excluded_blocks.tsv final_body_blocks.tsv visual_assets.tsv original.pdf

Diff Summary

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Truncation

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    "text_preview": "X. Liao, Q. Huang, S. Mai, X. Wang, M. Xu, L. Xing, Y. Liao, W. Li, J. Power Sources 272 (2014) 501 e 507."
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Excluded Page Overlays

这些框显示被排除块，同时叠加真实图表资产框。青色虚线表示该 text block 被图表资产 caption 吸收；红色 STOP 是截断触发点，红色框是截断后被排除的块。

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Visual Assets

这是实际图表资产输出，不是审计层重新推断。

#	type	label	page	caption source	confidence	bbox	caption
1	figure	Docling Figure 1	1	missing_caption	0.55	[196.92, 321.27, 246.16, 181.79]
2	figure	Fig. 1	2	direct_caption_ref	0.82	[131.0, 691.82, 342.01, 35.22]	Fig. 1. The reaction mechanism of eliminating H2O and HF by nitriles.
3	figure	Fig. 2	4	direct_caption_ref	0.82	[74.37, 66.21, 457.39, 410.28]	Fig. 2. (a) The conductivity of commercial electrolytes containing different weight ratios of succinonitrile at temperatures range from 30 C to 80 C. (b) LSV of the 1 M LiPF6/EC/ DEC commercial electrolyte with or without 1wt% SN. Working electrode: Pt, counter and reference electrodes: Li, scan rate: 1 mV s 1 . (c) Frontier molecular orbitals of EC, DEC and SN and their energies of occupied (HOMO) and unoccupied (LUMO) (in Ha). (d) Discharge capacity after 50 cycles of Li/Li1.2Ni0.2Mn0.6O2 half-cells containing various weight ratios of SN.
4	figure	Fig. 3	4	direct_caption_ref	0.82	[102.73, 543.9, 399.68, 163.5]	Fig. 3. Ac impedance spectra of the Li/Li1.2Ni0.2Mn0.6O2 half-cells containing various weight ratios of SN: (a) After 1 cycles, (b) After 5 cycles.
5	figure	Fig. 4	5	direct_caption_ref	0.82	[107.9, 66.22, 370.32, 148.69]	Fig. 4. TGA diagrams and DTG curves of commercial electrolyte (a) and 1wt % SN electrolyte (b).
6	figure	Fig. 5	5	direct_caption_ref	0.82	[35.06, 528.66, 245.99, 181.36]	Fig. 5. Discharge capacities and coulombic ef fi ciencies of the Li/Li1.2Ni0.2Mn0.6O2 half-cells at a 0.1 C current density with or without 1wt % SN at 55 C, the inset displays SEM images of the batteries after 50 cycles.
7	figure	Fig. 6	6	direct_caption_ref	0.82	[116.85, 66.57, 371.3, 279.88]	Fig. 6. Discharge capacities of Li/Li1.2Ni0.2Mn0.6O2 with 1wt% SN-based electrolyte at different cut-off voltages: (a) 2.0 e 4.8 V, (b) 2.0 e 4.9 V, (c) 2.0 e 5.0 V and (d) 2.0 e 5.2 V.
8	figure	Fig. 7	6	direct_caption_ref	0.82	[131.2, 382.85, 341.58, 172.34]	Fig. 7. SEM images of the surface of LNMO cathode after 5 cycles with: (a) commercial electrolyte (b) 1wt% SN.
9	figure	Fig. 8	7	direct_caption_ref	0.82	[52.24, 66.75, 482.78, 295.51]	Fig. 8. XPS spectra of the regions of Li1.2Ni0.2Mn0.6O2 after 50 cycles: (a) N1s with commercial electrolyte, (b) N1s with 1wt% SN-based electrolyte, (c) Mn2p with commercial electrolyte, (d) Mn2p with 1wt% SN-based electrolyte, (e) Ni2p with commercial electrolyte, (f) Ni2p with 1wt% SN-based electrolyte.

