Docling layout block audit

original.pdf docling.json layout_blocks.json layout_blocks.tsv layout_blocks.jsonl excluded_blocks.html excluded_blocks.tsv final_body_blocks.tsv visual_assets.tsv visual_assets.json

Summary

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Diff Summary

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Truncation

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Page Overlays

Green = final body chunks. Orange/purple asset boxes = actual figure/table assets used by ingestion. Cyan dashed text boxes = text blocks consumed by those assets as caption continuations. Red STOP = truncation trigger. Red boxes = blocks after truncation.

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Visual Assets

这里对齐真实图表资产提取链路。caption_source=embedded_table_cell 表示表注来自 Docling table cell，不会出现在 text block 审计差集里；caption_continuation_used_by_asset 表示某个 text block 已被图表 caption 吸收，不应按普通 metadata 解读。

#	type	label	page	caption source	confidence	bbox	caption
1	figure	Fig. 1	3	direct_caption_ref	0.82	[146.03, 61.95, 249.17, 173.37]	Fig. 1. XRD patterns of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2.
2	figure	Fig. 2	4	direct_caption_ref	0.82	[57.05, 61.21, 433.75, 492.05]	Fig. 2. SEM images of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2. x = (a) 1.0, (b) 0.9, (c) 0.7, (d) 0.5, (e) 0.3 and (f) 0.1.
3	figure	Fig. 3	5	direct_caption_ref	0.82	[152.06, 60.67, 235.65, 365.55]	Fig. 3. First charge/discharge curves of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2.
4	figure	Fig. 4	6	direct_caption_ref	0.82	[153.24, 61.51, 242.42, 376.61]	Fig. 4. (a) Electrochemical properties of mixed compounds ofLi2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2: ( & ) charge capacity and ( * ) discharge capacity. (b) Electrochemical properties of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2: ( & ) capacity retention and ( * ) initial capacity loss.
5	figure	Fig. 5	7	nearby_text_caption	0.82	[149.33, 61.61, 239.86, 178.42]	Fig. 5. Cycle performance of the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound after fifty cycles.
6	figure	Fig. 6	7	direct_caption_ref	0.82	[150.56, 282.17, 238.63, 173.87]	Fig. 6. Cyclic voltammograms of the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound. Scan rate is 0.1 mV/s. The voltage range is 2.0 -4.8 V.
7	figure	Fig. 7	7	direct_caption_ref	0.82	[149.22, 492.89, 240.55, 174.41]	Fig. 7. Voltage profile of the cell during two cycles. Representative scans of XANES measurements are indicated.
8	figure	Fig. 8	8	direct_caption_ref	0.82	[151.76, 60.75, 244.92, 557.46]	Fig. 8. (a) Mn K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during the first charge process. (b) Co K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during the first charge process. (c) Ni K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during the first charge process.
9	figure	Fig. 9	9	direct_caption_ref	0.82	[149.93, 61.61, 240.7, 543.61]	Fig. 9. (a) Mn K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during 2 cycles. (b) Co K-edge XANES spectra for the Li[Li1/ 6Mn1/2Ni1/6Co1/6]O2 compound during 2 cycles. (c) Ni K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during 2 cycles.
