Docling layout block audit

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Summary

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Diff Summary

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Truncation

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Page Overlays

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Visual Assets

这里对齐真实图表资产提取链路。caption_source=embedded_table_cell 表示表注来自 Docling table cell，不会出现在 text block 审计差集里；caption_continuation_used_by_asset 表示某个 text block 已被图表 caption 吸收，不应按普通 metadata 解读。

#typelabelpagecaption sourcesuppressedduplicate reasonrescue reasongroupconfidencebboxcaption
1figureFig. 13direct_caption_ref0.82[134.62, 56.55, 333.87, 121.09]Fig. 1. Optimized structures and Eb values of solvents-Li + and DTMS-Li + .
2figureFig. 23direct_caption_ref0.82[126.51, 219.03, 339.8, 241.36]Fig. 2. (a) Cycling performance and (b) rate capability of LRM/Li cell. (c) (d) 1st, 20th, 50th, and 100th charge -discharge curves of LRM/Li cell during cycling.
3figureFig. 34direct_caption_ref0.82[127.57, 56.82, 339.17, 237.05]Fig. 3. EIS results of LRM/Li cell in BE and 2 vol% DTMS electrolyte after (a) pre-cycling and (b) cycling. (c) Values of Rf and Rct.
4figureFig. 44direct_caption_ref0.82[126.02, 335.06, 341.65, 242.9]Fig. 4. TEM and SEM images of LRM cathodes after cycling (a), (c) with BE and (b), (d) 2 vol% DTMS electrolyte.
5figureFig. 55direct_caption_ref0.82[77.13, 57.01, 440.24, 486.67]Fig. 5. (a)XPS spectra of LRM cathodes after cycling with BE and 2 vol% DTMS electrolytes. (b) XRD patterns of LRM cathodes and (c) dissolution of transition metal on Li electrode taken from cell after cycling.
6figureFig. 66direct_caption_ref0.82[126.82, 57.22, 340.55, 172.57]Fig. 6. (a) Discharge profiles of cell during cycling with BE + 1000 ppm HF and 2 vol% DTMS-containing + 1000 ppm HF; F 1s XPS spectra of LRM cathodes after cycling with (b) BE + 1000 ppm HF and (c) 2 vol% DTMS-containing + 1000 ppm HF electrolyte.
7figureDocling Figure 76missing_caption0.55[127.42, 421.93, 340.9, 242.33]
8figureFig. 87direct_caption_ref0.82[128.27, 57.42, 337.83, 98.38]Fig. 8. Possible mechanism of DTMS.
9tableTable 12nearby_text_caption0.82[364.83, 83.37, 133.46, 53.61]Table 1 Calculated Eox (V vs. Li +

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white		False[224.72, 33.45, 145.08, 11.73]Journal of Power Sources 580 (2023) 233437Journal of Power Sources 580 (2023) 233437
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gray		False[228.42, 63.48, 142.99, 7.31]Contents lists available at ScienceDirectContents lists available at ScienceDirect
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gray		False[219.29, 87.36, 163.01, 12.79]Journal of Power SourcesJournal of Power Sources
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gray		False[195.48, 119.22, 208.78, 6.67]journal homepage: www.elsevier.com/locate/jpowsourjournal homepage:
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white		False[37.59, 168.03, 450.29, 46.81]Efficient improvement in electrochemical properties of high-voltage Li-rich Mn-based layered oxide cathode by addition of 1,3-divinyltetramethyldisiloxane to electrolyteEfficient improvement in electrochemical properties of high-voltage Li-rich Mn-based layered oxide cathode by addition of 1,3-divinyltetramethyldisiloxane to electrolyte
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white		False[37.59, 229.44, 339.84, 9.69]Tao Huang, Xiangzhen Zheng, Chunfeng Yan, Ying Pan , Maoxiang WuTao Huang, Xiangzhen Zheng, Chunfeng Yan, Ying Pan , Maoxiang Wu
16textaffiliationFalselowfirst_page_author_or_affiliationfirst_page_author_or_affiliation
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white		False[37.59, 248.69, 437.99, 5.85]Key Laboratory of Optoelectronic Materials Chemistry and Physics, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou,Key Laboratory of Optoelectronic Materials Chemistry and Physics, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou,
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white		False[37.59, 257.25, 56.39, 5.85]350002, PR China350002, PR China
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p1:body_region:0p1:front_matter:column_1_of_2:white[255, 255, 255]
white		False[37.59, 289.44, 75.13, 6.4]H I G H L I G H T SH I G H L I G H T S
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white		False[37.59, 308.87, 231.27, 6.58]DTMS improved cyclic stability of LRM cathode lithium-ion batteries.DTMS improved cyclic stability of LRM cathode lithium-ion batteries.