Excluded Blocks

risk	page	order	label	role	reason	parser reason	trunc	body region	region	bg	bbox	raw text	cleaned text
high	1	13	text	unknown_text	outside_body_flow	outside_body_flow			p1:page_body:column_1_of_2:white	[255, 255, 255] white	[32.83, 558.33, 107.65, 48.74]	Article history: Received 16 July 2015 Received in revised form 27 October 2015 Accepted 28 October 2015 Available online 13 December 2015	Article history: Received 16 July 2015 Received in revised form 27 October 2015 Accepted 28 October 2015 Available online 13 December 2015
medium	1	5	text	affiliation	front_matter_author_line	front_matter_author_line			p1:page_body:column_1_of_2:white	[255, 255, 255] white	[32.83, 217.13, 438.2, 26.17]	Renjie Chen a, b, * , Fan Liu a , Yan Chen a , Yusheng Ye a , Yongxin Huang a , Feng Wu a, b, ** , Li Li a, b	Renjie Chen a, b, * , Fan Liu a , Yan Chen a , Yusheng Ye a , Yongxin Huang a , Feng Wu a, b, ** , Li Li a, b
medium	1	21	text	abstract_candidate	inside_abstract	inside_abstract			p1:page_body:column_2_of_2:white	[255, 255, 255] white	[197.23, 551.28, 355.66, 73.58]	Succinonitrile (SN) has been used as functional additive to improve the thermal stability and broaden the oxidation electrochemical window of commercial electrolyte 1 M LiPF6/EC/DEC (1:1, by volume) for highvoltage LIBs (cathode: Li1.2Ni0.2Mn0.6O2, anode: Li). 1 wt % SN-based electrolyte showed a wide electrochemical oxidation window of 5.4 V vs Li þ /Li and excellent thermal stability demonstrated by thermogravimetry (TG) and X-ray photoelectron spectroscopy (XPS), as well as theoretical analysis according to molecular orbital theory. The LNMO (Li1.2Ni0.2Mn0.6O2) battery with 1 wt % SN-based electrolyte showed better cyclability and capacity retention when charged to higher cut-off voltage. The improved battery performance is mainly attributed to the formation of uniform cathode electrolyte interface (CEI)	Succinonitrile (SN) has been used as functional additive to improve the thermal stability and broaden the oxidation electrochemical window of commercial electrolyte 1 M LiPF6/EC/DEC (1:1, by volume) for highvoltage LIBs (cathode: Li1.2Ni0.2Mn0.6O2, anode: Li). 1 wt % SN-based electrolyte showed a wide electrochemical oxidation window of 5.4 V vs Li þ /Li and excellent thermal stability demonstrated by thermogravimetry (TG) and X-ray photoelectron spectroscopy (XPS), as well as theoretical analysis according to molecular orbital theory. The LNMO (Li1.2Ni0.2Mn0.6O2) battery with 1 wt % SN-based electrolyte showed better cyclability and capacity retention when charged to higher cut-off voltage. The improved battery performance is mainly attributed to the formation of uniform cathode electrolyte interface (CEI)
medium	2	23	text	abstract_candidate	inside_abstract	inside_abstract		p2:body_region:0	p2:front_matter:column_1_of_2:white	[255, 255, 255] white	[42.52, 106.77, 87.78, 5.94]	Cathode electrolyte interface	Cathode electrolyte interface
low	1	0	page_header	page_header	docling_page_header	docling_page_header			p1:top_margin:column_2_of_2:white	[255, 255, 255] white	[228.36, 47.78, 129.01, 6.37]	Journal of Power Sources 306 (2016) 70 e 77	Journal of Power Sources 306 (2016) 70 e 77
low	1	1	text	front_matter_heading	first_page_metadata	first_page_metadata			p1:page_body:column_2_of_2:gray	[229, 229, 229] gray	[216.51, 79.77, 156.17, 1.59]	Contents lists available at ScienceDirect	Contents lists available at ScienceDirect
low	1	2	section_header	title_candidate	non_body_heading	non_body_heading			p1:page_body:column_2_of_2:gray	[229, 229, 229] gray	[210.56, 98.49, 167.92, 12.99]	Journal of Power Sources	Journal of Power Sources
low	1	3	text	metadata	first_page_metadata	first_page_metadata			p1:page_body:column_2_of_2:gray	[229, 229, 229] gray	[165.09, 135.72, 258.93, 1.59]	j o urnal homepage: www.elsevier.com/locate/jpowsour	j o urnal homepage:
low	1	4	section_header	title_candidate	non_body_heading	non_body_heading			p1:page_body:column_1_of_2:white	[255, 255, 255] white	[32.83, 178.39, 420.44, 29.76]	An investigation of functionalized electrolyte using succinonitrile additive for high voltage lithium-ion batteries	An investigation of functionalized electrolyte using succinonitrile additive for high voltage lithium-ion batteries
low	1	6	footnote	footnote	docling_footnote	docling_footnote			p1:page_body:column_1_of_2:white	[255, 255, 255] white	[32.82, 250.08, 437.89, 15.93]	a School of Materials Science & Engineering, Beijing Key Laboratory of Environmental Science and Engineering, Beijing Institute of Technology, Beijing 100081, China	a School of Materials Science & Engineering, Beijing Key Laboratory of Environmental Science and Engineering, Beijing Institute of Technology, Beijing 100081, China
low	1	7	footnote	footnote	docling_footnote	docling_footnote			p1:page_body:column_1_of_2:white	[255, 255, 255] white	[32.83, 267.2, 250.38, 7.37]	b Collaborative Innovation Center of Electric Vehicles in Beijing, Beijing 100081, China	b Collaborative Innovation Center of Electric Vehicles in Beijing, Beijing 100081, China
low	1	8	section_header	front_matter_heading	front_matter_heading	front_matter_heading			p1:page_body:column_1_of_2:unknown	None unknown	[32.83, 305.29, 86.34, 0.06]	h i g h l i g h t s	h i g h l i g h t s
low	1	12	section_header	front_matter_heading	front_matter_heading	front_matter_heading			p1:page_body:column_1_of_2:unknown	None unknown	[32.83, 537.0, 95.61, 0.06]	a r t i c l e i n f o	a r t i c l e i n f o
low	1	14	footnote	footnote	first_page_metadata	first_page_metadata			p1:page_body:column_1_of_2:white	[255, 255, 255] white	[32.83, 648.88, 251.1, 24.01]	* Corresponding author. School of Materials Science & Engineering, Beijing Key Laboratory of Environmental Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.	* Corresponding author. School of Materials Science & Engineering, Beijing Key Laboratory of Environmental Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.
low	1	15	footnote	footnote	first_page_metadata	first_page_metadata			p1:page_body:column_1_of_2:white	[255, 255, 255] white	[32.83, 675.13, 251.1, 23.95]	** Corresponding author. School of Materials Science & Engineering, Beijing Key Laboratory of Environmental Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.	** Corresponding author. School of Materials Science & Engineering, Beijing Key Laboratory of Environmental Science and Engineering, Beijing Institute of Technology, Beijing 100081, China.
low	1	16	footnote	footnote	first_page_metadata	first_page_metadata			p1:page_body:column_1_of_2:white	[255, 255, 255] white	[32.83, 701.71, 250.98, 14.5]	E-mail addresses: chenrj@bit.edu.cn (R. Chen), wufeng863@vip.sina.com (F. Wu).	E-mail addresses: chenrj@bit.edu.cn (R. Chen), wufeng863@vip.sina.com (F. Wu).
low	1	17	page_footer	page_footer	first_page_metadata	first_page_metadata			p1:bottom_margin:column_1_of_2:white	[248, 251, 252] white	[32.83, 728.64, 144.66, 5.94]	http://dx.doi.org/10.1016/j.jpowsour.2015.10.105
low	1	18	page_footer	page_footer	first_page_metadata	first_page_metadata			p1:bottom_margin:column_1_of_2:white	[255, 255, 255] white	[32.83, 735.78, 156.13, 7.43]	0378-7753/ © 2015 Elsevier B.V. All rights reserved.	0378-7753/ © 2015 Elsevier B.V. All rights reserved.
low	1	19	section_header	body_heading	body_heading	body_heading			p1:page_body:column_2_of_2:unknown	None unknown	[197.22, 305.29, 152.63, 0.06]	g r a p h i c a l a b s t r a c t	g r a p h i c a l a b s t r a c t
low	1	20	section_header	abstract_heading	abstract_heading	abstract_heading			p1:page_body:column_2_of_2:unknown	None unknown	[197.23, 537.0, 67.73, 0.06]	a b s t r a c t	a b s t r a c t
low	2	22	text	front_matter_heading	front_matter_heading	front_matter_heading		p2:body_region:0	p2:front_matter:column_1_of_2:white	[255, 255, 255] white	[42.52, 72.47, 51.66, 31.68]	Keywords: Succinonitrile High voltage Thermal stability	Keywords: Succinonitrile High voltage Thermal stability
low	2	24	section_header	body_heading	body_heading	body_heading		p2:body_region:0	p2:body_zone:column_1_of_2:white	[255, 255, 255] white	[42.52, 155.29, 62.12, 7.97]	1. Introduction	1. Introduction