10	table	Docling Table 10	2	missing_caption	0.55	[40.11, 83.95, 467.97, 62.92]

Blocks

page	order	label	role	included	risk	reason	parser reason	trunc	region	bg	frame	bbox	raw text	cleaned text
1	0	text	body_heading	False	low	before_body_started	before_body_started		p1:front_matter:left_crossing:white	[255, 255, 255] white	False	[171.89, 99.61, 163.34, 6.95]	Materials Research Bulletin 43 (2008) 3543 -3552	Materials Research Bulletin 43 (2008) 3543 -3552
1	1	text	metadata	False	low	document_web_address	document_web_address		p1:front_matter:right:white	[255, 255, 255] white	False	[391.75, 109.07, 111.36, 6.95]	www.elsevier.com/locate/matresbu
1	2	section_header	body_heading	False	low	first_page_front_matter_heading	first_page_front_matter_heading		p1:front_matter:full:white	[255, 255, 255] white	False	[50.12, 143.16, 439.71, 54.63]	Electrochemical behaviors of Li[Li(1 x )/3Mn(2 x )/3Ni x /3Co x /3]O2 cathode series (0 < x < 1) synthesized by sucrose combustion process for high capacity lithium ion batteries	Electrochemical behaviors of Li[Li(1 x )/3Mn(2 x )/3Ni x /3Co x /3]O2 cathode series (0 < x < 1) synthesized by sucrose combustion process for high capacity lithium ion batteries
1	3	text	affiliation	False	low	first_page_author_or_affiliation	first_page_author_or_affiliation		p1:front_matter:left_crossing:white	[255, 255, 255] white	False	[91.16, 207.17, 357.6, 14.17]	Gu-Yeon Kim a, * , Seung-Beob Yi b , Yong Joon Park c , Ho-Gi Kim a	Gu-Yeon Kim a, * , Seung-Beob Yi b , Yong Joon Park c , Ho-Gi Kim a
1	4	text	affiliation	False	low	first_page_author_or_affiliation	first_page_author_or_affiliation		p1:front_matter:full:white	[255, 255, 255] white	False	[59.19, 227.9, 418.91, 18.57]	a Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, 373-1 Guseong-dong, Yuseong-gu, Daejeon 305-701, Republic of Korea	a Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, 373-1 Guseong-dong, Yuseong-gu, Daejeon 305-701, Republic of Korea
1	5	text	affiliation	False	low	first_page_author_or_affiliation	first_page_author_or_affiliation		p1:front_matter:left_crossing:white	[255, 255, 255] white	False	[115.03, 247.86, 307.31, 8.59]	b Energy Business Division Development Team, SAMSUNG SDI, 508 Sungsung-dong, Chenan,	b Energy Business Division Development Team, SAMSUNG SDI, 508 Sungsung-dong, Chenan,
1	6	text	affiliation	False	low	first_page_author_or_affiliation	first_page_author_or_affiliation		p1:front_matter:left_crossing:white	[255, 255, 255] white	False	[189.24, 259.66, 161.46, 6.77]	Chungcheongnam-do 330-300, Republic of Korea	Chungcheongnam-do 330-300, Republic of Korea
1	7	text	affiliation	False	low	first_page_author_or_affiliation	first_page_author_or_affiliation		p1:front_matter:left_crossing:white	[255, 255, 255] white	False	[95.64, 267.76, 346.04, 8.65]	c Division of Advanced Industrial Engineering, Kyonggi University, 94-6 Yiui-dong, Yeongtong-gu, Suwon,	c Division of Advanced Industrial Engineering, Kyonggi University, 94-6 Yiui-dong, Yeongtong-gu, Suwon,
1	8	text	affiliation	False	low	first_page_author_or_affiliation	first_page_author_or_affiliation		p1:front_matter:left_crossing:white	[255, 255, 255] white	False	[219.35, 279.56, 101.26, 6.77]	Kyonggi-do, Republic of Korea	Kyonggi-do, Republic of Korea
1	9	text	reference	False	low	first_page_metadata	first_page_metadata		p1:front_matter:left_crossing:white	[255, 255, 255] white	False	[105.45, 292.47, 329.04, 16.93]	Received 9 November 2007; received in revised form 21 December 2007; accepted 17 January 2008 Available online 29 January 2008	Received 9 November 2007; received in revised form 21 December 2007; accepted 17 January 2008 Available online 29 January 2008
1	10	section_header	abstract_heading	False	low	abstract_heading	abstract_heading		p1:front_matter:left:white	[255, 255, 255] white	False	[36.85, 329.56, 33.31, 7.9]	Abstract	Abstract