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white		False[37.59, 318.9, 179.65, 6.58]The DTMS-derived layer maintains interface stability.The DTMS-derived layer maintains interface stability.
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white		False[37.59, 328.99, 170.36, 6.58]DTMS reacts with the HF/F from the electrolyte.DTMS reacts with the HF/F from the electrolyte.
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white		False[37.59, 363.31, 88.53, 6.4]A R T I C L E I N F OA R T I C L E I N F O
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white		False[202.0, 363.31, 67.15, 6.4]A B S T R A C TA B S T R A C T
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white		False[37.59, 382.2, 93.07, 40.15]Keywords: Lithium-ion battery Li-rich layered oxide cathode Solid electrolyte interphase film Interfacial stabilityKeywords: Lithium-ion battery Li-rich layered oxide cathode Solid electrolyte interphase film Interfacial stability
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white		False[37.59, 425.06, 94.03, 5.85]1,3-divinyltetramethyldisiloxane1,3-divinyltetramethyldisiloxane
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white		False[202.0, 382.68, 357.8, 73.53]1,3-Divinyltetramethyldisiloxane (DTMS) is a multifunctional additive that is used to improves the cycling stability and capacity retention of Li-rich Mn-based layered oxide cathodes (LRMs). Cycling performance evaluati…1,3-Divinyltetramethyldisiloxane (DTMS) is a multifunctional additive that is used to improves the cycling stability and capacity retention of Li-rich Mn-based layered oxide cathodes (LRMs). Cycling performance evaluati…
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white		False[37.59, 488.79, 62.58, 7.31]1. Introduction1. Introduction
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white		False[37.59, 509.71, 253.44, 132.83]Lithium ion batteries (LIBs) have been used in electric vehicles because of their high energy density, safety, and low price; however, these qualities need to be further enhanced to extend the maximum distance that elec…Lithium ion batteries (LIBs) have been used in electric vehicles because of their high energy density, safety, and low price; however, these qualities need to be further enhanced to extend the maximum distance that elec…
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white		False[42.63, 672.84, 153.92, 16.16]* Corresponding author. E-mail address: mxwu@fjirsm.ac.cn (M. Wu).* Corresponding author. E-mail address: mxwu@fjirsm.ac.cn (M. Wu).
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white		False[37.59, 699.43, 160.64, 6.58]https://doi.org/10.1016/j.jpowsour.2023.233437
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white		False[37.52, 708.95, 299.92, 17.48]Available online 26 July 2023 Received 28 February 2023; Received in revised form 7 June 2023; Accepted 17 July 2023Available online 26 July 2023 Received 28 February 2023; Received in revised form 7 June 2023; Accepted 17 July 2023
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white		False[37.52, 724.32, 167.09, 11.73]0378-7753/© 2023 Elsevier B.V. All rights reserved.0378-7753/© 2023 Elsevier B.V. All rights reserved.
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white		False[306.59, 488.79, 125.16, 7.31]electrode/electrolyte interface [9].electrode/electrolyte interface [9].