low	2	29	page_header	page_header	docling_page_header	docling_page_header		p2:body_region:1	p2:top_margin:column_2_of_2:white	[255, 255, 255] white	[218.72, 47.78, 167.65, 6.37]	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77
low	2	30	page_header	page_header	docling_page_header	docling_page_header		p2:body_region:1	p2:top_margin:column_2_of_2:white	[255, 255, 255] white	[555.48, 48.2, 7.11, 5.94]	71	71
low	2	32	text	metadata	outside_body_flow_metadata_line	outside_body_flow_metadata_line		p2:body_region:1	p2:front_matter:column_2_of_2:white	[255, 255, 255] white	[425.93, 95.74, 136.69, 8.36]	© 2015 Elsevier B.V. All rights reserved.	© 2015 Elsevier B.V. All rights reserved.
low	2	36	section_header	body_heading	body_heading	body_heading		p2:body_region:1	p2:body_zone:column_2_of_2:white	[255, 255, 255] white	[311.53, 511.09, 65.35, 7.97]	2. Experimental	2. Experimental
low	2	37	section_header	body_heading	body_heading	body_heading		p2:body_region:1	p2:body_zone:column_2_of_2:white	[255, 255, 255] white	[311.53, 532.44, 139.92, 7.42]	2.1. Preparation of electrolyte systems	2.1. Preparation of electrolyte systems
low	2	39	caption	caption	outside_body_flow_caption	outside_body_flow_caption		p2:body_region:1	p2:bottom_margin:column_2_of_2:white	[255, 255, 255] white	[199.33, 737.02, 206.37, 6.38]	Fig. 1. The reaction mechanism of eliminating H2O and HF by nitriles.	Fig. 1. The reaction mechanism of eliminating H2O and HF by nitriles.
low	3	40	page_header	page_header	docling_page_header	docling_page_header		p3:body_region:0	p3:top_margin:column_1_of_2:white	[255, 255, 255] white	[32.82, 48.21, 7.16, 5.94]	72	72
low	3	41	section_header	body_heading	body_heading	body_heading		p3:body_region:0	p3:body_zone:column_1_of_2:white	[255, 255, 255] white	[32.83, 66.77, 229.41, 7.42]	2.2. Preparation of the electrodes and the construction of cells	2.2. Preparation of the electrodes and the construction of cells
low	3	43	section_header	body_heading	body_heading	body_heading		p3:body_region:0	p3:body_zone:column_1_of_2:white	[255, 255, 255] white	[32.83, 171.36, 129.89, 7.42]	2.3. Electrochemical measurements	2.3. Electrochemical measurements
low	3	48	section_header	body_heading	body_heading	body_heading		p3:body_region:0	p3:body_zone:column_1_of_2:white	[255, 255, 255] white	[32.83, 453.81, 116.72, 7.42]	2.4. Materials characterizations	2.4. Materials characterizations
low	3	51	section_header	body_heading	body_heading	body_heading		p3:body_region:0	p3:body_zone:column_1_of_2:white	[255, 255, 255] white	[32.83, 568.41, 105.41, 7.97]	3. Results and discussions	3. Results and discussions
low	3	54	page_header	page_header	docling_page_header	docling_page_header			p3:top_margin:column_2_of_2:white	[255, 255, 255] white	[209.03, 47.78, 167.65, 6.37]	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77
low	4	60	page_header	page_header	docling_page_header	docling_page_header			p4:top_margin:right_crossing:white	[255, 255, 255] white	[218.72, 47.78, 167.65, 6.37]	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77
low	4	61	page_header	page_header	docling_page_header	docling_page_header			p4:top_margin:right:white	[255, 255, 255] white	[555.42, 48.2, 7.16, 5.94]	73	73
low	4	62	caption	caption	outside_body_flow_caption	outside_body_flow_caption			p4:page_body:full:white	[255, 255, 255] white	[42.52, 485.86, 520.07, 32.94]	Fig. 2. (a) The conductivity of commercial electrolytes containing different weight ratios of succinonitrile at temperatures range from 30 C to 80 C. (b) LSV of the 1 M LiPF6/EC/ DEC commercial electrolyte with or without 1wt% SN. Working electrode: Pt, counter and reference electrodes: Li, scan rate: 1 mV s 1 . (c) Frontier molecular orbitals of EC, DEC and SN and their energies of occupied (HOMO) and unoccupied (LUMO) (in Ha). (d) Discharge capacity after 50 cycles of Li/Li1.2Ni0.2Mn0.6O2 half-cells containing various weight ratios of SN.	Fig. 2. (a) The conductivity of commercial electrolytes containing different weight ratios of succinonitrile at temperatures range from 30 C to 80 C. (b) LSV of the 1 M LiPF6/EC/ DEC commercial electrolyte with or without 1wt% SN. Working electrode: Pt, counter and reference electrodes: Li, scan rate: 1 mV s 1 . (c) Frontier molecular orbitals of EC, DEC and SN and their energies of occupied (HOMO) and unoccupied (LUMO) (in Ha). (d) Discharge capacity after 50 cycles of Li/Li1.2Ni0.2Mn0.6O2 half-cells containing various weight ratios of SN.