1	11	text	reference	False	low	first_page_summary	first_page_summary		p1:front_matter:full:white	[255, 255, 255] white	False	[36.85, 346.64, 466.27, 73.59]	A mixed cathode material between Li2MnO3 and Li[Mn1/3Ni1/3Co1/3]O2 for high capacity lithium secondary batteries was introduced in this study. It was prepared using the sucrose combustion process because this is a simpl…	A mixed cathode material between Li2MnO3 and Li[Mn1/3Ni1/3Co1/3]O2 for high capacity lithium secondary batteries was introduced in this study. It was prepared using the sucrose combustion process because this is a simpl…
1	12	text	front_matter_heading	False	low	front_matter_heading	front_matter_heading		p1:front_matter:full:white	[255, 255, 255] white	False	[36.85, 431.43, 408.25, 6.95]	Keywords: A. Inorganic compounds; B. Chemical synthesis; C. XAFS (EXAFS and XANES); D. Electrochemical properties	Keywords: A. Inorganic compounds; B. Chemical synthesis; C. XAFS (EXAFS and XANES); D. Electrochemical properties
1	13	section_header	body_heading	False	low	body_heading	body_heading		p1:body_zone:left:white	[255, 255, 255] white	False	[36.85, 473.51, 66.61, 8.78]	1. Introduction	1. Introduction
1	14	text	body	True		body	body		p1:body_zone:full:white	[255, 255, 255] white	False	[36.85, 497.57, 466.25, 68.45]	The Li-ion secondary battery industry has rapidly developed, as there have been many advances in technology regarding mobile electronic devices such as mobile phones, laptop computers and HEVs. As a cathode for lithium …	The Li-ion secondary battery industry has rapidly developed, as there have been many advances in technology regarding mobile electronic devices such as mobile phones, laptop computers and HEVs. As a cathode for lithium …
1	15	text	body	True		body	body		p1:body_zone:full:white	[255, 255, 255] white	False	[36.85, 569.29, 466.24, 33.56]	Thus, numerous investigations have been made into the realization of high-capacity batteries using solid solution compounds between two cathodes. Hong et al. reported a solid solution of Li[Ni0.20Li0.20Mn0.60]O2 and Li[…	Thus, numerous investigations have been made into the realization of high-capacity batteries using solid solution compounds between two cathodes. Hong et al. reported a solid solution of Li[Ni0.20Li0.20Mn0.60]O2 and Li[…
1	16	footnote	footnote	False	low	first_page_metadata	first_page_metadata		p1:body_zone:left:white	[255, 255, 255] white	False	[41.39, 633.6, 172.87, 16.93]	* Corresponding author. Fax: +82 42 869 8650. E-mail address: antiserra@kaist.ac.kr (G.-Y. Kim).	* Corresponding author. Fax: +82 42 869 8650. E-mail address: antiserra@kaist.ac.kr (G.-Y. Kim).
1	17	page_footer	page_footer	False	low	first_page_metadata	first_page_metadata		p1:body_zone:left_crossing:white	[255, 255, 255] white	False	[36.85, 665.33, 240.11, 17.06]	0025-5408/$ -see front matter # 2008 Elsevier Ltd. All rights reserved. doi:10.1016/j.materresbull.2008.01.011	0025-5408/$ -see front matter # 2008 Elsevier Ltd. All rights reserved. doi:10.1016/j.materresbull.2008.01.011
2	18	page_header	page_header	False	low	docling_page_header	docling_page_header		p2:top_margin:left:white	[255, 255, 255] white	False	[41.16, 45.41, 15.94, 6.95]	3544	3544
2	19	page_header	page_header	False	low	docling_page_header	docling_page_header		p2:top_margin:right_crossing:white	[255, 255, 255] white	False	[164.3, 45.41, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
2	20	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p2:front_matter:left_crossing:white	[255, 255, 255] white	False	[41.16, 63.78, 274.88, 16.93]	Table 1 c/a values, lattice parameters and theoretical capacity of layered oxide compositions	Table 1 c/a values, lattice parameters and theoretical capacity of layered oxide compositions
2	21	text	body	True		body	body		p2:front_matter:full:white	[255, 255, 255] white	False	[41.16, 172.04, 466.18, 20.65]	Moreover, a Li[Li1/3 2 x /3Mn2/3 x /3Ni x ]O2 solid solution between Li2MnO3 and Li[Mn x Ni1 x ]O2 is known to be a high capacity cathode material [4,5,6,7].	Moreover, a Li[Li1/3 2 x /3Mn2/3 x /3Ni x ]O2 solid solution between Li2MnO3 and Li[Mn x Ni1 x ]O2 is known to be a high capacity cathode material [4,5,6,7].