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white		False[306.59, 499.22, 253.42, 143.32]To overcome these problems, several approaches have been explored in the past decade, including doping and coating [10 -13]. Recently, a simple and economical strategy has been developed: the formation of a protective i…To overcome these problems, several approaches have been explored in the past decade, including doping and coating [10 -13]. Recently, a simple and economical strategy has been developed: the formation of a protective i…
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white		False[433.38, 33.65, 124.91, 10.42]Journal of Power Sources 580 (2023) 233437Journal of Power Sources 580 (2023) 233437
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p2:body_region:0p2:top_margin:column_1_of_2:white[255, 255, 255]
white		False[37.59, 37.0, 463.07, 5.85]T. Huang et al.T. Huang et al.
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white		False[37.59, 55.48, 253.45, 289.75]O2/Li cell from 81% to 26% after 200 cycles [16]. Lan et al. reported [17] that the electrode capacity retention in an electrolyte without any additive was 40%, which is much lower than the 72% observed in an electrolyt…O2/Li cell from 81% to 26% after 200 cycles [16]. Lan et al. reported [17] that the electrode capacity retention in an electrolyte without any additive was 40%, which is much lower than the 72% observed in an electrolyt…
229textbodyTruebodybody
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white		False[37.59, 348.41, 253.44, 90.99]Some studies have reported that the improvement of the electrochemical behavior of NCM622-based cells and LNMO-based cells are a result of silicon-based electrolyte additives [26 -28]. In this paper, 1, 3-divinyltetrame…Some studies have reported that the improvement of the electrochemical behavior of NCM622-based cells and LNMO-based cells are a result of silicon-based electrolyte additives [26 -28]. In this paper, 1, 3-divinyltetrame…
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white		False[37.59, 453.13, 58.23, 7.31]2. Experiment2. Experiment
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white		False[37.59, 474.05, 158.65, 7.31]2.1. Preparation of electrolytes and electrodes2.1. Preparation of electrolytes and electrodes
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white		False[37.59, 494.97, 253.43, 101.48]The LRM cathode was composed of 80 wt% LRM (LRM300, Ningbo Li-rich Battery Material Technology Co., Ltd., China), 10 wt% polyvinylidene fluoride (PVDF) binder, and 10 wt% acetylene black in N -methyl-2-pyrrolidone. The …The LRM cathode was composed of 80 wt% LRM (LRM300, Ningbo Li-rich Battery Material Technology Co., Ltd., China), 10 wt% polyvinylidene fluoride (PVDF) binder, and 10 wt% acetylene black in N -methyl-2-pyrrolidone. The …
233textbodyTruebodybody
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white		False[37.59, 599.57, 253.44, 38.72]A total of 1000 ppm of hydrofluoric acid (HF) was then added into the BE and BE + 2 vol%DTMS electrolytes to prepare HF-containing electrolytes using a 40 wt% HF aqueous solution [25]. All electrolytes were prepared in …A total of 1000 ppm of hydrofluoric acid (HF) was then added into the BE and BE + 2 vol%DTMS electrolytes to prepare HF-containing electrolytes using a 40 wt% HF aqueous solution [25]. All electrolytes were prepared in …
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white		False[37.59, 652.4, 96.4, 7.31]2.2. Electrochemical testing2.2. Electrochemical testing
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white		False[37.59, 673.32, 253.45, 70.07]The charge -discharge performance of the cells was evaluated using a computer-controlled test system (CT2001A, China). The LRM/Li cells were pre-cycled in the following schedule: 0.1C (1C = 300 mA g 1 ) for three cycles…The charge -discharge performance of the cells was evaluated using a computer-controlled test system (CT2001A, China). The LRM/Li cells were pre-cycled in the following schedule: 0.1C (1C = 300 mA g 1 ) for three cycles…
236captioncaptionFalselowdocling_captiondocling_caption
p2:body_region:1p2:top_margin:column_2_of_2:white[255, 255, 255]
white		False[366.12, 56.3, 79.26, 16.16]Table 1 Calculated Eox (V vs. Li +Table 1 Calculated Eox (V vs. Li +
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white		False[366.12, 65.88, 134.12, 16.16]/Li) of EC, DMC, EMC, and DTMS./Li) of EC, DMC, EMC, and DTMS.