low	4	63	caption	caption	outside_body_flow_caption	outside_body_flow_caption			p4:page_body:right_crossing:white	[255, 255, 255] white	[95.02, 716.67, 415.04, 6.98]	Fig. 3. Ac impedance spectra of the Li/Li1.2Ni0.2Mn0.6O2 half-cells containing various weight ratios of SN: (a) After 1 cycles, (b) After 5 cycles.	Fig. 3. Ac impedance spectra of the Li/Li1.2Ni0.2Mn0.6O2 half-cells containing various weight ratios of SN: (a) After 1 cycles, (b) After 5 cycles.
low	5	64	page_header	page_header	docling_page_header	docling_page_header		p5:body_region:0	p5:top_margin:column_1_of_2:white	[255, 255, 255] white	[32.82, 48.2, 6.82, 5.94]	74	74
low	5	65	caption	caption	outside_body_flow_caption	outside_body_flow_caption			p5:page_body:column_1_of_2:white	[255, 255, 255] white	[150.29, 225.77, 285.11, 6.38]	Fig. 4. TGA diagrams and DTG curves of commercial electrolyte (a) and 1wt % SN electrolyte (b).	Fig. 4. TGA diagrams and DTG curves of commercial electrolyte (a) and 1wt % SN electrolyte (b).
low	5	68	caption	caption	outside_body_flow_caption	outside_body_flow_caption		p5:body_region:0	p5:bottom_margin:column_1_of_2:white	[255, 255, 255] white	[32.82, 719.9, 251.05, 23.4]	Fig. 5. Discharge capacities and coulombic ef fi ciencies of the Li/Li1.2Ni0.2Mn0.6O2 half-cells at a 0.1 C current density with or without 1wt % SN at 55 C, the inset displays SEM images of the batteries after 50 cycles.	Fig. 5. Discharge capacities and coulombic ef fi ciencies of the Li/Li1.2Ni0.2Mn0.6O2 half-cells at a 0.1 C current density with or without 1wt % SN at 55 C, the inset displays SEM images of the batteries after 50 cycles.
low	5	69	page_header	page_header	docling_page_header	docling_page_header			p5:top_margin:column_2_of_2:white	[255, 255, 255] white	[209.03, 47.78, 167.65, 6.37]	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77
low	6	73	page_header	page_header	docling_page_header	docling_page_header			p6:top_margin:column_2_of_2:white	[255, 255, 255] white	[218.72, 47.78, 167.65, 6.37]	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77
low	6	74	page_header	page_header	docling_page_header	docling_page_header		p6:body_region:1	p6:top_margin:column_2_of_2:white	[255, 255, 255] white	[555.25, 48.21, 7.29, 5.94]	75	75
low	6	75	caption	caption	outside_body_flow_caption	outside_body_flow_caption			p6:page_body:column_1_of_2:white	[255, 255, 255] white	[49.04, 356.3, 506.98, 7.01]	Fig. 6. Discharge capacities of Li/Li1.2Ni0.2Mn0.6O2 with 1wt% SN-based electrolyte at different cut-off voltages: (a) 2.0 e 4.8 V, (b) 2.0 e 4.9 V, (c) 2.0 e 5.0 V and (d) 2.0 e 5.2 V.	Fig. 6. Discharge capacities of Li/Li1.2Ni0.2Mn0.6O2 with 1wt% SN-based electrolyte at different cut-off voltages: (a) 2.0 e 4.8 V, (b) 2.0 e 4.9 V, (c) 2.0 e 5.0 V and (d) 2.0 e 5.2 V.
low	6	76	caption	caption	outside_body_flow_caption	outside_body_flow_caption			p6:page_body:column_1_of_2:white	[255, 255, 255] white	[137.93, 565.02, 329.18, 6.38]	Fig. 7. SEM images of the surface of LNMO cathode after 5 cycles with: (a) commercial electrolyte (b) 1wt% SN.	Fig. 7. SEM images of the surface of LNMO cathode after 5 cycles with: (a) commercial electrolyte (b) 1wt% SN.
low	7	79	page_header	page_header	docling_page_header	docling_page_header		p7:body_region:0	p7:top_margin:left:white	[255, 255, 255] white	[32.82, 48.21, 7.05, 5.94]	76	76
low	7	80	page_header	page_header	docling_page_header	docling_page_header			p7:top_margin:left_crossing:white	[255, 255, 255] white	[209.03, 47.78, 167.65, 6.37]	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77	R. Chen et al. / Journal of Power Sources 306 (2016) 70 e 77
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