2	22	text	body	True		body	body		p2:front_matter:full:white	[255, 255, 255] white	False	[41.16, 195.97, 466.24, 80.41]	Recently, investigations of solid solutions between Li2MnO3 and other cathode materials have been reported [8]. There are two advantages of a solid solution between Li2MnO3 and other layered cathode materials. First, th…	Recently, investigations of solid solutions between Li2MnO3 and other cathode materials have been reported [8]. There are two advantages of a solid solution between Li2MnO3 and other layered cathode materials. First, th…
2	23	text	body	True		body	body		p2:front_matter:full:white	[255, 255, 255] white	False	[41.16, 279.65, 466.24, 68.44]	In the present work, mixed compounds of Li[Li1 x /3Mn2 x /3Ni x /3Co x /3]O2, as composed of Li2MnO3 and Li[Ni1/ 3Co1/3Mn1/3]O2 were synthesized via a SCP (Sucrose Combustion Process) method. Compared with other syn…	In the present work, mixed compounds of Li[Li1 x /3Mn2 x /3Ni x /3Co x /3]O2, as composed of Li2MnO3 and Li[Ni1/ 3Co1/3Mn1/3]O2 were synthesized via a SCP (Sucrose Combustion Process) method. Compared with other syn…
2	24	section_header	body_heading	False	low	body_heading	body_heading		p2:body_zone:left:white	[255, 255, 255] white	False	[41.16, 363.19, 70.77, 8.78]	2. Experimental	2. Experimental
2	25	text	body	True		body	body		p2:body_zone:full:white	[255, 255, 255] white	False	[41.16, 387.25, 466.25, 235.86]	Mixed compounds Li[Li(1 x )/3Mn(2 x )/3Ni x /3Co x /3]O2 composed of Li[Ni1/3Co1/3Mn1/3]O2 and Li2MnO3 were prepared by a SCP method from LiNO3, Mn(NO3)2 6H2O, Ni(NO3)2 6H2O and Co(NO3)2 6H2O as precursors. In…	Mixed compounds Li[Li(1 x )/3Mn(2 x )/3Ni x /3Co x /3]O2 composed of Li[Ni1/3Co1/3Mn1/3]O2 and Li2MnO3 were prepared by a SCP method from LiNO3, Mn(NO3)2 6H2O, Ni(NO3)2 6H2O and Co(NO3)2 6H2O as precursors. In…
2	26	section_header	body_heading	False	low	body_heading	body_heading		p2:body_zone:left:white	[255, 255, 255] white	False	[41.16, 638.15, 109.24, 8.78]	3. Results and discussion	3. Results and discussion
2	27	text	body	True		body	body		p2:bottom_margin:full:white	[255, 255, 255] white	False	[41.16, 662.21, 466.19, 21.6]	Fig. 1 shows X-ray diffraction patterns of the Li[Li(1 x )/3Mn(2 x )/3Ni x /3Co x /3]O2 cathode materials. The XRD data is indexed with that of layered LiCoO2 ( a -NaFeO2 type, space group R-3m, hexagonal). It has b…	Fig. 1 shows X-ray diffraction patterns of the Li[Li(1 x )/3Mn(2 x )/3Ni x /3Co x /3]O2 cathode materials. The XRD data is indexed with that of layered LiCoO2 ( a -NaFeO2 type, space group R-3m, hexagonal). It has b…
3	28	page_header	page_header	False	low	docling_page_header	docling_page_header		p3:top_margin:left_crossing:white	[255, 255, 255] white	False	[159.99, 45.41, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
3	29	page_header	page_header	False	low	docling_page_header	docling_page_header		p3:top_margin:right:white	[255, 255, 255] white	False	[487.22, 45.41, 15.94, 6.95]	3545	3545
3	30	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p3:page_body:left_crossing:white	[255, 255, 255] white	False	[133.11, 243.89, 273.72, 7.7]	Fig. 1. XRD patterns of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2.	Fig. 1. XRD patterns of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2.
3	31	text	body	True		body	body		p3:page_body:full:white	[255, 255, 255] white	False	[36.85, 267.69, 466.24, 45.52]	layered structures showed a good splitting of the peaks assigned to (108, 110) with c/a values higher than 4.899 [10]. The clearly split (108, 110) pairs and the c/a ratio (when higher than 4.899) in all compositions of…	layered structures showed a good splitting of the peaks assigned to (108, 110) with c/a values higher than 4.899 [10]. The clearly split (108, 110) pairs and the c/a ratio (when higher than 4.899) in all compositions of…
3	32	text	body	True		body	body		p3:page_body:full:white	[255, 255, 255] white	False	[36.85, 315.04, 466.26, 68.94]	The XRD data at compositions of x = 0.1 and x = 0.3 show superlattice peaks in the range of 21 -23 8 which cannot be indexed to R-3m symmetry. These superlattice peaks have been considered to reflect the degree of catio…	The XRD data at compositions of x = 0.1 and x = 0.3 show superlattice peaks in the range of 21 -23 8 which cannot be indexed to R-3m symmetry. These superlattice peaks have been considered to reflect the degree of catio…