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white		False[306.59, 153.91, 253.39, 28.23]impedance spectroscopy (EIS) was employed in the frequency range of 10 5 to 0.1 Hz with an amplitude of 5 mV, using a frequency response analyzer (VSP, Bio-logic).impedance spectroscopy (EIS) was employed in the frequency range of 10 5 to 0.1 Hz with an amplitude of 5 mV, using a frequency response analyzer (VSP, Bio-logic).
239section_headerbody_headingFalselowbody_headingbody_heading
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white		False[306.6, 197.1, 104.56, 7.31]2.3. Physical characterization2.3. Physical characterization
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p2:body_region:1p2:body_zone:column_2_of_2:white[255, 255, 255]
white		False[306.6, 218.02, 253.4, 80.56]To understand the influence of DTMS on the cycling performance of LRM/Li cells, scanning electron microscopy (SEM; S-4800, Hitachi), transmission electron microscopy (TEM; JEM-2010, JELO), XRD analysis (XRD; Bruker D8 A…To understand the influence of DTMS on the cycling performance of LRM/Li cells, scanning electron microscopy (SEM; S-4800, Hitachi), transmission electron microscopy (TEM; JEM-2010, JELO), XRD analysis (XRD; Bruker D8 A…
241section_headerbody_headingFalselowbody_headingbody_heading
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white		False[306.6, 313.49, 61.58, 7.31]2.4. Calculations2.4. Calculations
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p2:body_region:1p2:body_zone:column_2_of_2:white[255, 255, 255]
white		False[306.6, 334.41, 253.4, 38.72]The Gaussian 09 software package was used for theoretical calculations. The equilibrium structures were determined using the B3LYP/6311G(d,p) level [28]. The oxidation potential (Eox) was obtained as follows[28]:The Gaussian 09 software package was used for theoretical calculations. The equilibrium structures were determined using the B3LYP/6311G(d,p) level [28]. The oxidation potential (Eox) was obtained as follows[28]:
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p2:body_region:1p2:body_zone:column_2_of_2:white[255, 255, 255]
white		False[306.6, 380.54, 236.56, 9.34]Eox (Li + /Li) = [G(M + ) - G(M)]/F - 1.4 VEox (Li + /Li) = [G(M + ) - G(M)]/F - 1.4 V
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white		False[306.6, 420.93, 100.96, 7.31]3. Results and discussion3. Results and discussion
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white		False[306.6, 441.84, 114.37, 7.31]3.1. Oxidative stability of DTMS3.1. Oxidative stability of DTMS
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white		False[306.6, 460.54, 253.42, 166.47]The as-calculated oxidation potential and Li + binding affinity (Eb) are often used to forecast the oxidation tendency of an additive on the cathode surface [29,30]. The film-forming electrolyte additives have a lower o…The as-calculated oxidation potential and Li + binding affinity (Eb) are often used to forecast the oxidation tendency of an additive on the cathode surface [29,30]. The film-forming electrolyte additives have a lower o…
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white		False[306.6, 641.91, 167.94, 7.31]3.2. Impact of DTMS at electrochemical perform3.2. Impact of DTMS at electrochemical perform
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white		False[306.6, 662.83, 253.42, 80.56]Supplementary Material. 2 shows the charge -discharge curve performance of LRM/Li cells with and without 2 vol% DTMS electrolytes during the first pre-cycle process. It can be found that the cells in the 2 vol% DTMS-con…Supplementary Material. 2 shows the charge -discharge curve performance of LRM/Li cells with and without 2 vol% DTMS electrolytes during the first pre-cycle process. It can be found that the cells in the 2 vol% DTMS-con…
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white		False[433.38, 33.65, 124.91, 10.42]Journal of Power Sources 580 (2023) 233437Journal of Power Sources 580 (2023) 233437
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white		False[37.59, 36.99, 463.07, 5.85]T. Huang et al.T. Huang et al.
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white		False[179.09, 187.18, 241.32, 8.3]Fig. 1. Optimized structures and Eb values of solvents-Li + and DTMS-Li + .Fig. 1. Optimized structures and Eb values of solvents-Li + and DTMS-Li + .
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white		False[38.95, 472.99, 521.55, 6.58]Fig. 2. (a) Cycling performance and (b) rate capability of LRM/Li cell. (c) (d) 1st, 20th, 50th, and 100th charge -discharge curves of LRM/Li cell during cycling.Fig. 2. (a) Cycling performance and (b) rate capability of LRM/Li cell. (c) (d) 1st, 20th, 50th, and 100th charge -discharge curves of LRM/Li cell during cycling.
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white		False[37.59, 494.91, 253.44, 174.67]different electrolytes. The LRM/Li cells with 2 vol% DTMS showed great cycling stability. The discharge capacity of LRM/Li cells in the BE electrolyte decreased from 262.3 to 57.7 mAh g 1 after 100 cycles (57.2% capacit…different electrolytes. The LRM/Li cells with 2 vol% DTMS showed great cycling stability. The discharge capacity of LRM/Li cells in the BE electrolyte decreased from 262.3 to 57.7 mAh g 1 after 100 cycles (57.2% capacit…
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white		False[37.59, 672.7, 253.44, 70.07]EIS was carried out on LRM/Li cells after pre-cycling and cycling with the BE and 2 vol% DTMS-containing electrolytes, as shown in Fig. 3. The results can be divided into two parts: a depressed semicircle followed by a …EIS was carried out on LRM/Li cells after pre-cycling and cycling with the BE and 2 vol% DTMS-containing electrolytes, as shown in Fig. 3. The results can be divided into two parts: a depressed semicircle followed by a …
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white		False[306.59, 494.91, 253.4, 38.66]in Rf and Rct compared with the cells with the DTMS-containing electrolyte. The electrolyte decomposition substantially deteriorates the properties of the interface between the LRM and BE electrolyte and thereby reduces…in Rf and Rct compared with the cells with the DTMS-containing electrolyte. The electrolyte decomposition substantially deteriorates the properties of the interface between the LRM and BE electrolyte and thereby reduces…
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white		False[306.59, 536.75, 253.43, 122.34]The surface morphologies of the cathodes in the BE and DTMScontaining electrolytes were analyzed after cycling by SEM and TEM (Fig. 4). As shown in Fig. 4a, the cathode surface in the BE electrolyte was covered with a t…The surface morphologies of the cathodes in the BE and DTMScontaining electrolytes were analyzed after cycling by SEM and TEM (Fig. 4). As shown in Fig. 4a, the cathode surface in the BE electrolyte was covered with a t…
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white		False[306.59, 662.27, 253.42, 80.5]Fig. 5a depicts the obtained XPS of LRM cells with BE and DMSEcontaining electrolytes after cycling. The C 1s peaks at 290.3 and 285.4 eV correspond to PVDF [19,25], and the peak at 284.6 eV is assigned to acetylene bla…Fig. 5a depicts the obtained XPS of LRM cells with BE and DMSEcontaining electrolytes after cycling. The C 1s peaks at 290.3 and 285.4 eV correspond to PVDF [19,25], and the peak at 284.6 eV is assigned to acetylene bla…
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white		False[433.38, 33.65, 124.91, 10.42]Journal of Power Sources 580 (2023) 233437Journal of Power Sources 580 (2023) 233437
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white		False[37.59, 36.99, 463.07, 5.85]T. Huang et al.T. Huang et al.