3	33	text	body	True		body	body		p3:page_body:full:white	[255, 255, 255] white	False	[36.85, 387.25, 466.25, 80.41]	SEM images of Li[Li(1 x )/3Mn(2 x )/3Ni x /3Co x /3]O2 are shown in Fig. 2. The particle sizes measured via Malvern Mastersize S were 1.24, 1.17, 0.84, 1.44, 1.88 and 3.04 m mat x = 0.1, 0.3, 0.5, 0.7, 0.9 and 1.0, …	SEM images of Li[Li(1 x )/3Mn(2 x )/3Ni x /3Co x /3]O2 are shown in Fig. 2. The particle sizes measured via Malvern Mastersize S were 1.24, 1.17, 0.84, 1.44, 1.88 and 3.04 m mat x = 0.1, 0.3, 0.5, 0.7, 0.9 and 1.0, …
3	34	text	body	True		body	body		p3:page_body:full:white	[255, 255, 255] white	False	[36.85, 470.93, 466.22, 44.58]	Fig. 3 shows the initial charge/discharge curves for all compositions during the first cycle. The measurement was carried out between 2.0 and 4.8 Vat a constant current density of 0.2 C rate. Two plateaus were observed …	Fig. 3 shows the initial charge/discharge curves for all compositions during the first cycle. The measurement was carried out between 2.0 and 4.8 Vat a constant current density of 0.2 C rate. Two plateaus were observed …
3	35	text	body	True		body	body		p3:bottom_margin:full:white	[255, 255, 255] white	False	[36.85, 518.78, 466.27, 165.03]	Fig. 4(a) shows the charge/discharge capacity. The sample at x = 0.1 shows a low discharge capacity of 12 mAh/g, as also reported by Gopukumar and coworkers [13], and the sample at x = 0.5 shows the highest discharge ca…	Fig. 4(a) shows the charge/discharge capacity. The sample at x = 0.1 shows a low discharge capacity of 12 mAh/g, as also reported by Gopukumar and coworkers [13], and the sample at x = 0.5 shows the highest discharge ca…
4	36	page_header	page_header	False	low	docling_page_header	docling_page_header		p4:top_margin:left:white	[255, 255, 255] white	False	[41.16, 45.41, 15.94, 6.95]	3546	3546
4	37	page_header	page_header	False	low	docling_page_header	docling_page_header		p4:top_margin:right_crossing:white	[255, 255, 255] white	False	[164.3, 45.41, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
4	38	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p4:page_body:full:white	[255, 255, 255] white	False	[48.59, 562.05, 451.38, 7.7]	Fig. 2. SEM images of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2. x = (a) 1.0, (b) 0.9, (c) 0.7, (d) 0.5, (e) 0.3 and (f) 0.1.	Fig. 2. SEM images of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2. x = (a) 1.0, (b) 0.9, (c) 0.7, (d) 0.5, (e) 0.3 and (f) 0.1.
4	39	text	body	True		body	body		p4:page_body:full:white	[255, 255, 255] white	False	[41.16, 602.46, 466.22, 44.52]	by itself, the Li2MnO3 inside a domain structure is active when the voltage is higher than 4.4 V. When charged, one Li2MnO3 loses one O 2 ion and two Li + ions in forms of Li2O at above 4.4 V and becomes MnO2. When di…	by itself, the Li2MnO3 inside a domain structure is active when the voltage is higher than 4.4 V. When charged, one Li2MnO3 loses one O 2 ion and two Li + ions in forms of Li2O at above 4.4 V and becomes MnO2. When di…
4	40	text	body	True		body	body		p4:page_body:full:white	[255, 255, 255] white	False	[41.16, 650.25, 466.2, 32.62]	Considering the results shown in Fig. 4(a) and (b), it was determined that the optimized composition is x = 0.5, as the compounds of x = 0.5 and Li[Li1/6Mn1/2Ni1/6Co1/6]O2 incorporate the advantages of both structural s…	Considering the results shown in Fig. 4(a) and (b), it was determined that the optimized composition is x = 0.5, as the compounds of x = 0.5 and Li[Li1/6Mn1/2Ni1/6Co1/6]O2 incorporate the advantages of both structural s…
5	41	page_header	page_header	False	low	docling_page_header	docling_page_header		p5:top_margin:left_crossing:white	[255, 255, 255] white	False	[159.99, 45.41, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
5	42	page_header	page_header	False	low	docling_page_header	docling_page_header		p5:top_margin:right:white	[255, 255, 255] white	False	[487.22, 45.41, 15.94, 6.95]	3547	3547
5	43	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p5:page_body:left_crossing:white	[255, 255, 255] white	False	[108.17, 434.43, 323.61, 7.75]	Fig. 3. First charge/discharge curves of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2.	Fig. 3. First charge/discharge curves of mixed compounds of Li2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2.