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white		False[86.63, 307.39, 426.25, 6.58]Fig. 3. EIS results of LRM/Li cell in BE and 2 vol% DTMS electrolyte after (a) pre-cycling and (b) cycling. (c) Values of Rf and Rct.Fig. 3. EIS results of LRM/Li cell in BE and 2 vol% DTMS electrolyte after (a) pre-cycling and (b) cycling. (c) Values of Rf and Rct.
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white		False[112.82, 587.51, 373.83, 6.58]Fig. 4. TEM and SEM images of LRM cathodes after cycling (a), (c) with BE and (b), (d) 2 vol% DTMS electrolyte.Fig. 4. TEM and SEM images of LRM cathodes after cycling (a), (c) with BE and (b), (d) 2 vol% DTMS electrolyte.
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white		False[37.59, 609.43, 253.44, 132.83](ROCO2Li, ROLi, and Li2CO3) at 286 and 288.8 eV were observed. The peak intensities for the electrolyte with DTMS were lower than those for the BE electrolyte. The same result can be observed in O 1s spectra. The peak i…(ROCO2Li, ROLi, and Li2CO3) at 286 and 288.8 eV were observed. The peak intensities for the electrolyte with DTMS were lower than those for the BE electrolyte. The same result can be observed in O 1s spectra. The peak i…
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white		False[306.59, 609.43, 253.42, 49.15]conclusion, the peak intensities for the electrolyte decomposition products on the cathode in the DTMS-containing electrolyte were weaker, confirming that the electrolyte decomposition could be inhibited by DTMS. The ex…conclusion, the peak intensities for the electrolyte decomposition products on the cathode in the DTMS-containing electrolyte were weaker, confirming that the electrolyte decomposition could be inhibited by DTMS. The ex…
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white		False[306.59, 661.76, 253.43, 80.5]The XRD results for the cathodes before and after cycling with the BE and 2% DTMS-containing electrolytes are shown in Fig. 5b: the XRD peak intensity of the cathode in the BE electrolyte reduces drastically after cycli…The XRD results for the cathodes before and after cycling with the BE and 2% DTMS-containing electrolytes are shown in Fig. 5b: the XRD peak intensity of the cathode in the BE electrolyte reduces drastically after cycli…
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white		False[433.38, 33.65, 124.91, 10.42]Journal of Power Sources 580 (2023) 233437Journal of Power Sources 580 (2023) 233437
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white		False[37.59, 36.99, 463.07, 5.85]T. Huang et al.T. Huang et al.
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white		False[37.59, 557.13, 522.17, 16.1]Fig. 5. (a)XPS spectra of LRM cathodes after cycling with BE and 2 vol% DTMS electrolytes. (b) XRD patterns of LRM cathodes and (c) dissolution of transition metal on Li electrode taken from cell after cycling.Fig. 5. (a)XPS spectra of LRM cathodes after cycling with BE and 2 vol% DTMS electrolytes. (b) XRD patterns of LRM cathodes and (c) dissolution of transition metal on Li electrode taken from cell after cycling.