5	44	text	body	True		body	body		p5:page_body:full:white	[255, 255, 255] white	False	[36.85, 470.93, 466.29, 92.37]	Fig. 5 shows the cyclic performance levels for the cells with the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 cathode material after fifty cycles between 2.0 and 4.8 V at a 0.2 C rate. Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compounds showed very st…	Fig. 5 shows the cyclic performance levels for the cells with the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 cathode material after fifty cycles between 2.0 and 4.8 V at a 0.2 C rate. Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compounds showed very st…
5	45	text	body	True		body	body		p5:page_body:full:white	[255, 255, 255] white	False	[36.85, 566.57, 466.26, 116.29]	In order to observe these reactions during a charge/discharge process, Mn, Co and Ni K-edge XANES measurements were made of Li[Li1/6Mn1/2Ni1/6Co1/6]O2 as a function of the degree of charge. The cycling curve of Li[Li1/6…	In order to observe these reactions during a charge/discharge process, Mn, Co and Ni K-edge XANES measurements were made of Li[Li1/6Mn1/2Ni1/6Co1/6]O2 as a function of the degree of charge. The cycling curve of Li[Li1/6…
6	46	page_header	page_header	False	low	docling_page_header	docling_page_header		p6:top_margin:left:white	[255, 255, 255] white	False	[41.16, 45.41, 15.94, 6.95]	3548	3548
6	47	page_header	page_header	False	low	docling_page_header	docling_page_header		p6:top_margin:right_crossing:white	[255, 255, 255] white	False	[164.3, 45.41, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
6	48	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p6:page_body:full:white	[255, 255, 255] white	False	[41.16, 446.26, 466.28, 27.33]	Fig. 4. (a) Electrochemical properties of mixed compounds ofLi2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2: ( & ) charge capacity and ( * ) discharge capacity. (b) Electrochemical properties of mixed compounds of Li2MnO3 and Li[Ni1/…	Fig. 4. (a) Electrochemical properties of mixed compounds ofLi2MnO3 and Li[Ni1/3Co1/3Mn1/3]O2: ( & ) charge capacity and ( * ) discharge capacity. (b) Electrochemical properties of mixed compounds of Li2MnO3 and Li[Ni1/…
6	49	text	body	True		body	body		p6:page_body:full:white	[255, 255, 255] white	False	[41.16, 506.82, 466.22, 20.65]	compounds (scan 0) are tetravalent, trivalent and divalent state, respectively, which corresponds to results reported by other research groups [15,16,17,18].	compounds (scan 0) are tetravalent, trivalent and divalent state, respectively, which corresponds to results reported by other research groups [15,16,17,18].
6	50	text	body	True		body	body		p6:page_body:full:white	[255, 255, 255] white	False	[41.16, 530.68, 466.24, 152.18]	Fig. 8(a) -(c) shows the change of the valence state of Mn, Co and Ni ions, respectively, in the Li[Li1/6Mn1/2Ni1/ 6Co1/6]O2 during first charge measurement. It can be seen in Fig. 8(a) that the edge shape of the Mn ion…	Fig. 8(a) -(c) shows the change of the valence state of Mn, Co and Ni ions, respectively, in the Li[Li1/6Mn1/2Ni1/ 6Co1/6]O2 during first charge measurement. It can be seen in Fig. 8(a) that the edge shape of the Mn ion…
7	51	page_header	page_header	False	low	docling_page_header	docling_page_header		p7:top_margin:left_crossing:white	[255, 255, 255] white	False	[159.99, 45.41, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
7	52	page_header	page_header	False	low	docling_page_header	docling_page_header		p7:top_margin:right:white	[255, 255, 255] white	False	[487.22, 45.41, 15.94, 6.95]	3549	3549
7	53	caption	caption	False	low	docling_caption	docling_caption		p7:page_body:left_crossing:white	[255, 255, 255] white	False	[123.87, 248.31, 292.28, 7.75]	Fig. 5. Cycle performance of the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound after fifty cycles.	Fig. 5. Cycle performance of the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound after fifty cycles.
7	54	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p7:page_body:full:white	[255, 255, 255] white	False	[55.39, 464.42, 429.17, 7.7]	Fig. 6. Cyclic voltammograms of the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound. Scan rate is 0.1 mV/s. The voltage range is 2.0 -4.8 V.	Fig. 6. Cyclic voltammograms of the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound. Scan rate is 0.1 mV/s. The voltage range is 2.0 -4.8 V.