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white		False[37.59, 588.57, 253.44, 80.56]cathode was well maintained in DTMS-containing electrolyte. This further confirms that the DTMS is beneficial for maintaining structure stability during cycling. As shown in Fig. 5c, the Mn, Ni, and Co contents were 0.2…cathode was well maintained in DTMS-containing electrolyte. This further confirms that the DTMS is beneficial for maintaining structure stability during cycling. As shown in Fig. 5c, the Mn, Ni, and Co contents were 0.2…
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white		False[37.59, 683.75, 124.69, 7.31]3.3. Interaction of DTMS with HF/F3.3. Interaction of DTMS with HF/F
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white		False[37.59, 704.67, 253.41, 38.72]To study the interaction of DTMS with HF/F , the cycling performance of the coin cell in the BE + 1000 ppm HF electrolyte and the 2 vol % DTMS-containing + 1000 ppm HF electrolyte was analyzed (Fig. 6a). A significant c…To study the interaction of DTMS with HF/F , the cycling performance of the coin cell in the BE + 1000 ppm HF electrolyte and the 2 vol % DTMS-containing + 1000 ppm HF electrolyte was analyzed (Fig. 6a). A significant c…
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white		False[306.59, 586.33, 253.42, 93.22]BE + 1000 ppm HF electrolyte: from 246.4 to 60.3 mAh g 1 . However, the discharge capacity in the 2 vol% DTMS-containing + 1000 ppm HF electrolyte changed from 240.3 to 190.6 mAh g 1 . DTMS can effectively suppress the …BE + 1000 ppm HF electrolyte: from 246.4 to 60.3 mAh g 1 . However, the discharge capacity in the 2 vol% DTMS-containing + 1000 ppm HF electrolyte changed from 240.3 to 190.6 mAh g 1 . DTMS can effectively suppress the …
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white		False[306.6, 682.73, 253.42, 59.58]NMR spectra are used for analyzing the composition changes after storage for 24 h in the electrolyte upon the addition of HF [32] (Fig. 7). A pair of peaks at 75 ppm can be found for all electrolytes, which are assigned…NMR spectra are used for analyzing the composition changes after storage for 24 h in the electrolyte upon the addition of HF [32] (Fig. 7). A pair of peaks at 75 ppm can be found for all electrolytes, which are assigned…
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white		False[37.59, 36.99, 463.07, 5.85]T. Huang et al.T. Huang et al.
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white		False[37.59, 243.16, 522.15, 16.16]Fig. 6. (a) Discharge profiles of cell during cycling with BE + 1000 ppm HF and 2 vol% DTMS-containing + 1000 ppm HF; F 1s XPS spectra of LRM cathodes after cycling with (b) BE + 1000 ppm HF and (c) 2 vol% DTMS-containi…Fig. 6. (a) Discharge profiles of cell during cycling with BE + 1000 ppm HF and 2 vol% DTMS-containing + 1000 ppm HF; F 1s XPS spectra of LRM cathodes after cycling with (b) BE + 1000 ppm HF and (c) 2 vol% DTMS-containi…
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white		False[92.13, 673.38, 415.22, 8.36]Fig. 7. 19 F NMR spectra of BE and DTMS-containing electrolytes before (a and b) and after (c and d) 1000 ppm HF was added.Fig. 7. 19 F NMR spectra of BE and DTMS-containing electrolytes before (a and b) and after (c and d) 1000 ppm HF was added.
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white		False[37.59, 697.02, 253.41, 38.72]assigned to PO2F2 formed from the partial hydrolysis of LiPF6 [25], and the peak at 190 ppm corresponds to HF. However, the HF peak intensity for the 2 vol% DTMS-containing + 1000 ppm HF electrolyte is lower than that f…assigned to PO2F2 formed from the partial hydrolysis of LiPF6 [25], and the peak at 190 ppm corresponds to HF. However, the HF peak intensity for the 2 vol% DTMS-containing + 1000 ppm HF electrolyte is lower than that f…
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white		False[306.59, 697.02, 253.42, 38.72]new small peak at 162 ppm corresponding to the BE + 2 vol%DTMS containing 1000 ppm of the HF electrolyte is shown in Fig. 7d, which can be attributed to the reaction between DTMS and HF/F .Supplementary Material 3 prese…new small peak at 162 ppm corresponding to the BE + 2 vol%DTMS containing 1000 ppm of the HF electrolyte is shown in Fig. 7d, which can be attributed to the reaction between DTMS and HF/F .Supplementary Material 3 prese…
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white		False[433.38, 33.65, 124.91, 10.42]Journal of Power Sources 580 (2023) 233437Journal of Power Sources 580 (2023) 233437
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white		False[37.59, 36.99, 463.07, 5.85]T. Huang et al.T. Huang et al.