7	55	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p7:page_body:left_crossing:white	[255, 255, 255] white	False	[82.94, 675.32, 374.11, 6.95]	Fig. 7. Voltage profile of the cell during two cycles. Representative scans of XANES measurements are indicated.	Fig. 7. Voltage profile of the cell during two cycles. Representative scans of XANES measurements are indicated.
8	56	page_header	page_header	False	low	docling_page_header	docling_page_header		p8:top_margin:left:white	[255, 255, 255] white	False	[41.16, 45.41, 15.94, 6.95]	3550	3550
8	57	page_header	page_header	False	low	docling_page_header	docling_page_header		p8:top_margin:right_crossing:white	[255, 255, 255] white	False	[164.3, 45.41, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
8	58	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p8:page_body:full:white	[255, 255, 255] white	False	[41.16, 625.94, 466.25, 26.91]	Fig. 8. (a) Mn K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during the first charge process. (b) Co K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during the first charge process. (…	Fig. 8. (a) Mn K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during the first charge process. (b) Co K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during the first charge process. (…
9	59	page_header	page_header	False	low	docling_page_header	docling_page_header		p9:top_margin:left_crossing:white	[255, 255, 255] white	False	[159.99, 45.41, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
9	60	page_header	page_header	False	low	docling_page_header	docling_page_header		p9:top_margin:right:white	[255, 255, 255] white	False	[487.22, 45.41, 15.94, 6.95]	3551	3551
9	61	caption	caption	False	low	outside_body_flow_caption	outside_body_flow_caption		p9:page_body:full:white	[255, 255, 255] white	False	[36.85, 613.58, 466.26, 17.68]	Fig. 9. (a) Mn K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during 2 cycles. (b) Co K-edge XANES spectra for the Li[Li1/ 6Mn1/2Ni1/6Co1/6]O2 compound during 2 cycles. (c) Ni K-edge XANES spectra for …	Fig. 9. (a) Mn K-edge XANES spectra for the Li[Li1/6Mn1/2Ni1/6Co1/6]O2 compound during 2 cycles. (b) Co K-edge XANES spectra for the Li[Li1/ 6Mn1/2Ni1/6Co1/6]O2 compound during 2 cycles. (c) Ni K-edge XANES spectra for …
10	62	page_header	page_header	False	low	docling_page_header	docling_page_header		p10:top_margin:left:white	[255, 255, 255] white	False	[41.16, 45.4, 15.94, 6.95]	3552	3552
10	63	page_header	page_header	False	low	docling_page_header	docling_page_header		p10:top_margin:right_crossing:white	[255, 255, 255] white	False	[164.3, 45.4, 219.98, 6.95]	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552	G.-Y. Kim et al. / Materials Research Bulletin 43 (2008) 3543 -3552
10	64	text	body	True		body	body		p10:front_matter:full:white	[255, 255, 255] white	False	[41.16, 64.44, 466.25, 128.26]	Fig. 9(a) -(c) shows the change in the valence states of Mn, Co and Ni ions, respectively, in the Li[Li1/6Mn1/2Ni1/ 6Co1/6]O2 during two cycles and after fifty cycles. It is shown in Fig. 9(a) that the entire edge of th…	Fig. 9(a) -(c) shows the change in the valence states of Mn, Co and Ni ions, respectively, in the Li[Li1/6Mn1/2Ni1/ 6Co1/6]O2 during two cycles and after fifty cycles. It is shown in Fig. 9(a) that the entire edge of th…
10	65	text	body	True		body	body		p10:front_matter:full:white	[255, 255, 255] white	False	[41.16, 193.75, 466.18, 34.84]	Considering the XANES results, it can be concluded that the redox reactions of Ni (Ni 2+ $ Ni 3+ ) ions and Co (Co 3+ $ Co 3.5+ ) are dominant at a 4.1 V plateau during charge/discharge cycles, whereas the valence state…	Considering the XANES results, it can be concluded that the redox reactions of Ni (Ni 2+ $ Ni 3+ ) ions and Co (Co 3+ $ Co 3.5+ ) are dominant at a 4.1 V plateau during charge/discharge cycles, whereas the valence state…
10	66	section_header	body_heading	False	low	body_heading	body_heading		p10:body_zone:left:white	[255, 255, 255] white	False	[41.16, 243.68, 63.93, 8.78]	4. Conclusions	4. Conclusions
10	67	text	body	True		body	body		p10:body_zone:full:white	[255, 255, 255] white	False	[41.16, 267.68, 466.21, 56.54]	As an alternative cathode material to LiCoO2, Li[Li1 x /3Mn2 x /3Ni x /3Co x /3]O2 powders ( x = 0.1, 0.3, 0.5, 0.7 and 0.9) were investigated. The powders were synthesized easily using a sucrose combustion process.…	As an alternative cathode material to LiCoO2, Li[Li1 x /3Mn2 x /3Ni x /3Co x /3]O2 powders ( x = 0.1, 0.3, 0.5, 0.7 and 0.9) were investigated. The powders were synthesized easily using a sucrose combustion process.…
10	68	text	body	True		body	body		p10:body_zone:full:white	[255, 255, 255] white	False	[41.16, 327.5, 466.22, 44.52]	Via XANES spectra measurements, the electrochemical reaction of Ni and Co ions at 4.1 V ions is reversible during charge/discharge cycling. The local environmental change of Mn ions is irreversible during the first cycl…	Via XANES spectra measurements, the electrochemical reaction of Ni and Co ions at 4.1 V ions is reversible during charge/discharge cycling. The local environmental change of Mn ions is irreversible during the first cycl…
10	69	section_header	back_matter_heading	False	low	back_matter_heading	back_matter_heading	stop_trigger	p10:body_zone:left:white	[255, 255, 255] white	False	[41.16, 387.11, 78.62, 8.78]	Acknowledgement	Acknowledgement
10	70	text	body_candidate_excluded	False	medium	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left_crossing:white	[255, 255, 255] white	False	[53.07, 411.17, 240.66, 8.69]	Experiments at PLS were supported in part by POSTECH.	Experiments at PLS were supported in part by POSTECH.
10	71	section_header	back_matter_heading	False	low	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left:white	[255, 255, 255] white	False	[41.16, 434.96, 46.53, 8.78]	References	References
10	72	list_item	affiliation	False	low	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left:white	[255, 255, 255] white	False	[45.13, 458.3, 158.85, 6.95]	K. Ozawa, Solid State Ionics 69 (1994) 212.	K. Ozawa, Solid State Ionics 69 (1994) 212.
10	73	list_item	reference	False	low	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left_crossing:white	[255, 255, 255] white	False	[45.13, 468.28, 305.85, 6.95]	Y.S. Hong, Y.J. Park, K.S. Ryu, S.H. Chang, Y.J. Shin, J. Power Sources 147 (2005) 214.	Y.S. Hong, Y.J. Park, K.S. Ryu, S.H. Chang, Y.J. Shin, J. Power Sources 147 (2005) 214.
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10	75	list_item	reference	False	low	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left_crossing:white	[255, 255, 255] white	False	[45.13, 488.18, 298.37, 6.95]	Y.J. Park, Y.S. Hong, X. Wu, K.S. Ryu, S.H. Chang, J. Power Sources 129 (2004) 288.	Y.J. Park, Y.S. Hong, X. Wu, K.S. Ryu, S.H. Chang, J. Power Sources 129 (2004) 288.
10	76	list_item	reference	False	low	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left:white	[255, 255, 255] white	False	[45.13, 498.16, 199.16, 6.95]	S.H. Kang, K. Amine, J. Power Sources 124 (2003) 533.	S.H. Kang, K. Amine, J. Power Sources 124 (2003) 533.
10	77	list_item	reference	False	low	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left_crossing:white	[255, 255, 255] white	False	[45.13, 508.13, 356.42, 6.95]	Z. Lu, L.Y. Beaulieu, R.A. Donaberger, C.L. Thomas, J.R. Dahn, J. Electrochem. Soc. 149 (2002) A778.	Z. Lu, L.Y. Beaulieu, R.A. Donaberger, C.L. Thomas, J.R. Dahn, J. Electrochem. Soc. 149 (2002) A778.
10	78	list_item	affiliation	False	low	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left:white	[255, 255, 255] white	False	[45.13, 518.06, 207.56, 6.95]	A.D. Robertson, P.G. Bruce, Chem. Mater. 15 (2003) 1984.	A.D. Robertson, P.G. Bruce, Chem. Mater. 15 (2003) 1984.
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10	90	list_item	affiliation	False	low	after_back_matter_stop	after_back_matter_stop	after_stop	p10:body_zone:left:white	[255, 255, 255] white	False	[41.16, 637.62, 206.64, 6.95]	B. Ammundsen, J. Paulsen, J. Adv. Mater. 13 (2001) 943.	B. Ammundsen, J. Paulsen, J. Adv. Mater. 13 (2001) 943.