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white		False[37.59, 189.96, 253.44, 49.15]electrolytes collected from the LRM/Li cells after evaluating their cycling performance. In them, the peak at 162 ppm corresponding to the products of the reaction of DTMS with HF/F disappears. Combined with the Si 2p X…electrolytes collected from the LRM/Li cells after evaluating their cycling performance. In them, the peak at 162 ppm corresponding to the products of the reaction of DTMS with HF/F disappears. Combined with the Si 2p X…
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white		False[37.59, 242.23, 253.43, 28.23]The possible DTMS reaction on the interface of the cathode is shown in Fig. 8. We hypothesize that the Si -O bond can react with HF, Lewis acids, and EC [28,33].The possible DTMS reaction on the interface of the cathode is shown in Fig. 8. We hypothesize that the Si -O bond can react with HF, Lewis acids, and EC [28,33].
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white		False[37.59, 284.81, 60.27, 7.31]4. Conclusions4. Conclusions
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white		False[37.59, 305.72, 253.42, 80.56]In conclusion, the cycling performance of the LRM cathode can be greatly improved by adding DTMS. The capacity loss decreased from 57.2% to 25% at 0.5C after 100 cycles. Experimental results show that DTMS is preferenti…In conclusion, the cycling performance of the LRM cathode can be greatly improved by adding DTMS. The capacity loss decreased from 57.2% to 25% at 0.5C after 100 cycles. Experimental results show that DTMS is preferenti…
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white		False[37.59, 400.63, 164.27, 7.31]CRediT authorship contribution statementCRediT authorship contribution statement
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white		False[37.59, 421.55, 253.42, 38.66]Tao Huang: Investigation, Methodology, Writing -original draft. Xiangzhen Zheng: Investigation. Chunfeng Yan: Validation. Ying Pan: Software. Maoxiang Wu: Conceptualization, Writing -review & editing.Tao Huang: Investigation, Methodology, Writing -original draft. Xiangzhen Zheng: Investigation. Chunfeng Yan: Validation. Ying Pan: Software. Maoxiang Wu: Conceptualization, Writing -review & editing.
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white		False[37.59, 476.94, 130.92, 7.31]Declaration of competing interestDeclaration of competing interest
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white		False[49.55, 497.86, 187.21, 7.31]The authors declare no competing financial interest.The authors declare no competing financial interest.
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white		False[37.59, 518.78, 65.84, 7.31]Data availabilityData availability
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white		False[49.55, 539.7, 142.71, 7.31]Data will be made available on request.Data will be made available on request.
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white		False[37.59, 561.35, 72.63, 7.31]AcknowledgementAcknowledgement
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white		False[37.59, 582.27, 253.44, 28.23]This work was supported by the Science and Technology Planning Project of Fujian Province (Grant No. 2022H0038, 2020H0037, 2022T3001).This work was supported by the Science and Technology Planning Project of Fujian Province (Grant No. 2022H0038, 2020H0037, 2022T3001).
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white		False[37.59, 624.85, 130.96, 7.31]Appendix A. Supplementary dataAppendix A. Supplementary data
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white		False[37.59, 645.77, 253.41, 17.74]Supplementary data to this article can be found online at https://doi. org/10.1016/j.jpowsour.2023.233437.Supplementary data to this article can be found online at org/10.1016/j.jpowsour.2023.233437.
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white		False[37.59, 677.86, 43.55, 7.31]ReferencesReferences
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white		False[40.99, 721.22, 230.83, 21.78]Q. Zhong, A. Bonakclarpour, M. Zhang, Y. Gao, J.R. Da, Synthesis and electrochemistry of LiNiMn2-xO4, J. Electrochem. Soc. 144 (1997) 205 -213, https://doi.org/10.1021/ja3091438.Q. Zhong, A. Bonakclarpour, M. Zhang, Y. Gao, J.R. Da, Synthesis and electrochemistry of LiNiMn2-xO4, J. Electrochem. Soc. 144 (1997) 205 -213,
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white		False[236.98, 168.04, 125.53, 6.58]Fig. 8. Possible mechanism of DTMS.Fig. 8. Possible mechanism of DTMS.
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